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Development of high performance polycrystalline metallic materials by precise evaluation of grain boundary microstructure based on fractal analysis

Research Project

Project/Area Number 17K06820
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Composite materials/Surface and interface engineering
Research InstitutionAshikaga University

Principal Investigator

Kobayashi Shigeaki  足利大学, 工学部, 教授 (00323931)

Project Period (FY) 2017-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2020: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2019: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2018: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2017: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Keywords表界面工学 / 粒界 / 組織制御 / 疲労破壊 / 粒界腐食 / 電気抵抗率 / フラクタル / 粒界工学 / フェライト系ステンレス鋼 / 結晶粒界 / 加工熱処理 / ニッケル / 表面・界面物性 / 構造・機能材料
Outline of Final Research Achievements

The quantitative evaluation of the spatial distribution of grain boundaries which predominantly affected to fracture and corrosion in polycrystalline metallic materials can be achieved using fractal analysis. It was clarified that the fractal dimension of grain boundary spatial distribution is proportional to the grain boundary density which determined by the length of specific type grain boundaries per unit area. This result provides the fundamental knowledge of the control method of grain boundary spatial distribution. This study revealed that the control of segregation embrittlement, fatigue fracture, intergranular corrosion and electrical resistivity can be achieved by the grain boundary spatial distribution control.

Academic Significance and Societal Importance of the Research Achievements

粒界工学を用いた多結晶材料の高性能化・長寿命化に関する研究は、これまで主として粒界性格分布と呼ばれる、異なる性格をもつ粒界の存在頻度を統計的にまとめた組織因子の評価によって行われてきた。本研究では、粒界工学の精密化を目的として、特定の粒界の空間的な分布状態を定量化することを試み、フラクタルを用いた新しい粒界微細組織の評価手法を見出した点において当該分野の学術基盤の強化に寄与するものと考える。また、本研究の粒界空間幾何学分布の制御は、材料の長寿命化を可能とすることから省資源化や環境負荷低減など社会的にも意義は大きい。

Report

(5 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • 2017 Research-status Report
  • Research Products

    (13 results)

All 2021 2020 2019 2018 2017

All Journal Article (3 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 3 results,  Open Access: 2 results) Presentation (10 results) (of which Int'l Joint Research: 2 results,  Invited: 3 results)

  • [Journal Article] Low-angle boundary engineering for improving high-cycle fatigue property of 430 ferritic stainless steel2020

    • Author(s)
      Shigeaki Kobayashi, Weitao Yang, Yuuki Tomobe, Rei Okada, Sadahiro Tsurekawa
    • Journal Title

      Journal of Materials Science

      Volume: 55 Issue: 22 Pages: 9273-9285

    • DOI

      10.1007/s10853-020-04555-0

    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Grain Boundary Engineering for Control of Fatigue Fracture in 316L Austenitic Stainless Steel2019

    • Author(s)
      Shigeaki Kobayashi, Satoshi Ogou, Sadahiro Tsurekawa
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 60 Issue: 5 Pages: 623-630

    • DOI

      10.2320/matertrans.MB201804

    • NAID

      130007636512

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2019-03-01
    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of grain boundary microstructure on fatigue crack propagation in ferritic stainless steel2018

    • Author(s)
      楊 蔚涛、小林 重昭、斎藤 栄
    • Journal Title

      Transactions of the JSME (in Japanese)

      Volume: 84 Issue: 857 Pages: 17-00353-17-00353

    • DOI

      10.1299/transjsme.17-00353

    • NAID

      130006320923

    • ISSN
      2187-9761
    • Related Report
      2018 Research-status Report 2017 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] フェライト系ステンレス鋼に対する低角粒界導入型粒界工学プロセスの検討2021

    • Author(s)
      小林重昭, 寺門雅文, 江幡向晟, 連川貞弘
    • Organizer
      日本金属学会2021年春期講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] SUS430鋼の低角粒界導入型粒界制御による特性評価2020

    • Author(s)
      寺門雅文, 小林重昭
    • Organizer
      日本機械学会第28回機械材料・材料加工技術講演会(M&P2020)
    • Related Report
      2020 Annual Research Report
  • [Presentation] SUS304ステンレス鋼の耐粒界腐食性向上のための粒界制御2019

    • Author(s)
      岡田伶, 小林重昭
    • Organizer
      日本金属学会2019年秋期講演大会
    • Related Report
      2019 Research-status Report
  • [Presentation] 粒界制御によるフェライト系ステンレス鋼の疲労特性向上2019

    • Author(s)
      小林重昭, 友部優希
    • Organizer
      日本機械学会2019年度年次大会
    • Related Report
      2019 Research-status Report
  • [Presentation] Control of low-angle boundary network for improving high-cycle fatigue in 430 ferritic stainless steel2019

    • Author(s)
      Shigeaki Kobayashi, Weitao Yang, Yuuki Tomobe, Rei Okada, Sadahiro Tsurekawa
    • Organizer
      Intergranular and Interphase Boundaries in Materials (IIB2019)
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] Grain boundary engineering based on fractal analysis for control of intergranular corrosion in metallic materials2018

    • Author(s)
      S. Kobayashi, W. Yang, R. Okada, S. Tsurekawa
    • Organizer
      International Conference on Processing & Manufacturing of Advanced Materials (THERMEC 2018)
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 粒界微細組織のフラクタル解析に基づく粒界工学の精密化と金属材料の高性能化2018

    • Author(s)
      小林重昭
    • Organizer
      日本金属学会2018年春期(第162回)講演大会
    • Related Report
      2018 Research-status Report
    • Invited
  • [Presentation] 粒界の空間幾何学分布のフラクタル解析に基づくニッケルの偏析脆性制御2018

    • Author(s)
      小林重昭, 松原定弘
    • Organizer
      日本機械学会2018年次大会
    • Related Report
      2018 Research-status Report
  • [Presentation] SUS304ステンレス鋼の双晶導入型粒界制御プロセスの最適化2017

    • Author(s)
      岡田伶,小林重昭
    • Organizer
      山梨講演会2017
    • Related Report
      2017 Research-status Report
  • [Presentation] 粒界微細組織のフラクタル解析に基づく粒界工学の精密化と金属材料の高性能化2017

    • Author(s)
      小林重昭
    • Organizer
      日本金属学会春期講演大会
    • Related Report
      2017 Research-status Report
    • Invited

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Published: 2017-04-28   Modified: 2022-01-27  

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