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Development of transparent colored zirconia ceramics

Research Project

Project/Area Number 16K20496
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Prosthodontics/ Dental materials science and
Research InstitutionOsaka University

Principal Investigator

Usami Hirofumi  大阪大学, 歯学部附属病院, 医員 (30573456)

Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Fiscal Year 2018: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywordsジルコニア / 低温劣化 / 水熱劣化 / ジルコニアブロック / 透光性 / ミストCVD / 透過性 / セラミックス
Outline of Final Research Achievements

High-translucent yttria stabilized tetragonal zirconia (Y-TZP) with less content of alumina than conventional Y-TZP is becoming popular in dentistry in order to realize full-contour zirconia restorations.Although decreasing the amount of alumina addition can increase the translucency, high-translucent Y-TZP may degrade in a humid and low temperature environment such as the oral cavity.The purpose of this study was to evaluate the fitting accuracy and fracture resistance of monolithic zirconia crowns of a new silica-doped Y-TZP.
The experimental 0.2 wt% silica doped Y-TZP sintered at 1500 ℃ showed high-translucency and superior hydrothermal stability.In addition, from the experimental zirconia powder, We made zirconia blocks and was able to make zirconia crowns with a milling machine. We succeeded in making a color with the yellow that was near to teeth color by adding a very small amount of iron oxide in zirconia powder.

Academic Significance and Societal Importance of the Research Achievements

本研究により、イットリア安定型ジルコニア(Y-TZP)の湿潤な環境で劣化する性質を改善することができ、そのモノリシックジルコニアクラウンを製作することができた。また、そのジルコニア粉末から歯質に近い黄色みのある色調を作ることに成功した。
これにより、強度、劣化抵抗性と審美性を兼ね備えたクラウンを製作することが今後可能となり、口腔内でより長期間安定する補綴装置を製作できる可能性が示唆された。

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • 2016 Research-status Report
  • Research Products

    (6 results)

All 2018 2017 2016

All Journal Article (2 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 2 results,  Open Access: 2 results,  Acknowledgement Compliant: 1 results) Presentation (4 results) (of which Int'l Joint Research: 2 results)

  • [Journal Article] Fluorescence of thulium-doped translucent zirconia2018

    • Author(s)
      NAKAMURA Takashi、OKAMURA Shinya、NISHIDA Hisataka、USAMI Hirofumi、NAKANO Yoshiro、WAKABAYASHI Kazumichi、SEKINO Tohru、YATANI Hirofumi
    • Journal Title

      Dental Materials Journal

      Volume: 37 Issue: 6 Pages: 1010-1016

    • DOI

      10.4012/dmj.2017-384

    • NAID

      130007538092

    • ISSN
      0287-4547, 1881-1361
    • Year and Date
      2018-11-27
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Translucency and low-temperature degradation of silica-doped zirconia: A pilot study2016

    • Author(s)
      Nakamura T, Nakano Y, Usami H, Wakabayashi K, Ohnishi H, Sekino T, Yatani H.
    • Journal Title

      Dental Materials Journal

      Volume: 35 Issue: 4 Pages: 571-577

    • DOI

      10.4012/dmj.2015-274

    • NAID

      10025916604

    • ISSN
      0287-4547, 1881-1361
    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] Fluorescence of translucent dental zirconia doped with Thulium2018

    • Author(s)
      Takashi NAKAMURA, Shinya OKAMURA, Hisataka NISHIDA, Hirofumi USAMI, Yoshiro NAKANO, Kazumichi WAKABAYASHI, Tohru SEKINO, Hirofumi YATANI
    • Organizer
      43rdAnnual Meeting of American Academy of Esthetic Dentistry
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 低温劣化を抑制した高透光性ジルコニアの開発2017

    • Author(s)
      中野芳郎,中村隆志,岡村真弥,塩見祥子,天羽康介,宇佐美博文,若林一道,矢谷博文
    • Organizer
      第126回日本補綴歯科学会学術大会
    • Related Report
      2017 Research-status Report
  • [Presentation] Effect of different sintering methods on the fracture resistance of monolithic zirconia crowns after aging.2017

    • Author(s)
      9)Nakano, Y., Nakamura, T., Usami, H., Miyamae, M., Wakabayashi, K. and Yatani H
    • Organizer
      10th World Congress of International Federation of Esthetic Dentistry
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] 低温劣化がシリカ添加高透光性ジルコニアの機械的特性に及ぼす影響2016

    • Author(s)
      中野芳郎,中村隆志,岡 雄造,宇佐美博文, 西田尚敬,若林一道,関野 徹,矢谷博文
    • Organizer
      第67回日本歯科理工学会学術講演会
    • Place of Presentation
      九州大学医学部百年講堂(福岡県福岡市)
    • Year and Date
      2016-04-16
    • Related Report
      2016 Research-status Report

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Published: 2016-04-21   Modified: 2020-03-30  

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