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Development of real-time multi-species laser concentration measurement by standard addition method

Research Project

Project/Area Number 17206018
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Thermal engineering
Research InstitutionNagoya University

Principal Investigator

YOSHIKAWA Norihiko  Nagoya University, Graduate School of Engineering, Professor (60135423)

Co-Investigator(Kenkyū-buntansha) HAYASHI Shigeru  Japan Aerospace Exploration Agency, Aviation Program Group, Clean Engine Them Leader (10358492)
HASEGAWA Tatsuya  Nagoya University, Eco Topia Science Institute, Professor (40164818)
SAITO Hiroyasu  Nagoya University, Graduate School of Engineering, Assistant, Professor (80362284)
Project Period (FY) 2005 – 2007
Project Status Completed (Fiscal Year 2007)
Budget Amount *help
¥37,050,000 (Direct Cost: ¥28,500,000、Indirect Cost: ¥8,550,000)
Fiscal Year 2007: ¥5,980,000 (Direct Cost: ¥4,600,000、Indirect Cost: ¥1,380,000)
Fiscal Year 2006: ¥12,740,000 (Direct Cost: ¥9,800,000、Indirect Cost: ¥2,940,000)
Fiscal Year 2005: ¥18,330,000 (Direct Cost: ¥14,100,000、Indirect Cost: ¥4,230,000)
KeywordsThermal Engineering / Monitoring / Measurement / Pollution protection and control
Research Abstract

New quantitative laser measurement techniques for combustion exhausts were developed using a standard addition method.
1.Laser-Induced Fluorescence(LIF)measurement of nitrogen monoxide(NO)in flames was achieved using a standard addition method. Absorption lines of P_<11>(23.5), P_<21>+Q_<11>(14.5), and Q_<22>+R_<12>(20.5)in A^2Σ^+←X^2 II(0,0) band at 226.03nm were used and the fluorescence intensity of A^2Σ^+←X^2II(0,2)band in 246-248nm were measured. Temperature was determined by two-line method using P_<11>(36.5)line at 225.18 nm and R_<22>(20.5)line at 225.59 nm. Methane-air premixed flames and methane and propane diffusion flames in small burners were examined. The results showed that the new LIF technique provides reliable data. The sampling probe method was not applicable for high temperature combustion gases. The measurement technique was tested for gas turbine exhaust gases. The concentration measu rement gave reliable data. The thermometry was obtained using O<12>(1.5)line at 226.89nm and O^_<12>(19.5)line at 226.90nm line for relatively lower temperature. The selections of the excitation lines were not adequate for getting accurate data.
2.A standard addition measurement technique by Laser-Induced Breakdown Spectroscopy(LIBS)was developed for low-concentration elements in solids. The technique was applied to the element detection in coal burnt ashes. Mass fractions of Mn and Cr were obtained. The mass fraction of Mn was 453±17ppm in good agreement with the other chemical analysis data of 464ppm. The Cr concentration was determined 145ppm by saturation curve fitting. The method was also introduced in the measurement of soil contamination. The concentrations of Cd and Pb were 129±12ppm and 28.7ppm, respectively. It was demonstrated that these techniques are viable diagnostic tools in practical use.

Report

(4 results)
  • 2007 Annual Research Report   Final Research Report Summary
  • 2006 Annual Research Report
  • 2005 Annual Research Report
  • Research Products

    (27 results)

All 2008 2007 2006 2005

All Journal Article (8 results) (of which Peer Reviewed: 3 results) Presentation (19 results)

  • [Journal Article] 燃焼有害排気物の温度・濃度計測(標準添加レーザ誘起蛍光法による一酸化窒素の計測)2008

    • Author(s)
      吉川典彦
    • Journal Title

      日本機械学会誌 111

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Temperature and concentration measurement of hazard combustion exhaust-measurement of nitrogen monoxide by standard addition LIF method (in Japanese)2008

    • Author(s)
      Norihiko, Yoshikawa
    • Journal Title

      Journal of the Japan Society of Mechanical Engineers Vol.111, No.1071

      Pages: 104-107

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] 標準添加LIF画像分光法による火炎中の一酸化窒素の濃度・温度計測2006

