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Hydrogen embrittlement-resistant upgradation and its mechanism of ultrahigh strength steel through texture control

Research Project

Project/Area Number 17K06852
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Structural/Functional materials
Research InstitutionJapan Atomic Energy Agency

Principal Investigator

XU Pingguang  国立研究開発法人日本原子力研究開発機構, 原子力科学研究部門 原子力科学研究所 物質科学研究センター, 研究副主幹 (80554667)

Project Period (FY) 2017-04-01 – 2020-03-31
Project Status Completed (Fiscal Year 2019)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2019: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2018: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2017: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Keywords集合組織 / 鉄鋼材料 / 水素脆化 / 中性子回折 / Texture evaluation / Hydrogen embrittlement / High stength steel plate / Neutron diffraction / Texture analysis / Tensile deformation / high strength steel / Hydrogen charging / High strength steel / 遅れ破壊 / 超高強度鋼 / 集合組織制御
Outline of Final Research Achievements

The hydrogen-charged and non-charged high strength steel plates were investigated using the neutron diffraction experiments of tensile deformation. The formation of tensile textures during the uniform deformation were both observed for two cases, however, the formation of fiber texture in the hydrogen-charged case was found much rapider than that in the non-charged case. Hydrogen reduces the cohesive strength of iron cubic cell atoms along crystallographic planes, which results into the lower cooperative deformation capability among various oriented grains and the rapider formation of crystal defects. Accordingly, the heterogeneous deformation occurs in some grains than the others, finally leads to a reduced uniform elongation rate. Moreover, the rolling direction of steel plate shows better hydrogen embrittlement resistance than the transverse direction, so that the texture optimization is found possible to improve the directionality of hydrogen embrittlement of steel plate.

Academic Significance and Societal Importance of the Research Achievements

自動車などの軽量化のために超高強度鋼が急速開発されている一方、微量な水素による危険な延性低下現象が生じるメカニズムの解明が必要である。これまで多くの水素脆化学説があったが、その統合的な解明には、バルク材料を負荷しながら水素脆化破断に至る結晶配向を含むその場組織変形挙動が不可欠だった。本研究では、水素含有有無の条件は集合組織がある高強度鋼板の単軸変形挙動とその異方向特性に影響すること、また、集合組織制御によって、水素脆化の異方向特性が一定程度に改善される可能性があることを解明した。この研究が今後の超高強度鋼板の開発に応用され、将来的には地球温暖化問題の解決にも貢献していくと期待できる。

Report

(4 results)
  • 2019 Annual Research Report   Final Research Report ( PDF )
  • 2018 Research-status Report
  • 2017 Research-status Report
  • Research Products

    (13 results)

All 2020 2019 2018 2017

All Journal Article (2 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 2 results,  Open Access: 2 results) Presentation (10 results) (of which Int'l Joint Research: 3 results,  Invited: 3 results) Funded Workshop (1 results)

  • [Journal Article] In-house texture measurement using a compact neutron source2020

    • Author(s)
      Xu, P.G., Ikeda, Y., Hakoyama, T., Takamura, M., Otake, Y. & Suzuki, H.
    • Journal Title

      Journal of Applied Crystallography

      Volume: 53 Issue: 2 Pages: 444-454

    • DOI

      10.1107/s1600576720002551

    • NAID

      120006956365

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] High stereographic resolution texture and residual stress evaluation using time-of-flight neutron diffraction2018

    • Author(s)
      Xu Pingguang、Harjo Stefanus、Ojima Mayumi、Suzuki Hiroshi、Ito Takayoshi、Gong Wu、Vogel Sven C.、Inoue Junya、Tomota Yo、Aizawa Kazuya、Akita Koichi
    • Journal Title

      Journal of Applied Crystallography

      Volume: 51 Issue: 3 Pages: 746-760

    • DOI

      10.1107/s1600576718004004

    • Related Report
      2017 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Presentation] Effect of Hydrogen Charging on Anisotropic Tensile Deformation Behavior of High Strength Steel Plate2019

