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Time Resolved X-ray Diffraction using Parametric X-ray Radiation

Research Project

Project/Area Number 17560046
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Applied physics, general
Research InstitutionNihon University

Principal Investigator

TAKAHASHI Yumiko  Nihon University, College of Science and Technology, Research Associate, 理工学部, 助手 (70339258)

Co-Investigator(Kenkyū-buntansha) HAYAKAWA Yasushi  Nihon University, College of Science and Technology, Associate Professor, 理工学部, 助教授 (40307799)
TAKANO Yoshiki  Nihon University, College of Science and Technology, Professor, 理工学部, 教授 (30171466)
Project Period (FY) 2005 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥3,400,000 (Direct Cost: ¥3,400,000)
Fiscal Year 2006: ¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 2005: ¥1,400,000 (Direct Cost: ¥1,400,000)
KeywordsParametric X-ray radiation / X-ray diffraction / Imaging / Time resolved measurement / Structure of materials / Soft matter / Accelerator
Research Abstract

In the Laboratory for Electron Beam Research and Application (LEBRA) at Nihon University, a parametric X-ray radiation (PXR) generator system was constructed using high-energy electron beams from the 125 MeV electron linear accelerator. For an application to the material science, a new X-ray measurement system using PXR was studied
(1) Construction of PXR beam line
A fundamental X-ray diffraction system was assembled on the PXR beam line. Application facilities for Fluorescence X-ray analysis and imaging were also added to the system.
(2) Stabilization of PXR
Stability of the electron beam, optical elements and control devices were investigated. After the improvement, the fluctuation of electron beam has been controlled under 0.05 %. Since the angular instability of goniometer, which was about 1 arcsec/h is not enough for precision measurement, it was changed to the high spec machine. It was clarified that the effect of environment such as the room temperature is not negligible.
(3) Time resolved measurement
Time resolved measurement became practicable by using the RF signal of accelerator. It is applied to the gate system of CCD as a trigger signal.
(4) Application
The structures of macromolecules and biological materials were measured. The applied study using PXR was achieved for the first time in the world.

Report

(3 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • Research Products

    (17 results)

All 2007 2006 2005 Other

All Journal Article (17 results)

  • [Journal Article] Phase Contrast Imaging of Biological Materials using LEBRA-PXR2007

    • Author(s)
      T.Kuwada
    • Journal Title

      AIP Conference Proceedings 879

      Pages: 1968-1971

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Phase Contrast Imaging of Biological Materials using LEBRA-PXR2007

    • Author(s)
      T.Kuwada, Y.Hayakawa a, K.Nogami, T.Sakai, T.Tanaka, K.Hayakawa, I.Sato
    • Journal Title

      AIP Conference Proceedings 879

      Pages: 1968-1971

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Status of the parametric X-ray generator at LEBRA, Nihon University.2006

    • Author(s)
      Y.Hayakawa
    • Journal Title

      Nucl. Instr. and Meth. B 252

      Pages: 102-110

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Application of LEBRA-PXR to the diffraction analysis of minerals.2006

    • Author(s)
      Toshiro Sakae
    • Journal Title

      Journal of Mineralogical and Petrological Sciences 101

      Pages: 10-13

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Phase-contrast Imaging Using the LEBRA-PXR System at Nihon University2006

    • Author(s)
      Y.Hayakawa
    • Journal Title

      Proceedings of the 3rd Annual Meeting of Particle Accelerator Society of Japan and the 31st Linear Accelerator Meeting in Japan

      Pages: 172-174

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Status of the parametric X-ray generator at LEBRA, Nihon University.2006

    • Author(s)
      Y.Hayakawa a, I.Sato, K.Hayakawa, T.Tanaka, A.Mori, T.Kuwada, T.Sakai, K.Nogami, K.Nakao, T.Sakae
    • Journal Title

      Nucl. Instr. and Meth,. B252

      Pages: 102-110

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Application of LEBRA-PXR to the diffraction analysis of minerals.2006

    • Author(s)
      Toshiro Sakae, Yasushi Hayakawa, Akira Mori, Takao Kuwada, Takeshi Sakai, Kyoko Nogami, Toshinari Tanaka, Ken, Hayakawa, Isamu Sato
    • Journal Title

      Journal of Mineralogical and Petrological Sciences 101

      Pages: 10-13

    • NAID

      10016735578

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Phase-contrast Imaging Using the LEBRA-PXR System at Nihon University2006

    • Author(s)
      Yasushi Hayakawa, Ken Hayakawa, Manabu Inagaki, Takao Kuwada, Akira Mori, Keisuke Nakao, Kyoko Nogami, Toshiro Sakae, Takeshi Sakai, Isamu Sato, Yumiko Takahashi, Toshinari Tanaka
    • Journal Title

      Proceedings of the 3rd Annual Meeting of Particle Accelerator Society of Japan and the 31st Linear Accelerator Meeting in Japan

      Pages: 172-176

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Intralayer molecular orientation in the Bl phase of a proto-type bent-core molecule P-6-O-PIMB studied by X-ray microbeam diffraction.2006

    • Author(s)
      Y.Takanishi
    • Journal Title

      J. Mater. Chem. 16

      Pages: 815-817

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Heavy fermion like behavior in layered Ce-based oxysulfides2006

    • Author(s)
      Y.Takano
    • Journal Title

      Journal of Alloys and Compound 408-412

      Pages: 101-103

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Dynamic Response of Local Layer and Molecular Orientation in Smectic Liquid Crystals by Time Resolved X-ray Micro-Diffraction2005

    • Author(s)
      Yumiko Takahashi
    • Journal Title

      Bussei Kenkyu 84

      Pages: 921-922

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] Dynamic and microscopic X-ray characterization of a compound chevron layer in electroclinic liquid crystals2005

    • Author(s)
      Atsuo Iida
    • Journal Title

      Liquid Crystals 32

      Pages: 717-726

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Dynamic Response of Local Layer and Molecular Orientation in Smectic Liquid Crystals by Time Resolved X-ray Micro-Diffraction2005

    • Author(s)
      Yumiko Takahashi, Atsuo Iida, Yoichi Takanishi, Hideo Takezoe, Kouichi Takase, Yoshiki Takano, Kazuko Sekizawa
    • Journal Title

      Bussei Kenkyu 84

      Pages: 921-922

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Dynamic and microscopic X-ray characterization of a compound chevron layer in electroclinic liquid crystals2005

    • Author(s)
      ATSUO IIDA, YUMIKO TAKAHASHI, YOICHI TAKANISHI, MICHI NAKATA, KEN ISHIKAWA, HIDEO TAKEZOE
    • Journal Title

      Liquid Crystals 31

      Pages: 717-726

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] パラメトリックX線の今後の展望2005

    • Author(s)
      佐藤 勇
    • Journal Title

      第2回日本加速器学会年回・第30回リニアック技術研究会報告

      Pages: 114-114

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Advanced applications of PXR at LEBRA, Nihon University

    • Author(s)
      Y.Hayakawa
    • Journal Title

      Proceedings of the International Conference on Charged and Neutral Particles Channeling Phenomena (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Advanced applications of PXR at LEBRA, Nihon University

    • Author(s)
      Y.Hayakawa, Y.Hayakawa, K.Hayakawa, M.Inagaki, T.Kuwada, A.Mori, K.Nakao, K.Nogami, T.Sakae, T.Sakai, I.Sato, Y.Takahashi, T.Tanaka
    • Journal Title

      Proceedings of the International Conference on Charged and Neutral Particles Channeling Phenomena (in print.)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary

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Published: 2005-04-01   Modified: 2016-04-21  

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