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3D/4D mesoscopic materials science led by ultra-high resolution X-ray microscopy

Research Project

Project/Area Number 17H01328
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionKyushu University

Principal Investigator

Toda Hiroyuki  九州大学, 工学研究院, 教授 (70293751)

Co-Investigator(Kenkyū-buntansha) 小林 正和  豊橋技術科学大学, 工学(系)研究科(研究院), 准教授 (20378243)
Project Period (FY) 2017-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥43,290,000 (Direct Cost: ¥33,300,000、Indirect Cost: ¥9,990,000)
Fiscal Year 2020: ¥9,100,000 (Direct Cost: ¥7,000,000、Indirect Cost: ¥2,100,000)
Fiscal Year 2019: ¥9,100,000 (Direct Cost: ¥7,000,000、Indirect Cost: ¥2,100,000)
Fiscal Year 2018: ¥16,120,000 (Direct Cost: ¥12,400,000、Indirect Cost: ¥3,720,000)
Fiscal Year 2017: ¥8,970,000 (Direct Cost: ¥6,900,000、Indirect Cost: ¥2,070,000)
Keywordsシンクロトロン / トモグラフィー / X線顕微鏡 / 高エネルギー / 構造用金属材料 / 転位 / 原子空孔 / 3D/4D / 強度・破壊靭性 / 可視・評価技術 / 3Dイメージング / 3DのX線回析 / 高分解能 / 強度・破壊靱性
Outline of Final Research Achievements

Imaging experiments have been performed at first for aluminum using the X-ray energy of 20 keV and subsequently for steels et al. using 30 keV or more, which was realized by combining a large-scale X-ray microscope and a phase contrast technique. The projection CT, by which the whole sample is visualized and the X-ray microscope were combined with an adjoining XRD setup with a collimated X-ray beam, thereby the evaluation of the-whole-sample and full-time observation of the weakest point is realized in spite of the high-resolution observation. In addition, the coarsening techniques, which analyzes a huge number of microstructural features in a 3D image, was studied. Dislocations and vacancies, and polycrystalline structures were measured in 3D in high density by employing our original 3D plastic strain mapping and diffraction-amalgamated grain boundary tracking technique, respectively. This enables us to conduct the real multi-scale imaging ranging between nanoscale and macroscale.

Academic Significance and Societal Importance of the Research Achievements

アルミニウム、チタン、鉄鋼等の構造材料内部にある複雑なミクロ構造とマクロ挙動とを結びつける研究手段が確立した。1本の試験片の1回の力学試験とその「その場観察」を実施することで、結晶学的情報、転位、原子空孔の3D分布やそれらの粗密をマクロな力学挙動と対応付けできる。このため、金属の各種力学挙動の理解と深い解析が解釈などを必要としない高い確度で実施できる。今後のマルチモーダル・マルチスケール3D/4Dアプローチの発展を促すと期待できる。一方、アルミニウムの水素脆化、チタンの亀裂伝播速度ばらつき、鉄鋼の歪み誘起相変態等の応用研究が平行して行われ、いずれも産業的に大きな成果を挙げつつある。

Report

(5 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Annual Research Report
  • 2018 Annual Research Report
  • 2017 Annual Research Report
  • Research Products

    (47 results)

All 2021 2020 2019 2018 2017

All Journal Article (11 results) (of which Peer Reviewed: 11 results,  Open Access: 7 results) Presentation (36 results) (of which Int'l Joint Research: 6 results,  Invited: 4 results)

  • [Journal Article] Tomography for Bridging Nano and Macro: Semi-spontaneous Iinterfacial Debonding2021

    • Author(s)
      戸田裕之, 山口正剛, 都留智仁, 清水一行, 松田健二, 平山恭介
    • Journal Title

      Materia Japan

      Volume: 60 Issue: 1 Pages: 13-18

    • DOI

      10.2320/materia.60.13

    • NAID

      130007964852

    • ISSN
      1340-2625, 1884-5843
    • Year and Date
      2021-01-01
    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High-energy x-ray nanotomography introducing an apodization Fresnel zone plate objective lens2021

    • Author(s)
      A. Takeuchi, K. Uesugi, M. Uesugi, H. Toda, K. Hirayama, K. Shimizu, K. Matsuo and T. Nakamura
    • Journal Title

      Review of Scientific Instruments

      Volume: 92 Issue: 2 Pages: 023701-023701

    • DOI

      10.1063/5.0020293

    • NAID

      120007187739

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] X線トモグラフィーの最近の進歩と動向2020

    • Author(s)
      戸田裕之,平山恭介
    • Journal Title

      ふぇらむ

      Volume: 25 Pages: 666-674

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Influence of nanovoids in the hydrogen embrittlement fracture of Al-Zn-Mg-Cu alloys2020

