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Development of High Resolution Magnetic Force Microscopy with High Sensitivity and Low Noise and Its Application to Nano-scale Magnetic Imaging

Research Project

Project/Area Number 17360036
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Applied physics, general
Research InstitutionAkita University

Principal Investigator

SAITO Hitoshi  Akita University, Faculty of Engineering and Resource Science, Professor, 工学資源学部, 教授 (00270843)

Co-Investigator(Kenkyū-buntansha) ISHIO Shunji  Akita University, Vice-president, 副学長 (90134006)
PEI Wenli  Akita University, Venture Business Laboratory, Post-doctoral fellow researcher, ベンチャー・ビジネス・ラボラトリー, 中核的研究機関研究員 (10375230)
Project Period (FY) 2005 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥15,100,000 (Direct Cost: ¥15,100,000)
Fiscal Year 2006: ¥6,100,000 (Direct Cost: ¥6,100,000)
Fiscal Year 2005: ¥9,000,000 (Direct Cost: ¥9,000,000)
KeywordsMagnetic force microscopy / Magnetic domain observation / Spatial resolution / Low temperature MFM / MFM tip / Nano material / Magnetic recording media / 交換スプリング磁石 / シミュレーション / 保磁力マッピング
Research Abstract

Magnetic force microscopy (MFM) is widely used for magnetic domain observation. However the spatial resolution of commercial MFM is about several 10nm and is not enough to observe the recording bits of high density recording media. The purpose of this study is development of high resolution MFM and its application to nano-scale magnetic imaging. The following results were obtained.
1. Development of high resolution MFM
(1.1) Low noise MFM using tip cooling
Low noise MFM was developed by adding the tip cooling equipment to high vacuum MFM. The noise of the MFM was reduced to the theoretical limit of thermodynamic noise of MFM cantilever by cooling a tip. The MFM can decrease the tip temperature and sample temperature to 42K and 32K, respectively. Low noise measuring condition can be obtained within 1 hour.
(1.2) Fabrication of high resolution MFM tips
High-coercivity tip was fabricated by depositing FePt film on a surface oxidized Si tip made by O_2 plasma oxidation treatment and post-annealing of the tip. The coercivity of the tip is above 15 kOe and MFM resolution is about 10 nm. For further improvement of MFM resolution, a new high-resolution MFM tip using the cross section of an exchange-spring trilayer film [hard (low M_s) /soft (high M_s)/hard (low M_s)] was proposed and clarified the theoretical resolution is less than 5 nm by computer simulation. FePt/FeCo/FePt trilayers was fabricated for the application of MFM tip.
2. Nano-scale magnetic imaging of high density magnetic recording media
Medium noise-coercivity overlapping method was developed by using magnetic force microscopy and was used to study the origin of medium noise of 400~600 Gbit/inch^2 class perpendicular media. It was made clear that medium noise arises from (1) a spatial fluctuation of magnetization reversal filed in the media, where fluctuation length extends to about 100nm, (2) an insufficient magnetic field gradient of recording head.

Report

(3 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • Research Products

    (33 results)

All 2007 2006 2005

All Journal Article (29 results) Book (2 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Study on magnetization reversal of perpendicular recording media by in-field MFM observation2007

    • Author(s)
      W.Pei, J.Yuan, T.Wang, Y.Fu, T.Washiya, T.Hasegawa, H.Saito, S.Ishio, N.Honda
    • Journal Title

      Acta Materialia (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Simulation of high-resolution MFM tip using exchange-spring magnet2007

    • Author(s)
      H.Saito, D.Yatsuyanagi, S.Ishio, A.Ito, H.Kawamura, K.Ise, K.Taguchi, S.Takahashi
    • Journal Title

      J. Magn. Magn. Mater. Vol.310

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Study on magnetite nanoparticles synthesized by chemical method2007

    • Author(s)
      W.Pei, H.Kumada, T.Natusme, H.Saito, S.Ishio
    • Journal Title

      J. Magn. Magn. Mater. Vol.310

      Pages: 2375-2377

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Study on magnetization reversal of perpendicular recording media by in-field MFM observation2007

    • Author(s)
      W.Pei, J.Yuan, T.Wang, Y.Fu, T.Washiya, T.Hasegawa, H.Saito, S.Ishio, N.Honda
    • Journal Title

      Acta Materialia (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Simulation of high-resolution MFM tip using exchange-spring magnet.2007

