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Study on the mechanism of micro/nanotribological behavior and the lubrication method

Research Project

Project/Area Number 17560128
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Design engineering/Machine functional elements/Tribology
Research InstitutionAichi Institute of Technology

Principal Investigator

TAKAGI Makoto  Aichi Institute of Technology, Department of Mechanical Engineering, Professor, 工学部, 教授 (40288428)

Co-Investigator(Kenkyū-buntansha) MATSUMURO Akihito  Aichi Institute of Technology, Department of Mechanical Engineering, Professor, 工学部, 教授 (80173889)
Project Period (FY) 2005 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥2,700,000 (Direct Cost: ¥2,700,000)
Fiscal Year 2006: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 2005: ¥1,900,000 (Direct Cost: ¥1,900,000)
Keywordsmicro / nanotribology / wear structure / silicon single crystal / atonic force microscope / scanning tunneling microscope / transmission electron microscope / microcrystalline alloy / surface modification / ナノ / マイクロ加工
Research Abstract

(1) Microstructural change of the surface of Si single crystal (Si(100)) after the scratching tests under very small loading forces was investigated. At first, line-scratching tests and scanning-scratching tests were carried out using an atomic force/friction force microscope (AFM/FFM). Next, cross-sectional TEM observations of the wear marks which were generated by the scratching tests were carried out. As a result of the TEM observations after the line-scratching tests, it was found that dislocations were observed in the area of less than 100nm thickness from the surface of the wear marks which were formed under the loading forces of more than 5 μN. In the case of the loading forces of more than 20 μN, an amorphous region was also observed just under the wear marks. As a result of the TEM observations after the scanning-scratching tests, it was found that the introduction of dislocations took place and no amorphous region appeared. It was also found that the several atomic layers at the top surface of the wear marks shifted in parallel to (100).
(2) The fabricating methods of nanoscale shapes on Si(100) surface by using atomic force microscope (AFM) and scanning tunneling microscope (STM) were investigated. As a result, nanoscale grooves and faces were fabricated by the scratching methods using AFM. Nanoscale pits, grooves and faces were fabricated by using STM. Cross-sectional TEM observations of the nanoscale grooves and faces fabricated by AFM and STM were carried out to study the microstructural change of Si single crystals. As a result of the TEM observations, it was found that many dislocations and an amorphous phase appeared in the surface of the grooves and faces fabricated by AFM. On the other hand, the single crystalline structure without a dislocation was preserved in the surface of the grooves and faces fabricated by STM.

Report

(3 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • Research Products

    (11 results)

All 2007 2006 2005

All Journal Article (11 results)

  • [Journal Article] Al/アモルファス半導体系二層膜の結晶化とパターン形成2007

    • Author(s)
      土井稔, 香月太, 熊谷洋志, 高木誠
    • Journal Title

      軽金属 57巻・1号

      Pages: 30-36

    • NAID

      10018494998

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] カーボンナノチューブ探針を用いた高アスペクト比ナノスケール穴加工法の開発-単層カーボンナノチューブ探針の作製と高配向焼結グラファイトの加工-2006

    • Author(s)
      有馬則和, 荻原高志, 金森晃宏, 松室昭仁
    • Journal Title

      精密工学会誌 72-1

      Pages: 116-120

    • NAID

      110002978321

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] TEM Observation of Microstructural Change of Silicon Single Crystal Caused by Scratching Tests Using SPM2005

    • Author(s)
      M.Takagi, K.Onodera, H.Iwata, T.Imura, K.Sasaki, H.Saka
    • Journal Title

      Materials Research Society Sympo. Proc. 841

      Pages: 247-252

    • NAID

      110004812516

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Tensile Properties of an Al-11 mass% Si Alloy at Elevated Temperature Processed by Rotary-Die Equal-Channel Angular Pressing2005

    • Author(s)
      A.-B.Ma, M.Takagi, N.Saito, H.Iwata, Y.Nishida, K.Suzuki, H.Iwata, I.Shigematsu
    • Journal Title

      Materials Science and Engineering A 408

      Pages: 147-153

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] High-Aspect-Ratio Nanofabrication Using Carbon Nanotube Probe in Scanning Tunneling Microscope2005

    • Author(s)
      N.Arima, A.Matsumuro
    • Journal Title

      2005 International Symposium on Micro-Nano Mechatronics and Human Science

      Pages: 189-192

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] Fabrication of High-Aspect-Ratio Nanoscale Pit Using Carbon Nanotube Probe and Effect on Its Microstructure2005

    • Author(s)
      N.Arima, A.Matsumuro
    • Journal Title

      The 4th International Conference on Materials Processing for Properties and Performance

      Pages: 328-331

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] TEM Observation of Microstructural Change of Silicon Single Crystal Caused by Scratching Tests Using SPM2005

    • Author(s)
      M.Takagi, K.Onodera, H.Iwata T.Imura, K.Sasaki, H.Saka
    • Journal Title

      Materials Research Society Sympo.Proc 841

      Pages: 247-252

    • NAID

      110004812516

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of Severe Plastic Deformation on Tensile Properties of a Cast A1-11 mass% Si Alloy2005

    • Author(s)
      A.-B.Ma, N.Saito, M.Takagi, Y.Nishida, H.Iwata, I.Shigematsu, A.Watazu
    • Journal Title

      Materials Science and Engineering A 395

      Pages: 70-76

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Tensile Properties of an A1-11 mass% Si Alloy at Elevated Temperature Processed by Rotary-Die Equal-Channel Angular Pressing2005

    • Author(s)
      A.-B.Ma, M.Takagi, N.Saito, H.Iwata, Y.Nishida, K.Suzuki, H.Iwata, I.Shigematsu
    • Journal Title

      Materials Science and Engineering A408

      Pages: 147-153

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] TEM Observation of Microstructural Change of Silicon Single Crystal Caused by Scratching Tests Using SPM2005

    • Author(s)
      M.Takagi, K.Onodera, H.Iwata, T.Imura, K.Sasaki, H.Saka
    • Journal Title

      Materials Research Society Sympo.Proc. 841

      Pages: 247-252

    • NAID

      110004812516

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Tensile Properties of an Al-11 mass% Si Alloy at Elevated Temperature Processed by Rotary-Die Equal-Channel Angular Pressing2005

    • Author(s)
      A.-B.Ma, M.Takagi, N.Saito, H.Iwata, Y.Nishida, K.Suzuki, H.Iwata, I.Shigematsu
    • Journal Title

      Materials Science and Engineering A408

      Pages: 147-153

    • Related Report
      2005 Annual Research Report

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Published: 2005-04-01   Modified: 2016-04-21  

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