    • Author(s)
      奥野和也, 他4名
    • Journal Title

      日本機械学会論文集B編 72

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] 火炎中一酸化窒素濃度分布のレーザー計測(燃焼装置の設計・実時間計測の新しいツール)2006

    • Author(s)
      吉川典彦, 斎藤寛泰, 奥野和也
    • Journal Title

      検査技術 11

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Measurement of concentration and temperature of nitrogen monoxide in flames by standard addition LIF imaging spectroscopy (in Japanese)2006

    • Author(s)
      Kazuya, Okuno, et. al.
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers, Part B Vol.72, No.723

      Pages: 2733-2740

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Laser measurement of concentration distribution of nitrogen monoxide in flames- a new diagnostic tool for design and real- time measurement of combustion devices (in Japanese)2006

    • Author(s)
      Norihiko, Yoshikawa, Hiroyasu, Saito, Kazuya, Okuno
    • Journal Title

      Inspection Engineering Vol.11, No.8

      Pages: 1-4

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] 標準添加LIF画像分光法による火炎中の一酸化窒素の濃度・温度計測2006

    • Author(s)
      奥野和也, 佐野高也, 斎藤寛泰, 吉川典彦, 林茂
    • Journal Title

      目本機械学会論文集 B編 72・723

      Pages: 2733-2740

    • NAID

      110006148752

    • Related Report
      2006 Annual Research Report
  • [Journal Article] 火炎中一酸化窒素濃度分布のレーザー計測(燃焼装置の設計・実時間計測の新しいツール)2006

    • Author(s)
      吉川典彦, 斎藤寛泰, 奥野和也
    • Journal Title

      検査技術 11・8

      Pages: 1-4

    • Related Report
      2006 Annual Research Report
  • [Presentation] ガスタービン排気ガス中一酸化窒素のLIF計測2008

    • Author(s)
      伊東和哉, 他5名
    • Organizer
      日本機械学会東海支部第57期総会・講演会
    • Place of Presentation
      名古屋大学
    • Year and Date
      2008-03-11
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
  • [Presentation] LIF measurements of nitrogen monoxide in gas turbine exhaust (in Japanese)2008

    • Author(s)
      Kazuya, Ito, et. al.
    • Organizer
      57th conference of Tokai section, Japan society of mechanical engineers
    • Place of Presentation
      Nagoya
    • Year and Date
      2008-03-11
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] LIF画像分光法によるジェット燃料火炎中の一酸化窒素濃度・温度計測2007

    • Author(s)
      伊東和哉, 他5名
    • Organizer
      第45回燃焼シンポジウム
    • Place of Presentation
      仙台国際センター
    • Year and Date
      2007-12-06
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
  • [Presentation] LIF measurements of nitrogen monoxide in jet fuel flames by LIF imaging spectroscopy (in Japanese)2007

    • Author(s)
      Kazuya, Ito, et. al.
    • Organizer
      45th Symposium (Japanese) on Combustion
    • Place of Presentation
      Sendai
    • Year and Date
      2007-12-06
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] LIBSによる粉体中微量元素質量分率の計測2007

    • Author(s)
      吉川典彦, 内藤昭仁, 斎藤寛泰
    • Organizer
      工程管理分析の高速化・高精度化のための新しい分析・解析技術
    • Place of Presentation
      東北大学金属材料研究所,仙台
    • Year and Date
      2007-12-04
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Mass fraction measurement of low-concentration elements in powders by LIBS (in Japanese)2007

    • Author(s)
      N. Yoshikawa, A. Naito, H. Saito
    • Organizer
      Symposium on new analytical techniques for process controls
    • Place of Presentation
      Sendai
    • Year and Date
      2007-12-04
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] LIBSによる粉体中微量元素質量分率の計測2007

    • Author(s)
      吉川典彦
    • Organizer
      工程管理分析の高速化・高精度化のための新しい分析・解析技術
    • Place of Presentation
      東北大学金属材料研究所
    • Year and Date
      2007-12-04
    • Related Report
      2007 Annual Research Report
  • [Presentation] 標準添加LIF法によるジェット燃料火炎中の一酸化窒素濃度・温度計測2007

