• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

Measurement and control of cooling/synthesis processes of carbon clusters in an arc reactor

Research Project

Project/Area Number 17540467
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Plasma science
Research InstitutionShizuoka University

Principal Investigator

MIENO Tetsu  Shizuoka University, Dept. Physics, Faculty of Science, Professor, 理学部, 教授 (50173993)

Co-Investigator(Kenkyū-buntansha) USUBA Shu  Shizuoka University, Advanced Industrial Science & Technology, Researcher, 研究員 (90160259)
Project Period (FY) 2005 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2006: ¥1,400,000 (Direct Cost: ¥1,400,000)
Fiscal Year 2005: ¥2,300,000 (Direct Cost: ¥2,300,000)
Keywordsnanotube / fullerene / arc discharge / thermal convection / production process / Mie scattering / carbon cluster / nano-material / 無重力合成 / 宇宙空間利用 / 合成過程測定 / ナノチューブ・フラーレン / プラズマ合成 / 気相反応 / 宇宙空間 / 無重力 / 拡散冷却
Research Abstract

1) Passive Mie scattering experiment
Under normal gravity condition, an obstacle plate is set in a reactor, and dispersed light is recorded by a CCD camera. It is found that about 0.5 micrometer size of carbon clusters generate around the arc plasma, and they flow upwards by natural heat convection (v~0.5 m/s). This flow is in good consistent with the result of fluid simulation. The generation place of carbon clusters is around the plasma, where the gas temperature decreases from 8000 K to less than 1200 K.
2) Active Mie scattering experiment
Laser light is irradiated from bottom side to upper side through center of the arc plasma. 90 degree-scattered laser-light is detected and processed by the pulse-modulation technique and the Lock'in amplification technique. As a result, larger signal is obtained according to the discharge current and the He-gas pressure. Vertical distribution of the scattered intensity changes a little above the arc plasma.
3) Production process of single-walled carbon nanotubes
A 8-ch cluster-collector is set aside of the arc plasma, and coming carbon particles are collected at the each position. From this measurement, spatial distribution of nanotubes is measured. As a result, nanotubes are almost produced around the periphery of the arc plasma, where the gas temperature sharply decreases.
4) Gas flow and production of multi-walled carbon nanotubes by a thermal CVD method
In a vertically set glass tube, a small steel-ball is set, on which Ni-catalyst-powder is coated. By flowing Ar gas and ethanol gas, and by 800 C of thermal heating, we could make carbon nanotubes. Depending on the flow direction of hydrocarbon gas,
nanotube-density is changed.

Report

(3 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • Research Products

    (47 results)

All 2007 2006 2005

All Journal Article (42 results) Book (5 results)

  • [Journal Article] Gravity Effect on the Gas Evaporation Synthesis of Fullerenes2007

    • Author(s)
      S.Usuba, Y.Kakudate, T.Mieno
    • Journal Title

      J. Jpn. Microgravity Appl. Vol. 24

      Pages: 26-32

    • NAID

      10018498622

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Gravity Effect on the Gas Evaporation Synthesis of Fullerenes", 13 papers2007

    • Author(s)
      S.Usuba, Y.Kakudate, T.Mieno
    • Journal Title

      J. Jpn. Microgravity Appl. 24

      Pages: 26-32

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Production of carbon clusters by means of the gravity-free arc discharge" (in Japanese)2007

    • Author(s)
      T.Mieno
    • Journal Title

      J. Plasma & Fusion Res. ( Special article sin Japanese) Vol. 83, No. 2

      Pages: 151-156

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 無対流アーク放電による炭素クラスター合成2007

    • Author(s)
      三重野 哲
    • Journal Title

      J. Plasma & Fusion Res.(プラズマ・核融合学会誌) 83巻、2号

      Pages: 151-156

    • NAID

      110006282230

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Gravity Effect on the Gas Evaporation Synthesis of Fullerenes2007

    • Author(s)
      S.Usuba, Y.Kakudate, T.Mieno
    • Journal Title

      J. Jpn. Soc. Microgravity Appl. 24巻、1号

      Pages: 26-32

    • NAID

      10018498622

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Gravity-free Production of Carbon Clusters by Arc Discharge Using a Vertical-Swing-Tower and a Jet Plane2006

    • Author(s)
      T.Mieno, A.Yamashiro, D.Kato
    • Journal Title

      Proc. 8th Int. Workshop on Short-Term Experiments under Strongly Reduced Gravity Conditions, 2006