    • Author(s)
      K. Shimizu, H. Toda, C. Kadogawa, H. Fujihara and A. Takeuchi
    • Journal Title

      Materialia

      Volume: 11 Pages: 100667-100667

    • DOI

      10.1016/j.mtla.2020.100667

    • NAID

      120006863159

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] アルミニウムの自発的な界面剥離現象の謎に迫る-より高強度の金属材料開発に向けて2020

    • Author(s)
      戸田裕之,都留智仁,山口正剛,松田健二,清水一行,平山恭介
    • Journal Title

      化学

      Volume: 75 Pages: 48-53

    • NAID

      40022365099

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 3D imaging of polycrystalline structure using diffraction contrast tomography2019

    • Author(s)
      Hirayama Kyosuke
    • Journal Title

      Journal of Japan Institute of Light Metals

      Volume: 69 Issue: 12 Pages: 587-590

    • DOI

      10.2464/jilm.69.587

    • NAID

      130007821800

    • ISSN
      0451-5994, 1880-8018
    • Year and Date
      2019-12-30
    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Hydrogen desorption behavior in Al–8%Zn–1%Mg alloy2019

    • Author(s)
      Fujihara Hiro、Toda Hiroyuki、Shimizu Kazuyuki、Takeuchi Akihisa、Uesugi Kentaro
    • Journal Title

      Journal of Japan Institute of Light Metals

      Volume: 69 Issue: 3 Pages: 186-193

    • DOI

      10.2464/jilm.69.186

    • NAID

      130007639766

    • ISSN
      0451-5994, 1880-8018
    • Year and Date
      2019-03-25
    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Hydrogen partitioning behavior and related hydrogen embrittlement in Al-Zn-Mg alloys2019

    • Author(s)
      Shimizu Kazuyuki、Toda Hiroyuki、Fujihara Hiro、Hirayama Kyosuke、Uesugi Kentaro、Takeuchi Akihisa
    • Journal Title

      Engineering Fracture Mechanics

      Volume: 216 Pages: 106503-106503

    • DOI

      10.1016/j.engfracmech.2019.106503

    • NAID

      120007124555

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Assessment of hydrogen embrittlement via image-based techniques in Al-Zn-Mg-Cu aluminum alloys2019

    • Author(s)
      Su Hang、Toda Hiroyuki、Shimizu Kazuyuki、Uesugi Kentaro、Takeuchi Akihisa、Watanabe Yoshio
    • Journal Title

      Acta Materialia

      Volume: 176 Pages: 96-108

    • DOI

      10.1016/j.actamat.2019.06.056

    • NAID

      120007143940

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Optimization of Mechanical Properties in Aluminum Alloys <i>via</i> Hydrogen Partitioning Control2019

    • Author(s)
      戸田 裕之、山口 正剛、松田 健二、清水 一行、平山 恭介、蘇 航、藤原 比呂、海老原 健、板倉 充洋、都留 智仁、西村 克彦、布村 紀男、李 昇原、土屋 大樹、竹内 晃久、上杉 健太朗
    • Journal Title

      Tetsu-to-Hagane

      Volume: 105 Issue: 2 Pages: 240-253

    • DOI

      10.2355/tetsutohagane.TETSU-2018-083

    • NAID

      130007585427

    • ISSN
      0021-1575, 1883-2954
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Influence of hydrogen on strain localization and fracture behavior in AlZnMgCu aluminum alloys2018

    • Author(s)
      Hang Su, Hiroyuki Toda, Ryohei Masunaga, Kazuyuki Shimizu, Hongye Gao, Katsuro Sasaki, Md Shahnewaz Bhuiyan, Kentaro Uesugi, Akihisa Takeuchi, Yoshio Watanabe
    • Journal Title

      Acta Materialia

      Volume: 159 Pages: 332-343

    • DOI

      10.1016/j.actamat.2018.08.024

    • NAID

      120006894974

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] Application of High-Resolution X-ray Tomography to Hydrogen Embrittlement in Aluminium2020

    • Author(s)
      Hiroyuki Toda
    • Organizer
      The 17th International Conference on Aluminium Alloys (ICAA17)
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] へテロ構造制御によるアルミニウム合金の力学特性向上の試み2020

    • Author(s)
      戸田裕之,山口正剛,都留智仁,清水一行,藤原比呂,平山恭介,松田健二
    • Organizer
      軽金属学会第139回秋期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] DCT法によるAl-Zn-Mg合金の水素脆化挙動の4D結晶解析2020

    • Author(s)
      平山恭介,鈴木尚史,清水一行,戸田裕之,上椙真之,竹内晃久
    • Organizer
      軽金属学会第139回秋期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 結晶塑性有限要素法と水素拡散解析を組み合わせたAl-ZnMg合金の局所水素分配挙動評価2020

    • Author(s)
      藤原比呂,戸田裕之,海老原健一,小林正和,竹内晃久,上椙真之
    • Organizer
      軽金属学会第139回秋期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Al-Zn-Mg合金の分散粒子による水素脆化抑制効果2020

    • Author(s)
      小川諒太,戸田裕之,清水一行,竹内晃久,上椙真之
    • Organizer
      軽金属学会第139回秋期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] X線CTと細束XRDからなる相補的トモグラフィー法とその応用2020

    • Author(s)
      平山恭介,岡村海,鈴木尚史,セクイーイン,清水一行,戸田裕之,上椙真之,竹内晃久
    • Organizer
      軽金属学会第139回秋期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Al-Zn-Mg-X合金の水素分配および水素脆化挙動2020

    • Author(s)
      清水一行,戸田裕之,小川諒太,山口正剛,竹内晃久
    • Organizer
      軽金属学会第138回春期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Al-Zn-Mg-Cu合金の水素脆化抑制における金属間化合物粒子の役割2020

    • Author(s)
      藤原比呂,戸田裕之,清水一行,池見優志,竹内晃久,上杉健太朗
    • Organizer
      軽金属学会第138回春期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Al-Zn-Mg合金の動的水素分配と水素脆化2020

    • Author(s)
      戸田裕之,清水一行,藤原比呂,日高純真,上杉健太朗,竹内晃久
    • Organizer
      軽金属学会第138回春期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Al-10Mg合金における応力腐食割れ挙動の3D/4D解析2020

    • Author(s)
      付東升,戸田裕之,平山恭介,竹内晃久,上杉健太朗,蘇航
    • Organizer
      軽金属学会第138回春期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Investigation of 3D short fatigue crack closure behavior in Ti-6Al-4V alloy using high energy imaging CT2020

    • Author(s)
      V. Tubei, H. Toda, K. Hirayama, A. Takeuchi, M. Uesugi
    • Organizer
      軽金属学会第138回春期大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 超高分解能X線CTと細束XRDからなる相補的トモグラフィー法とその加工誘起変態挙動への応用2020

    • Author(s)
      平山恭介,戸田裕之,竹田健吾,林邦夫,上椙真之,竹内晃久
    • Organizer
      日本鉄鋼協会第179回春季講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 4D characterization of the stress corrosion cracking behavior in Al-10Mg aluminium alloy via synchrotron X-ray tomography2019

    • Author(s)
      Fu, D., Toda, H., Su, H., Hirayama, K., Uesugi, K., Takeuchi, A.
    • Organizer
      The International Offshore and Polar Engineering Conference
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 3D/4Dイメージングによるフェライト/オーステナイト鋼の加工誘起変態・損傷挙動の直接可視化2019

    • Author(s)
      平山 恭介,泉田 恭輔,戸田 裕之,竹田 健吾,林 邦夫,上杉 健太朗,竹内 明久
    • Organizer
      日本機械学会 M&M2019材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 極細束X線回折によるフェライト/オーステナイト鋼の加工誘起変態挙動の評価2019

    • Author(s)
      鈴木 尚史, 平山 恭介,戸田 裕之,竹田 健悟 , 林 邦夫,上杉 健太朗,竹内 晃久
    • Organizer
      日本機械学会 M&M2019材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 高Zn Al-Zn-Mg-Cu合金における水素分配挙動と擬へき開破壊2019

    • Author(s)
      清水一行,戸田裕之,蘇航,竹内晃久
    • Organizer
      日本鉄鋼協会第177回春季講演大会
    • Related Report
      2019 Annual Research Report 2018 Annual Research Report
  • [Presentation] Assessment of 3D short crack closure in Ti-6Al-4V alloy utilizing synchorotron X-ray microtomography2019

    • Author(s)
      V. Tubei, M. Hassanipour, S. Watanabe, K. Hirayama, H. Toda, A. Takeuchi, K. Uesugi
    • Organizer
      金属学会・鉄鋼協会・軽金属学会九州支部合同学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Al-Zn-Mg合金の水素分配挙動と擬へき開破壊2019

    • Author(s)
      日高純真, 戸田裕之, 清水一行, 藤原比呂, 上杉健太朗, 竹内晃久
    • Organizer
      軽金属学会第137回秋期大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Al-Zn-Mg-Cu合金における水素誘起ナノボイドの発生・成長挙動2019

    • Author(s)
      清水一行, 戸田裕之, 平山恭介, 藤原比呂, 門川千宙, 上杉健太朗, 竹内晃久
    • Organizer
      軽金属学会第137回秋期大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Recent Progress in High Resolution X-ray Tomography at High X-ray Energies2019

    • Author(s)
      Hiroyuki TODA
    • Organizer
      The 10th Pacific Rim International Conference on Advance Materials and Processing (PRICM-10)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 3D/4D Hydrogen Embrittlrment Behaviour in Al-10Zn-2.4Mg alloys2019