    • Author(s)
      Pingguang Xu, Yasuhiro Ishijima, Hai Qiu, Satoshi Morooka, Wu Gong, Stefanus Harjo
    • Organizer
      J-PARC Symposium 2019
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Bulk Texture Measurement Technique using Compact Neutron Source2019

    • Author(s)
      Pingguang Xu, Ryunosuke Kakuta, Masato Takamura, Yoshie Otake, Hiroshi Suzuki
    • Organizer
      8th International Meeting of the Union for Compact Accelerator-Driven Neutron Sources
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 鉄鋼材料の集合組織測定研究に関する大型中性子施設とRIKEN小型中性子源の連携2019

    • Author(s)
      徐平光, 高村正人, 池田義雅,角田竜之介,箱山智之,岩本ちひろ,大竹淑恵,鈴木裕士
    • Organizer
      2019年度理研シンポジウム:小型中性子源がインフラ・ものづくり現場の非破壊評価分析を変える
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] 理研小型中性子源システムRANS―集合組織計測を中心に2019

    • Author(s)
      大竹淑恵、高村正人、徐平光、鈴木裕士
    • Organizer
      日本鉄鋼協会第177回春季講演大会シンポジウム:「金属微細化組織解析を指向した量子ビーム応用の最前線~小型中性子源や小角散乱、回折から見える新しい情報」
    • Related Report
      2018 Research-status Report
  • [Presentation] Elastoplastic deformation behavior of textured high strength steel after hydrogen charging studied by neutron diffraction2018

    • Author(s)
      P.G. Xu, Y. Ishijima, H. Qiu
    • Organizer
      日本鉄鋼協会第176回秋季講演大会
    • Related Report
      2018 Research-status Report
  • [Presentation] 中性子回折法を用いた集合組織を有する高張力鋼板の水素脆化挙動評価2018

    • Author(s)
      徐平光,石島暖大,邱海,諸岡聡,S.ハルヨ
    • Organizer
      日本中性子科学会第18回年会
    • Related Report
      2018 Research-status Report
  • [Presentation] ひずみ・応力+集合組織の同時評価技術とその応用研究の最前線2018

    • Author(s)
      徐平光、S. ハルヨ、鈴木裕士、井上純哉
    • Organizer
      日本鉄鋼協会シンポジウム「材料強度特性のミクロ組織メカニクス-X 線・中性子の新しい視点-」
    • Related Report
      2017 Research-status Report
    • Invited
  • [Presentation] Tensile deformation and texture evolution in brittle/ductile multilayered steel sheet studied by neutron diffraction2018

    • Author(s)
      P.G. Xu, M. Ojima, H. Suzuki, S. Nambu, J. Inoue, Y. Onuki, S. Harjo, K. Akita
    • Organizer
      THERMEC'2018 International Conference on Processing and Manufracturing of Advanced Materials, Paris, France.
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] High Orientation Resolution Texture and Residual Stress Measurement of Multilayered Steel Using Neutron Diffraction2017

    • Author(s)
      P.G. Xu, J. Inoue, W. Gong, S. Harjo, H. Suzuki, K.Akita
    • Organizer
      日本鉄鋼協会第174回秋季講演大会、北海道札幌市
    • Related Report
      2017 Research-status Report
  • [Presentation] 中性子回折を用いた複層鋼板の集合組織と残留応力テンソル測定2017

    • Author(s)
      徐平光,井上純哉,S.ハルヨ,鈴木裕士,秋田貢一
    • Organizer
      日本金属学会分科会第1回金属・無機・有機材料の結晶方位解析と応用技術研究会公開講演会
    • Related Report
      2017 Research-status Report
  • [Funded Workshop] J-PARC Symposium 20192019

    • Related Report
      2019 Annual Research Report

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Published: 2017-04-28   Modified: 2022-12-28  

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