      Pages: 33-34

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Thermal motion of carbon clusters and production of carbon nanotubes by gravity-free arc discharge2006

    • Author(s)
      T.Mieno, M.Takeguchi
    • Journal Title

      J. Appl. Phys. Vol. 99

    • NAID

      120001698997

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Diffusion and Reaction of Carbon Clusters in Gas Phase for Production of Carbon Nanotubes2006

    • Author(s)
      T.Mieno
    • Journal Title

      New Diamond and Frontier Carbon Technol (Review paper) Vol. 16

      Pages: 139-150

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Explosion Production of Fullerenes from Carbonaceous Bullet in Vacuum Using Rail Gun2006

    • Author(s)
      T.Mieno, A.Yamori
    • Journal Title

      Jpn. J. Appl. Phys. Vol. 45

      Pages: 2768-2770

    • NAID

      40007227508

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Measurement of Synthesis and Diffusion of Carbon Nanotubes in the Arc Discharge by the Mie-Scattering Method and the Sampling Method2006

    • Author(s)
      T.Mieno, D.Kato, K.Koga, M.Shiratani
    • Journal Title

      Abstract 8th Asia-Pacific Conf. Plasma Sci. Technol., Cairns

      Pages: 178-178

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Production of Carbon Clusters by Collisional Bullet-Target Explosion Using a Rail-Gun2006

    • Author(s)
      T.Mieno, S.Hasegawa, A.Yamori
    • Journal Title

      Abstract 8th Asia-Pacific Conf. Plasma Sca. Technol., Cairns

      Pages: 179-179

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Modification of dielectric properties of C_<60>, C_<70> and C_<84> thin films by oxygen absorption2006

    • Author(s)
      K.Hassan Bhuiyan, T.Mieno
    • Journal Title

      Thin Solid Films Vol. 506-507

      Pages: 239-243

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Gravity-free Production of Carbon Clusters by Arc Discharge Using a Vertical-Swing-Tower and a Jet Plane"2006

    • Author(s)
      T.Mieno, A.Yamashiro, D.Kato
    • Journal Title

      Proc. 8th Int. Workshop on Short-Term Experiments under Strongly Reduced Gravity Conditions, 2006. Oct. 30-Nov. 1

      Pages: 33-34

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Thermal motion of carbon clusters and production of carbon nanotubes by gravity-free arc discharge"2006

    • Author(s)
      T.Mieno, M.Takeguchi
    • Journal Title

      J. Appl. Phys. 99

    • NAID

      120001698997

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Diffusion and Reaction of Carbon Clusters in Gas Phase for Production of Carbon Nanotubes2006

    • Author(s)
      T.Mieno
    • Journal Title

      New Diamond and Frontier Carbon Technol. 16(Review Paper).

      Pages: 139-150

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Explosion Production of Fullerenes from Carbonaceous Bullet in Vacuum Using Rail Gun"2006

    • Author(s)
      T.Mieno, A.Yamori
    • Journal Title

      Jpn. J. Appl. Phys. 45

      Pages: 2768-2770

    • NAID

      40007227508

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Measurement of Synthesis and Diffusion of Carbon Nanotubes in the Arc Discharge by the Mie-Scattering Method and the Sampling Method"2006

    • Author(s)
      T.Mieno, D.Kato, K.Koga, M.Shiratani
    • Journal Title

      Abstract 8th Asia-Pacific Conf. Plasma Sci. Technol., Cairns, 2006. July 2-6

      Pages: 178-178

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Production of Carbon Clusters by Collisional Bullet-Target Explosion Using rail-Gun2006

    • Author(s)
      T.Mieno, S.Hasegawa, A.Yamori
    • Journal Title

      Abstract 8th Asia-Pacific Conf.. Plasma Sci. Technol., Cairns, 2006. July 2-6

      Pages: 179-179

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Modification of dielectric properties of C60, C70 and C84, thin films by oxygen absorption"2006

    • Author(s)
      K.Hassan Bhuiyan, T.Mieno
    • Journal Title

      Thin Solid Films 506-407

      Pages: 239-243

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Diffusion and Reaction of Carbon Clusters in Gas Phase for Production of Carbon Nanotubes2006

