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Heterogeneity of dislocation substructure in polycrystalline metals and its influence on mechanical properties

Research Project

Project/Area Number 17H06933
Research Category

Grant-in-Aid for Research Activity Start-up

Allocation TypeSingle-year Grants
Research Field Physical properties of metals/Metal-base materials
Research InstitutionKyushu University

Principal Investigator

Yamasaki Shigeto  九州大学, 総合理工学研究院, 助教 (00804741)

Research Collaborator Mitsuhara Masatoshi  
Nakashima Hideharu  
Project Period (FY) 2017-08-25 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Fiscal Year 2018: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2017: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Keywords転位 / 電子顕微鏡 / 金属材料 / 塑性変形 / 転位組織 / 金属 / 強度 / 変形 / 金属物性
Outline of Final Research Achievements

Dislocation substructure development in pure nickel deformed by SEM in-situ tensile test was observed by SEM electron channeling contrast method. In pure nickel, an increase in slip lines and dislocation pileup near grain boundaries were observed. In the case of hexagonal titanium alloys, dislocations mainly active in prism slip and basal slip were observed in the grains. On the other hand, in the vicinity of grain boundaries, dislocation lines considered to be active on the pyramidal surface were frequently observed. It is understood that this is because, in the hexagonal titanium alloy having low crystal symmetry, the activity of pyramidal slip is activated in the vicinity of the grain boundary in order to maintain the continuity of displacement with adjacent grains.

Academic Significance and Societal Importance of the Research Achievements

本研究成果より、強化が施された実用合金ではSEM-ECCI法により材料中の転位組織の発達やその不均一性を観察できることが明らかとなった。転位組織の発達挙動を理解することは材料の力学特性を理解する上で非常に重要であり、本手法は実用合金の組織評価に関して極めて有用な方法である。

Report

(3 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Annual Research Report
  • Research Products

    (4 results)

All 2018

All Presentation (4 results) (of which Int'l Joint Research: 2 results,  Invited: 2 results)

  • [Presentation] Relationship between Creep Deformation and Microstructure of Heat-Resistant Alloys2018

    • Author(s)
      Shigeto Yamasaki
    • Organizer
      MJIIT MICROSCOPY LABORATORY WORKSHOP SERIES-2
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 耐熱合金の微細組織の観察・測定と評価2018

    • Author(s)
      山﨑重人, 光原昌寿, 中島英治
    • Organizer
      IHI Materials Forum 2018
    • Related Report
      2018 Annual Research Report
  • [Presentation] 耐熱合金のクリープ変形の測定と定量的組織観察2018

    • Author(s)
      山﨑重人
    • Organizer
      第1回若手研究グループ「多様な先端観察・測定法を用いた組織の定量と力学特性解析への適用」
    • Related Report
      2018 Annual Research Report
  • [Presentation] Dislocation Structure Observation by FE-SEM2018

    • Author(s)
      Shigeto Yamasaki
    • Organizer
      MJIIT Microscopy Lab Workshop Series 2
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited

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Published: 2017-08-25   Modified: 2020-03-30  

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