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Continuous preparation of the mono-core coating of particle using the spouted bed with draft tube

Research Project

Project/Area Number 17560663
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Properties in chemical engineering process/Transfer operation/Unit operation
Research InstitutionKagoshima University

Principal Investigator

IJICHI Kazuya  Kagoshima University, Fac. of Eng., Professor (60041555)

Co-Investigator(Kenkyū-buntansha) TSUTSUI Toshio  Kagoshima Univ., Fac. of Eng., Associate Professor (60133097)
Project Period (FY) 2005 – 2007
Project Status Completed (Fiscal Year 2007)
Budget Amount *help
¥3,920,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥120,000)
Fiscal Year 2007: ¥520,000 (Direct Cost: ¥400,000、Indirect Cost: ¥120,000)
Fiscal Year 2006: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 2005: ¥2,900,000 (Direct Cost: ¥2,900,000)
KeywordsFine Particle Coating / Surface Modification / Functional Fine Particle / Spouted Bed / Draft-Tube / Mono-core Coating / Titanium Fine Powder / Handling / 超微粒子 / チタニア
Research Abstract

According as the development of new materials proceeds, the demand of minimization of raw materials and improvement of the surface characteristics of solid particles are raised up. If the mono-core coating of fine particle is achieved, it means that useful fine materials with difficult handling are coated on the seed particle with easy handling. This condition means that the application range extends as functional fine particle, furthermore, it seems to be able to efficiently carry out the addition of the new function in these materials.
In this experiment, the preparation of functional fine particle with the environmental cleanup function was tried by coating substrates such as Shirasu particles and glass beads with good handling ability with titanium fine particles which have environmental cleanup function but have strong cohesive property.
As a result, by installing Teflon tube with the water repellency to the tip of draft tube, continuous coating operation of 300 minutes would be pos … More sible, due to the choking of the tube was suppressed. Then, regardless of degree of polymerization of PVA and type of the seed particle, it was possible to coat the titanium fine particles at the 90% of the seed particle surface. And the preparation particle was excited by the ultraviolet irradiation by fluorescent lamp, and it was confirmed that there was the activity with the photocatalyst in decoloring the methylene blue which passed in the preparation particle bed. By flowing standard gas of methylene through the fixed bed of the preparation particle, photocatalyst performance of the particles were examined. Due to the binder liquid has covered over the titanium, decomposition reaction in short time could not be observed. Then it was found that selection of the appropriate binder liquid was necessary. By the fluidization test of the preparation particle, it was found that the exfoliation rate of the adhesive titanium fine particle was about 30%. The exfoliation rate was comparatively small, then it was proven that the ability as a photocatalyst of the preparation particle seems to have not been lost. Then the removal operation of the environmental pollutant using fluidized bed operation could be expected. Less

Report

(4 results)
  • 2007 Annual Research Report   Final Research Report Summary
  • 2006 Annual Research Report
  • 2005 Annual Research Report
  • Research Products

    (2 results)

All 2006

All Presentation (2 results)

  • [Presentation] ドラフト管付き噴流層によるシラス微粒子へのチタニアコーティング2006

    • Author(s)
      伊地知 和也
    • Organizer
      化学工学会室蘭大会
    • Place of Presentation
      室蘭工業大学
    • Year and Date
      2006-08-24
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Titania coating to shirasu fine particle using the spouted bed with draft tube2006

    • Author(s)
      K. Ijichi, et. al.
    • Organizer
      Kagakukougakkai Muroran taikai
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary

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Published: 2005-04-01   Modified: 2016-04-21  

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