    • Author(s)
      伊東和哉, 他5名
    • Organizer
      可視化情報全国講演会(岐阜2007)
    • Place of Presentation
      岐阜大学工学部
    • Year and Date
      2007-09-27
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
  • [Presentation] Concentration and temperature measurements of nitrogen monoxide in jet fuel flames by standard addition LIF method (in Japanese)2007

    • Author(s)
      Kazuya, Ito, et. al.
    • Organizer
      Visualization society of Japan Symposium in Gifu 2007
    • Place of Presentation
      Gifu
    • Year and Date
      2007-09-27
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Measurement of concentration and temperature distributions in flames by standard addition LIF imaging spectroscopy (in Japanese)2006

    • Author(s)
      Kazuya, Okuno, et. al.
    • Organizer
      43rd Symposium (Japanese) on Combustion
    • Place of Presentation
      Tokyo
    • Year and Date
      2006-12-06
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] LIF画像分光法による火炎中一酸化窒素の濃度・温度計測2006

    • Author(s)
      奥野和也, 他4名
    • Organizer
      第43回日本航空宇宙学会中部・関西支部 合同秋期大会講演会
    • Place of Presentation
      名城大学,名古屋
    • Year and Date
      2006-11-24
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Concentration and temperature measurements of nitrogen monoxide in flames by LIF imaging spectroscopy (in Japanese)2006

    • Author(s)
      Kazuya, Okuno, et. al.
    • Organizer
      43rd fall joint conference of Chubu-Kansai sections of Japan society for aeronautical and space sciences
    • Place of Presentation
      Nagoya
    • Year and Date
      2006-11-24
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] LIBSによる金属粉末中成分の質量分率測定2006

    • Author(s)
      岡田太郎, 他3名
    • Organizer
      日本分光学会レーザー誘起プラズマ分光部会・日本鉄鋼協会次世代鉄鋼迅速オンサイト分析実用化研究会 合同講演会
    • Place of Presentation
      日本経団連会館,東京
    • Year and Date
      2006-11-13
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Mass fraction measurement of metallic powders by LIBS (in Japanese)2006

    • Author(s)
      Taro, Okada, et. al.
    • Organizer
      Joint conference of Japan Spectroscopical society and Steel society
    • Place of Presentation
      Tokyo
    • Year and Date
      2006-11-13
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] 標準添加LIF画像分光法による火炎中の一酸化窒素の濃度・温度分布計測2005

    • Author(s)
      奥野和也, 他4名
    • Organizer
      第43回燃焼シンポジウム
    • Place of Presentation
      タワーホール船堀,東京
    • Year and Date
      2005-12-06
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] 標準添加LIBSによる微量金属元素濃度計測2005

    • Author(s)
      東宮祐介, 吉川典彦
    • Organizer
      平成17年度日本分光学会秋季講演会・シンポジウム
    • Place of Presentation
      島津製作所関西支社マルチホール,大阪
    • Year and Date
      2005-11-16
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Measurement of low concentration metallic elements by laser-induced breakdown spectroscopy (in Japanese)2005

    • Author(s)
      Yusuke, Tohmiya, Norihiko, Yoshikawa
    • Organizer
      Spectroscopical society of Japan fall symposium
    • Place of Presentation
      Osaka
    • Year and Date
      2005-11-16
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Absolute Concentration Measurement of Nitrogen Oxide in Flames by LIF Standard Addition Method2005

    • Author(s)
      N. Yoshikawa, et. al.
    • Organizer
      20th International Colloquium on the Dynamics of Explosions and Reactive Systems
    • Place of Presentation
      マクギル大学,モントリオール,カナダ
    • Year and Date
      2005-08-01
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Absolute concentration measurement of nitrogen oxide in flames by LIF standard addition method (in Japanese)2005

    • Author(s)
      N. Yoshikawa, et. al.
    • Organizer
      20th International Colloquium on the Dynamics of Explosions and Reactive Systems
    • Place of Presentation
      McGillUniversity, Montreal, Canada
    • Year and Date
      2005-08-01
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary

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Published: 2005-04-01   Modified: 2016-04-21  

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