    • Author(s)
      H.Saito, D.Yatsuyanagi, S.Ishio, A.Ito, H.Kawamura, K.Ise, K.Taguchi, S.Takahashi
    • Journal Title

      J.Magn.Magn., Mater. Vol.310

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Study on magnetite nanoparticles synthesized by chemical method.2007

    • Author(s)
      W.Pei, H.Kumada, T.Natusme, H.Saito, S.Ishio
    • Journal Title

      J.Magn.Magn.Mater. Vol.310

      Pages: 2375-2377

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Study on magnetization reversal of perpendicular recording media by in-field MFM observation2007

    • Author(s)
      W.Pei, J.Yuan, T.Wang, Y.Fu, T.Washiya, T.Hasegawa, H.Saito, S.Ishio, N.Honda
    • Journal Title

      Acta Materialia 印刷中

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Simulation of high-resolution MFM tip using exchange-spring magnet2007

    • Author(s)
      H.Saito, D.Yatsuyanagi, A.Ishito, A.Ito, H.Kawamura, K.Ise, K.Taguchi, S.Takahashi
    • Journal Title

      J. Magn. Magn. Mater. Vol.310

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Magnetic reversal field map combined with medium noise analysis in CoCrPt-SiO_2 granular perpendicular recording medium2006

    • Author(s)
      S.Ishio, T.Washiya, H.Saito, J.Bai, W.Pei
    • Journal Title

      J. Appl. Phys. Vol.99

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Structural transition from L1_0 phase to A1 phase in FePt films caused by ion irradiation2006

    • Author(s)
      T.Hasegawa, G.Q.Li, W.Pei, H.Saito, S.Ishio, K.Taguchi, K.Yamakawa, N.Honda, K.Ouchi, T.Aoyama, I.Sato
    • Journal Title

      J. Appl. Phys. Vol.99

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Anomalous magnetization processes and non-symmetrical domain wall displacements in L1_0 FePt particulate films2006

    • Author(s)
      G.Q.Li, H.Saito, S.Ishio, T.Shima, K.Takanashi
    • Journal Title

      J. Magn. Magn. Mater. Vol.303

      Pages: 14-19

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Magnetic reversal field map combined with medium noise analysis in CoCrPt-SiO_2 granular perpendicular recording medium.2006

    • Author(s)
      S.Ishio, T.Washiya, H.Saito, J.Bai, W.Pei
    • Journal Title

      J.Appl.Phys. Vol.99

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Structural transition from L1_0 phase to Al phase in FePt films caused by ion irradiation.2006

    • Author(s)
      T.Hasegawa, G.Q.Li, W.Pei, H.Saito, S.Ishio, K.Taguchi, K.Yamakawa, N.Honda, K.Ouchi, T.Aoyama, I.Sato
    • Journal Title

      J.Appl.Phys. Vol.99

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Anomalous magnetization processes and non-symmetrical domain wall displacements in L1_0 FePt particulate films.2006

    • Author(s)
      G.Q.Li, H.Saito, S.Ishio, T.Shima, K.Takanashi
    • Journal Title

      J.Magn.Magn.Mater. Vol.303

      Pages: 14-19

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Structural transition from Ll_0 phase to Al phase in FePt films caused by ion irradiation2006

    • Author(s)
      T.Hasegawa, G.Q.Li, W.Pei, H.Saito, S.Ishio, K.Taguchi, K.Yamakawa, N.Honda, K.Ouchi, T.Aoyama, I.Sato
    • Journal Title

      J. Appl. Phys. Vol.99

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Anomalous magnetization processes and non-symmetrical domain wall displacements in L1_0 FePt particulate films2006

    • Author(s)
      G.Q.Li, H.Saito, S.Ishio, T.Shima, K.Takanashi
    • Journal Title

      J.Magn.Magn.Mater. (In Press)

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Low-noise magnetic force microscopy with high resolution by tip cooling2005

    • Author(s)
      H.Saito, R.Sunahara, Y.W.Rheem, S.Ishio
    • Journal Title

      IEEE Trans. Magn. Vol.41, No.12

      Pages: 4394-4396

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Fabrication of FePt/FeCo/FePt exchange spring trilayer with very thin FeCo layer for high resolution MFM tips2005

    • Author(s)
      Y.W.Rheem, H.Saito, S.Ishio
    • Journal Title

      IEEE Trans. Magn. Vol.41, No.10

      Pages: 3793-3795

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Simulation of high resolution MFM tips for high density magnetic recording media with low bit aspect ratio2005

