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A challenge for ultra-high strength Mg alloys without any addition of rare earths

Research Project

Project/Area Number 17H03413
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionToyohashi University of Technology

Principal Investigator

Miura Hiromi  豊橋技術科学大学, 工学(系)研究科(研究院), 教授 (30219589)

Co-Investigator(Kenkyū-buntansha) 小林 正和  豊橋技術科学大学, 工学(系)研究科(研究院), 准教授 (20378243)
Project Period (FY) 2017-04-01 – 2020-03-31
Project Status Completed (Fiscal Year 2019)
Budget Amount *help
¥18,460,000 (Direct Cost: ¥14,200,000、Indirect Cost: ¥4,260,000)
Fiscal Year 2019: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Fiscal Year 2018: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2017: ¥13,130,000 (Direct Cost: ¥10,100,000、Indirect Cost: ¥3,030,000)
Keywordsマグネシウム合金 / 多軸鍛造 / 超微細粒 / 高強度 / 非希土類元素 / 組織制御
Outline of Final Research Achievements

Combined processes of multi-directional forgings under decreasing temperature conditions (dMDF) followed by MDFing at room temperature (rMDF) were applied to AZ91Mg and AZX61Mg alloys to attain ultrafine-grained structure and ultra-high strength. The gran size of the samples prepared by dMDF in advance was gradually decreased with increasing cumulative strain of rMDF and the tensile strength was increased. The ultimate tensile strengths achieved were 580 MPa and 520 MPa for AZ91Mg and AZX61Mg alloys, respectively. Therefore, 700 MPa was not attained. This was due to the b phase precipitation during dMDF and their suppression of mechanical twinning which cause grain refinement. It is concluded, therefore, dMDF before rMDF induces a negative influence on strengthening. Ultrafine-grained AZ80Mg was warm extruded by a mechanism of superplastic deformation to form a round tube and it possessed quite high strength of 414 MPa.

Academic Significance and Societal Importance of the Research Achievements

希土類の添加を必要としない超高強度マグネシウム合金の開発は、我が国の材料戦略上極めて重要であり、特に超々ジュラルミン代替材として構造部材に適用できれば、我が国の新技術・新産業分野開拓に及ぼすインパクトは極めて大きい。 世界的に研究ブームとなっている巨大ひずみ加工を難加工材であるマグネシウム合金に適用し、これまでの2倍近い強度を達成する技術開発と材料組織設計は、学術的にも極めて波及効果が大きい。

Report

(4 results)
  • 2019 Annual Research Report   Final Research Report ( PDF )
  • 2018 Annual Research Report
  • 2017 Annual Research Report
  • Research Products

    (46 results)

All 2020 2019 2018 2017 Other

All Journal Article (7 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 7 results,  Open Access: 4 results) Presentation (36 results) (of which Int'l Joint Research: 10 results,  Invited: 5 results) Remarks (1 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] 温間多軸鍛造 AZ80-Fマグネシウム合金の組織と機械的性質2020

    • Author(s)
      小林正和, 余田悠輔, 青葉知弥, 三浦博己
    • Journal Title

      日本金属学会誌

      Volume: 84 Pages: 190-199

    • NAID

      130007846049

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Tensile fracture behavior in wrought magnesium alloy fabricated by multi-directional forging technique2019

    • Author(s)
      A.Takahashi, H.Miura, M.Kobayashi
    • Journal Title

      International Journal of Innovations in Engineering and Technology (IJIET)

      Volume: 13 Pages: 117-123

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Superplasticity in a multi-directionally forged Mg-Li-Zn alloy2019

    • Author(s)
      A.Mehrabi, R.Mahmudi, H.Miura
    • Journal Title

      Materials Science and Engineering A

      Volume: 765 Pages: 138274-138274

    • DOI

      10.1016/j.msea.2019.138274

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructure and mechanical properties of plates warm extruded AZ80Mg alloy fabricated by MDF in advance2018

    • Author(s)
      H. Miura , K. Minami, T. Aoba, M. Kobayashi
    • Journal Title

      Procedia Manufacturing

      Volume: 15 Pages: 1533-1540

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Development of internal inhomogeneous plastic strain during cold rolling of Al-Mg alloys2018

