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APPLICATION FOR BIOMATERIALS OF CARBONATE APATITE BY SUPERPLASTIC DERFORMATION

Research Project

Project/Area Number 17592053
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 補綴理工系歯学
Research InstitutionAsahi University

Principal Investigator

ADACHI Masanori  Asahi University, SHCOOL OF DENTISTRY, ASSOCIATE PROFESSOR (60076057)

Co-Investigator(Kenkyū-buntansha) DOI YUTAKA  ASAHI UNIVERSITY, SCHOOL OF DENTISTRY, PROFESSOR (40116067)
WAKAMASTU Nobukazu  ASAHI UNIVERSITY, SCHOOL OF DENTISTRY, ASSITANT (00158594)
KAMEMIZU Hideo  ASAHI UNIVERSITY, SCHOOL OF DENTISTRY, LECTURER (00152877)
IIJIMA MAYUMI  ASAHI UNIVERISTY, SCHOOL OF DENTISTRY, ASSISTANT (80164838)
Project Period (FY) 2005 – 2007
Project Status Completed (Fiscal Year 2007)
Budget Amount *help
¥3,750,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥150,000)
Fiscal Year 2007: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2006: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 2005: ¥2,300,000 (Direct Cost: ¥2,300,000)
KeywordsAPATITE / SUPER PLASTIC DEFORMATION / LIQUID PHASE / X-RAY DIFRACTION / BIOCOMPATIBILITY / SINTERING / STRAIN SPEED / 曲げ変形 / 伸び変形 / 赤外分光分析
Research Abstract

To produce the desired shape of carbonate apatite (CAP) ceramics using superplastic deformation, deformation behavior of CAP ceramics under constant loading as well as physical properties after deformation were evaluated. Sintered CAP ceramics were plastically deformed in an electric furnace attached to a universal hydraulic testing machine under a constant load. CAP ceramics subjected to an initial compressive pressure of 10 Mpa showed appreciable amounts of plastic deformation at temperatures ranging from 720 to 800℃. Plastic deformation increased with increasing temperature from about 10% to 70% after 2 hrs loading. A marked plastic deformation of about 70% at 800℃ would be sufficient for near-net-shape production of bioresorbable CAP bone substitutes with complex shapes. X-ray diffraction analysis and SEM observations revealed that some CAP crystals were elongated and aligned with the c-axis normal to the loading direction during the superplastic deformation.

Report

(4 results)
  • 2007 Annual Research Report   Final Research Report Summary
  • 2006 Annual Research Report
  • 2005 Annual Research Report
  • Research Products

    (18 results)

All 2008 2007 2006 2005

All Journal Article (16 results) (of which Peer Reviewed: 2 results) Presentation (2 results)

  • [Journal Article] Superplastic deformation in carbonate apatite ceramics under constant compressive loading for near-net-shape production of bioresorbable bone substitutes2008

    • Author(s)
      M.Adachi, N.Wakamatu, Y.Doi
    • Journal Title

      Dental Materials Journal Vol27

      Pages: 93-98

    • NAID

      110006570544

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Fabrication of composite of collagen and OCP/apatite-mixed crystal with large aspect ratio2008

    • Author(s)
      M.Iijima, N.Wakamatu, H.Kamemizu, M.Adachi, Y.Doi
    • Journal Title

      Journal of the Ceramic Society of Japan Vol.116

      Pages: 316-319

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Superplastic deformation in carbonate apatite ceramics under constant compressive loading for near-net-shape production of bioresorbable bone substitutes.2008

    • Author(s)
      M. Adachi, N. Wakamatu, Y. Doi
    • Journal Title

      Dental Materials Journal Vol 27(1)

      Pages: 93-98

    • NAID

      110006570544

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Creation of a composite of collagen and OCP crytals with large morphological anisotropy.2008

    • Author(s)
      M. Iijima, N. Wakamastu, H. Kamemizu, M. Adachi, Y. Doi
    • Journal Title

      Journal of the Ceramic Society of Japan Vol 116(2)

      Pages: 316-319

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Superplastic Deformation in Carbonate-Apatite Ceramics under Constant Compressive Loading for Near-net-shape Production of Bioresorbable Bone Substitutes2008

    • Author(s)
      M. Adachi, N. Wkamastu and Y. Doi
    • Journal Title

      Dental Materials Journal 27(1)

      Pages: 93-98

    • NAID

      110006570544

    • Related Report
      2007 Annual Research Report
  • [Journal Article] Quasi-Superplastic Behavior and Physical Property in Sintered Carbonate Apatites2007