    • Author(s)
      Tetsu Mieno
    • Journal Title

      New Diamond and Frontier Carbon Technology (Review) 16巻、3号

      Pages: 139-150

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Thermal motion of carbon clusters and production of carbon nanotubes by gravity-free arc discharge2006

    • Author(s)
      T.Mieno, M.Takeguchi
    • Journal Title

      J. Appl. Phys. 99巻

    • NAID

      120001698997

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Measurement of Synthesis and Diffusion of Carbon Nanotubes in the Arc Discharge by the Mie-scattering Method and the Sampling Method2006

    • Author(s)
      T.Mieno, D.Kato, K.Koga, M.Shiratani
    • Journal Title

      Abstract 8^<th> Asia-Pacific Conf. Plasma Sci. Technol. (Cairns, Australia, 2-5th, July, 2006) 1巻

      Pages: 178-178

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Gravity-free Production of Carbon Clusters by Arc discharge Using a Vertical-Swing-Tower and a Jet plane2006

    • Author(s)
      T.Mieno, A.Yamashiro, D.Kato
    • Journal Title

      Abstract 8^<th> Int. Workshop on Short-Term Experiments under Strongly Reduced Gravity Conditions 1巻

      Pages: 33-34

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Explosion Production of Fullerenes from Carbonaceous Bullet in Vacuum Using Rail Gun2006

    • Author(s)
      T.Mieno, A.Yamori
    • Journal Title

      Jpn.J.Appl.Phys Vol.45, 4A(in press)

      Pages: 1-3

    • NAID

      40007227508

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Thermal motion of carbon clusters and production of carbon nanotubes by gravity-free arc discharge2006

    • Author(s)
      T.Mieno, M.Takeguchi
    • Journal Title

      J.Appl.Phys. Vol.100(in press)

    • NAID

      120001698997

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Gravity Effect on the Gas Evaporation Synthesis of Fullerenes2005

    • Author(s)
      S.Usuba, Y.Kakudate, T.Mieno
    • Journal Title

      Proc. 6th Japan/China Workshop on Microgravity Science, Saga

      Pages: 147-148

    • NAID

      10018498622

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Efficient Mass-Production of Fullerenes and Carbon Nanotubes by the JxB Arc Discharge Method2005

    • Author(s)
      T.Mieno, K.H.Bhuiyan, N.Matsumoto
    • Journal Title

      Proc. Inter-academia 2005, Wuppertal Vol. 1

      Pages: 123-132

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Efficient production offullerenes and nanotubes by means of the JxB gas-arc discharge2005

    • Author(s)
      T.Mieno, N.Matsumoto, Md.K.Hassan Bhuiyan, T.Sakamoto, M.Takeguchi
    • Journal Title

      Proc. 17th Int. Sympo. Plasma Chemistry, Toronto

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Thermal properties of gravity-free gas-arc discharge and its application to production of carbon clusters2005

    • Author(s)
      T.Mieno, D.Kato, A.Yamori
    • Journal Title

      Proc. 17th Int. Sympo. Plasma Chemistry, Toronto

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Carbon nanotubes and onions as lubricant additives2005

    • Author(s)
      L.Joly-Pottuz, J.M.Martin, F.Dassnoy, B.Vacher, T.Mieno, N.Ohmae
    • Journal Title

      Proc. World Tribology Conf. 2005

      Pages: 1-2

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Gravity Effect on the Gas Evaporation Synthesis of Fullerenes"2005

    • Author(s)
      S.Usuba, Y.Kakudate, T.Mieno
    • Journal Title

      Proc. 6th Japan/China Workshop on Microgravity Science, Saga, 2005. Oct. 22-25

      Pages: 147-148

    • NAID

      10018498622

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Efficient Mass-Production of Fullerenes and Carbon Nanotubes by the JxB Arc Discharge Method"2005

    • Author(s)
      T.Mieno, K.H.Bhuiyan, N.Matsumoto
    • Journal Title

      Proc. Inter-academia 2005, Wuppertal, 2005. Sep. 19-22, 1

      Pages: 123-132

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Efficient production of fullerenes and nanotubes by means of the JxB gas-arc discharge"2005

    • Author(s)
      T.Mieno, N.Matsumoto, Md.K.Hassan Bhuiyan, T.Sakamoto, M.Takeguchi
    • Journal Title

      Proc. 17th Int. Sympo. Plasma Chemistry, Toronto, 2005. Aug. 7-12(Proc. No. A7/108).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Thermal properties of gravity-free gas-arc discharge and its application to production of carbon clusters"2005