    • Author(s)
      M. Kobayashi, T. Aoba, H. Miura
    • Journal Title

      Procedia Manufacturing

      Volume: 15 Pages: 161-167

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Impact rupture behavior of AZ80 magnesium alloys fabricated by multi-directional forging under decreasing temperature conditions2017

    • Author(s)
      Tani Hirotaka、Aoba Tomoya、Kobayashi Masakazu、Takahashi Akihiro、Miura Hiromi
    • Journal Title

      Journal of Japan Institute of Light Metals

      Volume: 67 Issue: 8 Pages: 355-360

    • DOI

      10.2464/jilm.67.355

    • NAID

      130006107933

    • ISSN
      0451-5994, 1880-8018
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Strain-Rate and Temperature Dependences of Deformation Behavior of AZ61Mg Alloy Processed by Multi-directional Forging Under Decreasing Temperature Conditions2017

    • Author(s)
      Watanabe C.、Monzen R.、Ueji R.、Miura H.
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 48 Issue: 11 Pages: 5368-5375

    • DOI

      10.1007/s11661-017-4303-7

    • NAID

      120006370945

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] Multi-directional Forging of AZ80Mg Alloy Under Decreasing Temperature Conditions for Ultrafine-structure Evolution and High-strength Tube Forming2020

    • Author(s)
      H. Miura, M. Kobayashi
    • Organizer
      International Conference on Plasticity, Damage, and Fracture 2020
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] DRFマグネシウム合金の疲労特性に関する基礎的研究2019

    • Author(s)
      荻堂盛彬,政木清孝,三浦博己,小林正和
    • Organizer
      日本機械学会M&M2019
    • Related Report
      2019 Annual Research Report
  • [Presentation] “ヘテロナノ”超高強度合金材の開発とその特性, 国内発表・長野テクノ財団諏訪2019

    • Author(s)
      三浦博己
    • Organizer
      長野テクノ財団諏訪講演会
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] 真空蒸留・押出加工法による超高純度マグネシウム板材の作製2019

    • Author(s)
      井上 誠,水原 啓斗,会田 哲夫,松澤 和夫,青柳 成俊,三浦 博己
    • Organizer
      資源・素材学会 資源・素材2019
    • Related Report
      2019 Annual Research Report
  • [Presentation] Mg-Al-Ca-Sr-Mn系合金の真空蒸留・押出加工法による高純度マグネシウム板材の作製2019

    • Author(s)
      毛利拓哉,井上誠, 青柳成俊,三浦博己, 会田哲夫
    • Organizer
      資源・素材学会 関西支部 第15回「若手研究者・学生のための研究発表会」
    • Related Report
      2019 Annual Research Report
  • [Presentation] 微細Al31Fマグネシウム合金の静的再結晶における微視組織および機械的性質の変化2019

    • Author(s)
      池田光志,樫原恵蔵,青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会第第135回秋期大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Fabrication of Ultrafine-grained and High-strength Mg Alloy Tube by MDF and Warm Extrusion2019

    • Author(s)
      H. Miura, K. Minami, T. Aoba, and M. Kobayashi
    • Organizer
      BIT's 5th Annual World Congress of Smart Materials-2019
    • Related Report
      2019 Annual Research Report 2018 Annual Research Report
    • Invited
  • [Presentation] Mechanical Properties of Mg Alloys with Hetero-Nano or Homogeneous Ultrafine-Microstructures Developed by Multi-Directional Forging2019

    • Author(s)
      H. Miura
    • Organizer
      Lectures, Politecnico di Milano
    • Related Report
      2018 Annual Research Report
  • [Presentation] Mechanical Properties of Mg Alloys with Hetero-Nano or Homogeneous Ultrafine-Microstructures Developed by Multi-Directional Forging2018

    • Author(s)
      H. Miura and M. Kobayashi
    • Organizer
      International Symposium on Innovative Engineering 2018(ISIE 2018)
    • Related Report
      2018 Annual Research Report 2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Microstractural Evolution and Change in Mechanical Properties of Multi-Directionally Forged Al Alloy2018

