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Synthesis of a novel functional monomer and development of an adhesive system appropriate to laser-irradiated dental tissues

Research Project

Project/Area Number 17390517
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field 補綴理工系歯学
Research InstitutionOkayama University

Principal Investigator

SUZUKI Kazuomi  Okayama University, Med. Dent. and Pharm Okayama Univ, Prof (30050058)

Co-Investigator(Kenkyū-buntansha) YOSHIDA Yasuhiro  Okayama Univ, Med. Dent. and Pharm, Associate Prof (90281162)
IRIE Masao  Okayama Univ, Med. Dent. and Pharm, Assistant Prof (90105594)
TANAKA Jiro  Okayama Univ, Med. Dent. and Pharm, Assistant Prof (40171764)
NISHIYAMA Norihiro  Dentistry Nihon Univ, Matsudo, Prof. (90112953)
KUBOKI Takuo  Okayama Univ, Med. Dent. and Pharm, Prof. (00225195)
峯 篤吏  岡山大学, 医学部歯学部附属病院, 助手 (60379758)
Project Period (FY) 2005 – 2007
Project Status Completed (Fiscal Year 2007)
Budget Amount *help
¥16,390,000 (Direct Cost: ¥15,700,000、Indirect Cost: ¥690,000)
Fiscal Year 2007: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Fiscal Year 2006: ¥2,400,000 (Direct Cost: ¥2,400,000)
Fiscal Year 2005: ¥11,000,000 (Direct Cost: ¥11,000,000)
KeywordsDentin / Laser / Tooth restoration / Composite resin / Adhesion / Surface treatment / Polymer synthesis / Functional monomer / コンポレットレジン / 機械性モノマー
Research Abstract

Introduction: The use of Er:YAG laser for catty preparations during treatment of dental caries has received attention because there is no unpleasantness of noise and vibration as with air turbine and micromotor, and there is no need of anesthesia for treatment. However, we found that conventional dental adhesive systems do not perform sufficiently well on Er:YAG laser irradiated dental surfaces, and moreover, one of its reasons is the weakness of dental surfaces after laser irradiation. So, due to its importance and clinical significance, we aimed to clarify the dental structure after Er:YAG laser irradiation and its quality as an adhesive surface, along with the development of a new adhesive system appropriate to this surface.
Materials and Methods: 1) Adhesive surfaces preparation: Er:YAG laser (Erwin, Morita Co.) was irradiated with 127mJ, 10pps for 2 sec for enamel and with 69mJ, 10pps for 2 sec for dentin. 2) The primers of the adhesive systems were prepared with triazine-, aminoac … More id-, and epoxy-methacrylate/HEMA and alcohol. 3) The adhesive surfaces above were treated with each type of primer, phosphoric acid esther bonding agent and filled with composite resin (Clearfil APX, Kuraray Co.), then immersed in water at 37□for 24 hours before bond strength measurements.
Results and Discussion: The bond strength of epoxy type primer system to Er:YAG laser irradiated dental adhesive surfaces was 18.6MPa for enamel (control: Megabond/Kuraray Co.; 12MPa), and 17.2MPa for dentin (control: 9MPa). The authors say that these results may be due to oxygen that exists in the space created by microcracks that occurred during laser irradiation of dental adhesive surfaces. As conventional dental adhesives, used in the control group, are of radical polymerization type, the polymerization reaction decrease remarkably in the presence of oxygen. On the other hand, the ring opening polymerization type resin tested in this study may be not much influenced by the presence of oxygen during reaction. Less

Report

(4 results)
  • 2007 Annual Research Report   Final Research Report Summary
  • 2006 Annual Research Report
  • 2005 Annual Research Report
  • Research Products

    (14 results)

All 2008 2007 2006

All Journal Article (12 results) (of which Peer Reviewed: 4 results) Presentation (2 results)

  • [Journal Article] Class I gap-formation with highly-viscous glass-ionomer restorations minimized by delayed polishing2008