    • Author(s)
      H.Saito, Y.W.Rheem, S.Ishio
    • Journal Title

      J. Magn. Magn. Mater. Vol.287

      Pages: 102-106

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 高分解能MFMの開発 : 低ノイズ化と高分解能探針の作製2005

    • Author(s)
      齊藤準, 夏目貴史, 砂原亮介, 林映雨, 石尾俊二
    • Journal Title

      日本応用磁気学会誌 29巻,8号

      Pages: 773-778

    • NAID

      110002811834

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Low-noise magnetic force microscopy with high resolution by tip cooling.2005

    • Author(s)
      H.Saito, R.Sunahara, Y.W.Rheem, S.Ishio
    • Journal Title

      IEEE Trans.Magn. Vol.41, No.12

      Pages: 4394-4396

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Fabrication of FePt/FeCo/FePt exchange spring trilayer with very thin FeCo layer for high resolution MFM tips.2005

    • Author(s)
      Y.W.Rheem, H.Saito, S.Ishio
    • Journal Title

      IEEE Trans.Magn. Vol.41, No.10

      Pages: 3793-3795

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Simulation of high resolution MFM tips for high density magnetic recording media with low bit aspect ratio.2005

    • Author(s)
      H.Saito, Y.W.Rheem, S.Ishio
    • Journal Title

      J.Magn.Magn.Mater. Vol.287

      Pages: 102-106

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Reduction of noise and fabrication of high-resolution tips for a high-resolution magnetic force microscope.2005

    • Author(s)
      Hitoshi Saito, Takashi Natsume, Ryosuke Sunahara, Y.W.Rheem, Shunji Ishio
    • Journal Title

      J.Magn.Soc.Jpn. Vol.29, No.8

      Pages: 773-778

    • NAID

      110002811834

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Low noise MFM with high resolution by tip cooling2005

    • Author(s)
      H.Saito, R.Sunahara, Y.W.Rheem, S.Ishio
    • Journal Title

      IEEE Trans. Magn. 41・12

      Pages: 4394-4396

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Fabrication of FePt/FeCo/FePt exchange spring trilayer with very thin FeCo layer for high resolution MFM tips2005

    • Author(s)
      Y.W.Rheem, H.Saito, S.Ishio
    • Journal Title

      IEEE Trans. Magn. 41・10

      Pages: 3793-3795

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Simulation of high resolution MFM tips for high density magnetic recording media with low bit aspect ratio2005

    • Author(s)
      H.Saito, Y.W.Rheem, S.Ishio
    • Journal Title

      J.Magn.Magn.Mater. 287

      Pages: 102-106

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Mechanism of magnetization process of island-like L1_0 FePt films2005

    • Author(s)
      G.Q.Li, H.Takahoshi, H.Ito, T.Washiya, H.Saito, S.Ishio, T.Shima, K.Takanashi
    • Journal Title

      J.Magn.Magn.Mater. 287

      Pages: 219-223

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 高分解能MFMの開発:低ノイズ化と高分解能探針の作製(解説)2005

    • Author(s)
      齊藤準, 夏目貴史, 砂原亮介, 林映雨, 石尾俊二
    • Journal Title

      日本応用磁気学会誌 29・8

      Pages: 773-778

    • Related Report
      2005 Annual Research Report
  • [Book] ナノマテリアル工学大系第2巻ナノ金属2005

    • Author(s)
      石尾俊二
    • Total Pages
      6
    • Publisher
      フジテクノシステム
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Book] Nanomaterial Engineering Compendium, Vol.2, Nano-metal2005

    • Author(s)
      Shunji Ishio
    • Publisher
      Fujitec Corporation
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 磁気力顕微鏡用の磁性探針の製造方法2007

    • Inventor(s)
      斉藤準, 石尾俊二, 川村博, 伊藤亮
    • Industrial Property Rights Holder
      秋田大学, 日東光器(株)
    • Industrial Property Number
      2007-046962
    • Filing Date
      2007-02-27
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 磁気力顕微鏡用の磁性探針及びその製造方法2006

    • Inventor(s)
      石尾俊二, 斉藤準, 林映雨
    • Industrial Property Rights Holder
      秋田大学
    • Patent Publication Number
      2006-084449
    • Acquisition Date
      2006-03-30
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary

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Published: 2005-04-01   Modified: 2016-04-21  

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