    • Author(s)
      T. Aoba, M. Kobayashi
    • Organizer
      The 16th edition of conference series rotating worldwide provides the leading international forum (ICAA16)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Microstructure and mechanical properties of AZ80Mg plates fabricated by combined multi-directional forging and warm extrusion2018

    • Author(s)
      H. Miura, K. Minami, T. Aoba, M. Kobayashi and J. J. Jonas
    • Organizer
      The 4th International Workshop on Fundamental Research for Science and Technology 2018 (GEMS2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Tensile Properties and Microstructure Evolution by MDFed AZ31 Magnesium Alloy2018

    • Author(s)
      4.M.Ohara, A.Takahashi, N.Yamamoto, M.Fukuda, H.Miura and M.Kobayashi
    • Organizer
      The 4th International Workshop on Fundamental Research for Science and Technology 2018 (GEMS2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Warm extrusion of ultrafine-grained Mg alloys fabricated by MDF2018

    • Author(s)
      H. Miura
    • Organizer
      Materials Science and Engineering (MSE 2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Multi-directional forging and warm extrusion of AZ80 Mg alloy2018

    • Author(s)
      H. Miura , K. Minami, T. Aoba, M. Kobayashi
    • Organizer
      The 5th International Conference on New Forming Technology (ICNFT 2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Recycling of high purity magnesium sheet from Mg-Al-Ca system alloy by vacuum distillation and extrusion2018

    • Author(s)
      M. Inoue, T. Mouri,, N. Aoyagi, T. Aida and H. Miura
    • Organizer
      7th International GIGAKU Conference in Nagaoka (IGCN 2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 放射光X線CTによるAl-Mg合金の冷間圧延に おける内部局所塑性ひずみ分布評価2018

    • Author(s)
      小林正和,青葉知弥,三浦博己
    • Organizer
      日本鉄鋼協会2018年第175回春季講演大会シンポジウム
    • Related Report
      2018 Annual Research Report
  • [Presentation] 多軸鍛造加工を施したAl-Mg-Sc系合金の変形挙動のひずみ速度・温度依存性2018

    • Author(s)
      澤秀太郎, 渡辺千尋, 門前亮一, 青葉知弥, 三浦博己
    • Organizer
      軽金属学会第第134回春期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 多軸鍛造Al-Mg合金の組織と機械的性質2018

    • Author(s)
      青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会第第134回春期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Al-5%Mg-2%Si鋳造合金のミクロ組織と力学特性2018

    • Author(s)
      谷口皓平,古田将吾,小林正和,青葉知弥,三浦博己
    • Organizer
      日本鋳造工学会第171回全国講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 微細Al31Fマグネシウム合金の静的再結晶における微視組織および機械的性質の変化2018

    • Author(s)
      池田光志,樫原恵蔵,青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会第第135回秋期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] SrおよびP添加により共晶Si粒子を変化させたAl-7%Si鋳造合金の力学特性調査2018

    • Author(s)
      小林正和,谷口皓平,古田将吾,青葉知弥,三浦博己
    • Organizer
      軽金属学会第第135回秋期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Mg-Al-Ca-Sr-Mn系合金の真空蒸留・押出加工法による高純度マグネシウム板材の作製2018

    • Author(s)
      毛利拓哉,井上誠, 青柳成俊,三浦博己, 会田哲夫
    • Organizer
      資源・素材学会 関西支部 第15回「若手研究者・学生のための研究発表会」
    • Related Report
      2018 Annual Research Report
  • [Presentation] DRF加工されたマグネシウム合金の疲労特性評価2018

    • Author(s)
      荻堂盛彬,政木清孝,三浦博己,小林正和
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
    • Related Report
      2018 Annual Research Report
  • [Presentation] 放射光X線CTによるAl-Mg合金の冷間圧延における内部局所塑性ひずみ分布評価2018

    • Author(s)
      小林正和,青葉知弥,三浦博己
    • Organizer
      日本鉄鋼協会2018年第175回春季講演大会シンポ ジウム 茨城県中性子利用促進研究会平成29年度集合組織分科会「材料強度特 性のミクロ組織メカニクス―X線・中性子の新しい視点―」
    • Related Report
      2017 Annual Research Report
  • [Presentation] Internal Local strain distribution during cold rolling in Al-Mg alloys2017