    • Author(s)
      Irie, M., et. al.
    • Journal Title

      Operative Dentistry 33

      Pages: 196-202

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Surface Treatment with N,N'-Dimethacryloylcystine for Enhanced Bomding of Resin to Dental Alloys2007

    • Author(s)
      Tanaka. J., et. al.
    • Journal Title

      Dental Materials Journa, 26

      Pages: 514-518

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Antonucci, Kazuomi Suzuki : Surface Treatment with N,N - Dimethacryloyleystine for Enhanced Bomding of Resin to Dental Alloys2007

    • Author(s)
      Jiro, Tanaka, Jeffery, W., Stansbury, Joseph, M
    • Journal Title

      Dental WaterialsJournal 26(4)

      Pages: 514-518

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] In vitro study of 24-hour flexural and shear bond strength of flowable light-cured composites:A comparison analysis using Weibull statistics2007

    • Author(s)
      T jandrawinata, R., et. al.
    • Journal Title

      Dental Materias Journal 26

      Pages: 589-597

    • Related Report
      2007 Annual Research Report
  • [Journal Article] Spectroscopic characterization of enamel surfaces irradiated with Er: YAG laser.2006

    • Author(s)
      Mine, A., et. al.
    • Journal Title

      Dental Materials Journal 25

      Pages: 214-218

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Chemical interacyion of phosphoric acid ester with hydroxyapatite.2006

    • Author(s)
      Fukegawa, D., et. al.
    • Journal Title

      Journal of Dental Research 85

      Pages: 941-944

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Spectroscopic characterization of enamel surfaces irradiated with Er : YAG laser2006

    • Author(s)
      Mine, A., Yoshida, Y., Suzuki, K., Nakayama, Y., Yatani, H., Kuboki, T
    • Journal Title

      Dental Materials journal 25

      Pages: 214-218

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Chemical interacyion of phosphoric acid ester with hydroxyapatite2006

    • Author(s)
      Fukegawa, D., Hayakawa, S., Yoshida,Y., Suzuki, K., Osaka, A., Van Meerbeek, B
    • Journal Title

      Journal of Dental Research 85

      Pages: 941-944

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Root-surface gap-formation with RMGIC restorations minimized by reduced P/L ratio of the first increment and delayed polishing2006

    • Author(s)
      Irie, M., et al.
    • Journal Title

      Dental Materials Vol.22,No5

      Pages: 486-497

    • NAID

      120002311447

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Effect of surface pre-treatment on durability of resin-based cements bonded to titanium.2006

    • Author(s)
      Tsuchimoto Y., et al.
    • Journal Title

      Dental Materials Vol.22,No6

      Pages: 545-552

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Chemical interaction of phosphoric acid ester with hydroxyapatite.2006

    • Author(s)
      Fukegawa, D., et al.
    • Journal Title

      Journal of Dental Research Vol.85,No11

      Pages: 941-944

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Spectroscopic Characterization of Enamel surfaces irradiated with Er:YAG Laser.2006

    • Author(s)
      Mine, A., et al.
    • Journal Title

      Dental Materials Journal Vol.25,No2(in press)

    • NAID

      110004757969

    • Related Report
      2005 Annual Research Report
  • [Presentation] Effect of Delayed Polishing on Interfacial Gap-formation in Posterior Composites2006

    • Author(s)
      Irie. M., et. al.
    • Organizer
      84th Annual Meeting & Exhibition of the IADR
    • Place of Presentation
      Brisbane Convention & Exhibition Centre, Brisbane, Australia
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Watts : Effect of Delayed Polishing on Interfacial Gap-formation in Posterior Composites, # 0630, 20062006

    • Author(s)
      M., Irie, K., Suzuki, David, C
    • Organizer
      #0630, 84th Annual Meeting & Exhibition of the IADR
    • Place of Presentation
      Brisbane Convention & Exhibition Centre, Brisbane, Australia
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary

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Published: 2005-04-01   Modified: 2016-04-21  

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