    • Author(s)
      Adachi M, Wakamastu N, Kamemizu H, Iijima M, Doi Y
    • Journal Title

      Proceedings of the International Dental Materials Congress 2007

      Pages: 261-261

    • NAID

      130006962752

    • Related Report
      2007 Annual Research Report
  • [Journal Article] 炭酸含有アパタイト焼結体の塑性変形のメカニズム2007

    • Author(s)
      足立正徳、後藤隆泰、若松宣一、亀水秀男、飯島まゆみ、土井豊
    • Journal Title

      歯科材料・器械 26巻2号

      Pages: 194-194

    • NAID

      130006961756

    • Related Report
      2007 Annual Research Report
  • [Journal Article] OCP/apatite結晶とタイプIコラーゲン複合体の組成、構造と曲げ挙動の関係2007

    • Author(s)
      飯島まゆみ、若松宣一、亀水秀男、足立正徳、土井豊
    • Journal Title

      歯科材料・器械 26巻2号

      Pages: 197-197

    • NAID

      130006961753

    • Related Report
      2007 Annual Research Report
  • [Journal Article] 炭酸含有アパタイト焼結体の引張変形特性について2006

    • Author(s)
      足立正徳, 若松宣一, 亀水秀男, 飯島まゆみ, 土井豊
    • Journal Title

      歯科機材・器機 25巻2号

      Pages: 138-138

    • NAID

      130006962937

    • Related Report
      2006 Annual Research Report
  • [Journal Article] 炭酸含有アパタイト焼結体の塑性変形時の歪速度とクラック発生の関係2006

    • Author(s)
      足立正徳, 若松宣一, 亀水秀男, 飯島まゆみ, 土井豊
    • Journal Title

      歯科機材・器機 25巻5号

      Pages: 427-427

    • NAID

      130006963677

    • Related Report
      2006 Annual Research Report
  • [Journal Article] 陽イオン交換膜上で育成したOCP/apataite結晶と再構成タイプIコラーゲンの複合化2006

    • Author(s)
      飯島まゆみ, 竹中祥絋, 若松宣一, 亀水秀男, 足立正徳, 土井豊
    • Journal Title

      歯科機材・器機 25巻5号

      Pages: 429-429

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Preparation of Anisotropic hydroxyapatite/Poly-L-Lactic acid composites using hot-pressing2006

    • Author(s)
      N.Wkamastu, M.Iijimma, H.Kamemizu, M.Adachi, Y.Doi
    • Journal Title

      岐阜歯科学会雑誌 32巻2-3号

      Pages: 27-32

    • NAID

      110006155033

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Mechanical properties of superplastic deformed carbonate apatite.2005

    • Author(s)
      M. Adachi, N. Wakamatu, H. Kamemizu, M. Iijima, Y. Doi.
    • Journal Title

      Arch. BioCeram. Res. Vol.5

      Pages: 222-225

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Mechanical properties of superplastic deformed carbonate apatite2005

    • Author(s)
      M.Adachi, N.Wkamastu, H.Kamemizu, M.Iijima, Y.Doi
    • Journal Title

      Archives of BioCeramics Research Volume 5

      Pages: 222-225

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Ductile/brittle transition conditions in grinding of dental porcelain2005

    • Author(s)
      N.Wkamastu, M.Iijimma, H.Kamemizu, M.Adachi, Y.Doi
    • Journal Title

      Archives of BioCeramics Research Volume 5

      Pages: 252-256

    • NAID

      120005867823

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Synthesis of OCP crystal with large aspect ratio in polyacrylamide gels2005

    • Author(s)
      M.Iijimma, N.Wkamastu, H.Kamemizu, M.Adachi, Y.Doi
    • Journal Title

      Archives of BioCeramics Research Volume 5

      Pages: 186-189

    • Related Report
      2005 Annual Research Report
  • [Presentation] Quasi-superplastic Behavior and Physical Property in Sintered Carbonate Apatites2007

    • Author(s)
      Adachi M, Wakamastu N, Kamemizu H, Iijima M and Doi Y
    • Organizer
      The Japanese Society for Dental Materials and Devices
    • Place of Presentation
      Thailand
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Presentation] Quasi-superplastic Behavior and Physical Property in Sintered Carbonate Apat ites.2007

    • Author(s)
      Adachi M, Wakamastu N, Kamemizu H, Iijima M, Doi Y
    • Organizer
      The Japanese Society for Dental Materials and Devices
    • Place of Presentation
      Thailand
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary

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Published: 2005-04-01   Modified: 2016-04-21  

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