    • Author(s)
      M. Kobayashi, M. Nakayama, T. Aoba and H. Miura
    • Organizer
      The International Workshop on Fundamental Research for Science and Technology 2017 (GEMS2017)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Investigation of inhomogeneous deformation and microstructure during cold rolling in Al-Mg alloys by using 3D marker tracking method2017

    • Author(s)
      M.Kobayashi, M.Nakayama, T.Aoba and H.Miura
    • Organizer
      Proceedings of the 18th International Conference on Textures of Materials (ICOTOM-18)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Al-10%Si鋳造合金の熱処理におけるSi粒子形態変化と力学特性2017

    • Author(s)
      青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会第第132回春期大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Al-Mg合金の冷間圧延における局所ひずみ分布に対するMg量の影響2017

    • Author(s)
      中山将徳,小林正和,青葉知弥,三浦博己
    • Organizer
      軽金属学会第第132回春期大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 冷間多軸鍛造を施したAl-Zn-Mg 系合金の強度と環境疲労特性2017

    • Author(s)
      小林正和,上野宗太郎,青葉知弥,三浦博己
    • Organizer
      日本金属学会2017年第161回秋期講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 超微細粒Al-Mg-Sc 合金の変形挙動のひずみ速度・温度依存性2017

    • Author(s)
      渡辺千尋,門前亮一,青葉知弥,三浦博己
    • Organizer
      日本金属学会2017年第161回秋期講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Mg量の異なるAl-Mg合金の冷間圧延における内部局所塑性ひずみ分布2017

    • Author(s)
      小林正和,青葉知弥,三浦博己
    • Organizer
      軽金属学会主催第2回「アルミニウムの再結晶集合組織形成モデル化研究部会」公開講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 多軸鍛造を施したAl-Mg-Zn合金の機械的性質2017

    • Author(s)
      青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会第第133回秋期大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 降温多軸鍛造AZ61Mg合金の衝撃破壊挙動に関する研究2017

    • Author(s)
      齊藤哲郎,青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会東海支部 特別講演会およびポスター講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 降温多軸鍛造で作製した超微細粒AZ80Mg合金の押出成形に関する研究2017

    • Author(s)
      南佳一郎,青葉知弥,小林正和,三浦博己
    • Organizer
      軽金属学会東海支部 特別講演会およびポスター講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] AM60マグネシウム合金の真空蒸留・塑性加工法による高純度マグネシウム板材の作製2017

    • Author(s)
      佐伯蘭,井上誠,三浦博己
    • Organizer
      日本金属学会・日本鉄鋼協会北陸信越支部平成29年度総会・連合講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Mg-Al-Ca系合金の真空蒸留・押出加工法による高純度マグネシウム板材の作製2017

    • Author(s)
      毛利拓哉,井上誠,青柳成俊,三浦博己,会田哲夫
    • Organizer
      日本金属学会・日本鉄鋼協会北陸信越支部平成29年度総会・連合講演会
    • Related Report
      2017 Annual Research Report
  • [Remarks] 高強度マテリアル開発・評価研究室 研究テーマ

    • URL

      http://www.str.me.tut.ac.jp/about.html

    • Related Report
      2018 Annual Research Report 2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 高強度棒状マグネシウム合金の製造方法2019

    • Inventor(s)
      三浦博己, 川本忠 博、冨樫博巳
    • Industrial Property Rights Holder
      三浦博己, 川本忠 博、冨樫博巳
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2019-023155
    • Filing Date
      2019
    • Related Report
      2019 Annual Research Report
  • [Patent(Industrial Property Rights)] 高強度棒状マグネシウム合金の製造方法2019

    • Inventor(s)
      三浦博己, 川本忠博、冨樫博巳
    • Industrial Property Rights Holder
      三浦博己, 川本忠博、冨樫博巳
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2019-023155
    • Filing Date
      2019
    • Related Report
      2018 Annual Research Report

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Published: 2017-04-28   Modified: 2022-03-04  

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