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Highly efficient chemical mechanical polishing method for SiC substrates using enhanced slurry containing bubbles of plasma gas

Research Project

Project/Area Number 17K06094
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Production engineering/Processing studies
Research InstitutionKanazawa Institute of Technology

Principal Investigator

UNEDA Michio  金沢工業大学, 工学部, 教授 (00298324)

Co-Investigator(Kenkyū-buntansha) 佐野 泰久  大阪大学, 工学研究科, 准教授 (40252598)
Project Period (FY) 2017-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2019: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2018: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2017: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
KeywordsSiC基板 / プラズマガス / ナノバブル / CMP / 高能率 / 表面改質 / 超精密加工 / 研磨・CMP
Outline of Final Research Achievements

This study proposed a highly efficient method for chemical mechanical polishing (CMP) of silicon carbide (SiC) substrates using enhanced slurry. The enhanced slurry contains nano-bubbles of plasma gas in pure water mixed with a conventional commercially available slurry. Therefore, the enhanced slurry could be expected to have an oxidizing effect on the Si-face of SiC substrates. In order to investigate the effectiveness of bubbles enclosing plasma gas, both nano-indentation test and X-ray photoelectron spectroscopy (XPS) analysis were performed. As a result, the hardness decrease of the Si-face of the SiC substrate was observed through the nano-indentation test, and the reaction products was generated on Si-face of SiC substrate in the XPS analysis. From a series of experimental CMP results, the removal rate increased when the enhanced slurry was applied, comparing with that for the not only conventional commercially available slurry but also commercially available dedicated slurry.

Academic Significance and Societal Importance of the Research Achievements

本研究では低炭素社会を実現するために必須となる高効率パワーデバイスの開発に向けて,それに必要となるSiC基板の高能率研磨手法の開発に取り組んだものである.開発手法は特筆すべき装置を必要とせず,汎用の研磨装置へ適用可能なものであり,実用化を強く意識した内容である.その結果として,狙いとする高能率研磨の実現に成功するとともに,その原理(メカニズム)を明らかにしたことは,本研究における成果の信頼性向上(社会的意義)に加えて,学術的意義を明確にしたものであると言え,本研究の波及効果は極めて高いものと考えられる.

Report

(5 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • 2017 Research-status Report
  • Research Products

    (7 results)

All 2020 2019 2018 2017

All Journal Article (4 results) (of which Peer Reviewed: 4 results) Presentation (3 results)

  • [Journal Article] Highly efficient chemical mechanical polishing method for SiC substrates using enhanced slurry containing bubbles of ozone gas2020

    • Author(s)
      Uneda Michio、Fujii Koji
    • Journal Title

      Precision Engineering

      Volume: 64 Pages: 91-97

    • DOI

      10.1016/j.precisioneng.2020.03.015

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of High Efficiency Polishing Method of SiC Substrate assisted by Nanobubbles Containing Ozone Gas2019

    • Author(s)
      Koji Fujii and Michio Uneda
    • Journal Title

      Proceedings of International Conference on Planarization/CMP Technology 2019

      Volume: 1 Pages: 171-172

    • Related Report
      2019 Research-status Report
    • Peer Reviewed
  • [Journal Article] High Efficient CMP Method of SiC by Enhanced Slurry Containing Nano-bubbleswith Active Gas2018

    • Author(s)
      Koji Fujii, Michio Uneda, Kazutaka Shibuya, Yoshio Nakamura, Daizo Ichikawa and Ken-ichi Ishikawa
    • Journal Title

      Proceedings of International Conference on Planarization/CMP Technology 2018

      Volume: 1 Pages: 310-313

    • Related Report
      2018 Research-status Report
    • Peer Reviewed
  • [Journal Article] Chamical Mechanical Polishing of SiC Substrate Using Enhanced Slurry Containing Nanobubbles with Active Gas Generated by Plasma2017

    • Author(s)
      Shinya MIZUUCHI, Michio UNEDA, Kazutaka SHIBUYA, Yoshio NAKAMURA, Daizo ICHIKAWA and Ken-ichi ISHIKAWA
    • Journal Title

      Proceedings of International Conference on Planarization/CMP Technology 2017

      Volume: 1 Pages: 372-376

    • Related Report
      2017 Research-status Report
    • Peer Reviewed
  • [Presentation] オゾンガス内包ナノバブル添加スラリーによるSiC基板の高能率研磨加工法の研究2019

    • Author(s)
      藤井皐司,畝田道雄
    • Organizer
      2019年度精密工学会秋季大会学術講演会講演論文集
    • Related Report
      2019 Research-status Report
  • [Presentation] 活性ガス内包ナノバブル添加スラリーによるSiC基板の高能率研磨加工法の研究2018

    • Author(s)
      水内伸哉,畝田道雄,澁谷和孝,中村由夫,市川大造,石川憲一
    • Organizer
      2018年度精密工学会春季大会学術講演会講演論文集
    • Related Report
      2017 Research-status Report
  • [Presentation] 活性ガス内包ナノバブル添加スラリー供給装置の開発とそれによるSiC基板の高能率CMPの試み2017

    • Author(s)
      水内伸哉,畝田道雄,澁谷和孝,中村由夫,市川大造,石川憲一
    • Organizer
      2017年度精密工学会秋季大会学術講演会講演論文集
    • Related Report
      2017 Research-status Report

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Published: 2017-04-28   Modified: 2022-01-27  

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