    • Author(s)
      Hiroyuki TODA
    • Organizer
      The 9th international light metals technology conference
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Al-10Mg合金における応力腐食割れの3D/4D解析2019

    • Author(s)
      戸田裕之,平山恭介,蘇航,付東升,上杉健太朗,竹内晃久
    • Organizer
      軽金属学会第136回春期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 4D characterization of stress corrosion cracking behavior in Al-10Mg aluminum alloy2019

    • Author(s)
      付東升,戸田裕之,平山恭介,蘇航,上杉健太朗,竹内 晃久
    • Organizer
      日本金属学会第164回春期講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 水素分配制御によるアルミニウム合金の力学特性最適化2018

    • Author(s)
      戸田裕之、清水一行、平山恭介、山口正剛、海老原健一、板倉充洋、都留智仁、松田健二、西村克彦、布村紀男、李昇原、土屋大樹
    • Organizer
      JST産学共創基礎基盤研究プログラム「ヘテロ構造制御」公開シンポジウム
    • Related Report
      2018 Annual Research Report
  • [Presentation] Assessment of hydrogen embrittlement via in-situ imaging techniques in high Zn Al-Zn-Mg alloys2018

    • Author(s)
      Hiroyuki TODA, Hang Su, Kazuyuki Shimizu, Hiro Fujihara, Kyosuke Hirayama, Akihisa Takeuchi, Kentaro Uesugi
    • Organizer
      ECF22
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Hydrogen-Induced Strain Loclization and Nano-Voids in an Al-Zn-Mg Alloy2018

    • Author(s)
      K. Shimizu, H. Toda, H. Gao, K. Uesugi, A. Takeuchi
    • Organizer
      ICAA16
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 放射光ナノトモグラフィによるAl-Zn-Mg合金中の3D亀裂進展挙動解析2018

    • Author(s)
      戸田裕之, 清水一行, Su Hang, 竹内晃久, 上杉健太朗
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
    • Related Report
      2018 Annual Research Report
  • [Presentation] Assessment of 3DShortCrack Closure in Ti-6Al-4V Alloy Utilizing Synchrotron X-ray Microtomography2018

    • Author(s)
      Tubei Valary, Hassanipour Meysam, Watanabe Shinta, Hirayama kyosuke, Toda Hiroyuki, Takeuchi Akihisa, Uesugi Kentaro
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
    • Related Report
      2018 Annual Research Report
  • [Presentation] 水素分配制御に基づくAl-Zn-Mg合金の力学特性最適化2018

    • Author(s)
      蘇航,戸田裕之,清水一行,上杉健太朗,竹内晃久
    • Organizer
      日本機械学会九州支部第71期総会・講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 水素分配制御に基づくAl-Zn-Mg合金の力学特性向上2018

    • Author(s)
      清水一行,戸田裕之,高紅叶,蘇航,平山恭介,上杉健太朗,竹内晃久
    • Organizer
      日本機械学会九州支部第71期総会・講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] イメージベース解析による高Zn Al-Zn-Mg-Cu合金における水素分配挙動の評価2018

    • Author(s)
      蘇航,清水一行,戸田裕之,上杉健太朗,竹内晃久
    • Organizer
      日本鉄鋼協会第175回春季講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] X線顕微鏡による未変態オーステナイトの3D/4D加工誘起変態挙動の評価2018

    • Author(s)
      平山恭介,岡村海,泉田恭輔,戸田裕之,竹田健悟,林邦夫,竹内晃久,上杉健太朗
    • Organizer
      日本鉄鋼協会第175回春季講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] X線顕微鏡による未変態オーステナイトの3D/4D加工誘起変態挙動の評価2018

    • Author(s)
      岡村海,泉田恭輔,戸田裕之,竹田健悟,林邦夫,竹内晃久,上杉健太朗
    • Organizer
      日本機械学会九州支部九州学生会第49回学生員卒業研究発表講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 結像型位相コントラストトモグラフィー法を用いたアルミニウム合金中のナノボイド観察2017

    • Author(s)
      門川千宙,戸田裕之,清水一行,上杉健太朗,竹内晃久
    • Organizer
      軽金属学会第133回秋季講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Al-Zn-Mg-Cu合金の水素誘起ナノボイド2017

    • Author(s)
      高紅叶,門川千宙,清水一行,蘇航,戸田裕之
    • Organizer
      日本鉄鋼協会第174回秋期講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Influence of intermetallic particles on the hydrogen partitioning and embrittlement in Al-Zn-Mg-Cu aluminum alloys2017

    • Author(s)
      蘇航,戸田裕之,上杉健太朗,竹内晃久,坂口信人,渡辺良夫
    • Organizer
      日本金属学会第161回秋期講演大会
    • Related Report
      2017 Annual Research Report

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Published: 2017-04-28   Modified: 2022-01-27  

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