    • Author(s)
      T.Mieno, D.Kato, A.Yamori
    • Journal Title

      Proc. 17th Int. Sympo. Plasma Chemistry, Toronto, 2005 Aug. 7-12(Proc. No. F5/109).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Carbon nanotubes and onions as lubricant additives",2005

    • Author(s)
      L.Joly-Pottuz, J.M.Martin, F.Dassnoy, B.Vacher, T.Mieno, N.Ohmae
    • Journal Title

      Proc. World Tribology Conf. 2005, Sep. 12-16, Washington

      Pages: 1-2

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] THERMAL PROPERTIES OF GRAVITY-FREE GAS-ARC DISCHARGE MEASURED IN A JET PLANE AND ITS APPLICATION TO NANO-TUBE PRODUCTION2005

    • Author(s)
      T.Mieno, T.Mizutani, M.Takeguchi
    • Journal Title

      Novel Materials Processing by Advanced Electromagnetic Energy Sources, Ed. S. Miyake, (Elsevier BV, Amsterdam)

      Pages: 45-48

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Production of single-walled carbon nanotubes under gravity-free condition" (in Japanese)2005

    • Author(s)
      T.Mieno, M.Takeguchi
    • Journal Title

      NEW DIAMOND, (Topics in Japanese) Vol. 21, No. 3

      Pages: 26-27

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] ナノチューブの無重力アーク合成における微粒子の発生と拡散2005

    • Author(s)
      三重野哲, 竹口雅樹
    • Journal Title

      Space Utiliz.Res.(Proc.22th Space Utilization Sympo.)(Tokyo) Vol.22

      Pages: 32-35

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Thermal Properties of Gravity-free Arc discharge and Its Application to Production of Carbon Clusters2005

    • Author(s)
      T.Mieno, D.Kato, A.Yamashiro
    • Journal Title

      Proc.17^<th> Int.Sympo.Plasma Chem., (Tronto, 2005) Vol.1(CD)

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Efficient Mass-Production of Fullerenes and Carbon Nanotubes by the JxB Arc Discharge Method2005

    • Author(s)
      T.Mieno, Md.K.H.Bhuiyan, N.Matsumoto
    • Journal Title

      Proc.4^<th> Int.Conf.Global Research and Education (inter-academia 2005) (Wuppertal, Germany) Vol.1

      Pages: 123-132

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 無重力下での単層炭素ナノチューブ合成2005

    • Author(s)
      三重野 哲
    • Journal Title

      NEW DIAMOND, No.78 Vol.21,3

      Pages: 26-27

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Gravity Effect on the Gas Evaporation Synthesis of Fullerenes2005

    • Author(s)
      S.Usuba, Y.Kakudate, T.Mieno
    • Journal Title

      Proc.6th Japan China Workshop on Microgravity Science (Saga) Vol.1

      Pages: 147-148

    • NAID

      10018498622

    • Related Report
      2005 Annual Research Report
  • [Book] 小特集、無対流アーク放電による炭素クラスター合成(学会誌、Vol.83)2007

    • Author(s)
      三重野 哲
    • Publisher
      プラズマ・核融合学会
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Book] プラズマ・イオンビームとナノテクノロジー(上條榮治監修)、普及版第8章「フラーレン」の分担執筆2007

    • Author(s)
      三重野 哲
    • Total Pages
      7
    • Publisher
      シーエムシー出版
    • Related Report
      2006 Annual Research Report
  • [Book] Novel Materials Processing by Advanced Electromagnetic Energy Sources(Apart(pp.45-48))(Ed. S. Miyake)2005

    • Author(s)
      T.Mieno, T.Mizutani, M.Takeguchi
    • Publisher
      Elsevier BV, Amsterdam
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Book] NEW DIAMOND Vol.21,No.3、(トピックス、「無重力下での単層炭素ナノチューブ合成」)2005

    • Author(s)
      三重野哲, 竹口雅樹
    • Publisher
      オーム社
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Book] Novel Materials Processing by Advanced Electromagnetic Energy Source (Edited by S.Miyake)(分担)2005

    • Author(s)
      T.Mieno, T.Mizutani, M.Takeguchi
    • Publisher
      ELSEVIER, Netherlands
    • Related Report
      2005 Annual Research Report

URL: 

Published: 2005-04-01   Modified: 2016-04-21  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi