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Effect of alloying element on the ferrite transformation in nitrogen austenite

Research Project

Project/Area Number 17K17581
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Material processing/Microstructural control engineering
Structural/Functional materials
Research InstitutionTohoku University

Principal Investigator

Sato Mitsutaka  東北大学, 金属材料研究所, 助教 (10547706)

Research Collaborator Furuhara Tadashi  
Miyamoto Goro  
Project Period (FY) 2017-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2018: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Fiscal Year 2017: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywordsフェライト変態 / 窒素鋼 / 相界面析出 / エネルギー散逸 / 窒素オーステナイト / TRIP鋼 / 構造・機能材料 / 相変態
Outline of Final Research Achievements

In this research, ferrite transformation behavior of Fe-N alloy and the effect of alloying element were investigated using pure iron and 1 mass% of Mn, Mo and Cr added alloy. The nitrogen austenite was obtained by nitriding method, and then, the nitrided samples were isothermally treated in the α + γ two-phase region for several period of time.
The two types of morphology of AF and WF were obtained with changes in the driving force of ferrite transformation. The AF was nucleated from the prior austenite grain boundaries, and the AF has K-S OR with one side of the adjacent prior austenite grains and grew into the grains having non K-S OR. On the other hand, the WF had the K-S OR with the prior austenite grain. Transformation was retarded by the addition of Mn and Mo. In the Cr added alloy, the ferrite transformation progressed with the interface precipitation of CrN.

Academic Significance and Societal Importance of the Research Achievements

本研究により、Fe-N合金におけるフェライト変態はこれまでに報告されている炭素鋼における変態挙動と良く似た挙動を示し、炭素鋼での知見を基にFe-N系合金における変態挙動を理解することが可能であることが明らかとなった。一方で、窒化物形成能の高い元素であるCrを添加した試料では,CrN の相界面析出が生じることが明らかとなった。炭素鋼では相界面析出によりフェライトを強化した複相鋼板は高強度-高延性材料として現在幅広く利用されている鋼種であり、本研究の結果は窒素を利用した窒化物析出による新しい高強度鋼の開発へとつながる。

Report

(3 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • Research Products

    (13 results)

All 2019 2018 2017

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (12 results) (of which Int'l Joint Research: 2 results)

  • [Journal Article] Microstructure of reverted austenite in Fe-0.3N martensite2018

    • Author(s)
      Sato Mitsutaka、Matsumoto Sou、Miyamoto Goro、Furuhara Tadashi
    • Journal Title

      Scripta Materialia

      Volume: 156 Pages: 85-89

    • DOI

      10.1016/j.scriptamat.2018.07.020

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] 高窒素オーステナイトを含む複相鋼の引張特性2019

    • Author(s)
      菊地一茂、佐藤充孝、宮本吾郎、古原 忠
    • Organizer
      日本鉄鋼協会 第177回春季講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Fe-0.3NおよびFe-0.3N-1X (X : Cr, Mo, Mn)オーステナイトからのフェライト生成挙動2019

    • Author(s)
      佐藤充孝、村田貴優、宮本吾郎、古原 忠
    • Organizer
      日本鉄鋼協会 第177回春季講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Fe-1M-0.3mass%N(M : Si, Cr, Mo)のベイナイト変態挙動2018

    • Author(s)
      島谷将太,佐藤充孝,宮本吾郎,古原忠
    • Organizer
      日本鉄鋼協会第175回春季講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 窒素オーステナイトのフェライト変態挙動2018

    • Author(s)
      村田貴優、宮本吾郎、古原 忠
    • Organizer
      日本鉄鋼協会 第176回秋季講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Effect of alloying element on the microstructure during reverse transformation of Fe-0.3N martensite2018

    • Author(s)
      Mitsutaka Sato, Sou Matsumoto, Goro Miyamoto, Tadashi Furuhara
    • Organizer
      The 6th conference of the Combined Australian Materials Sciences
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 窒素マルテンサイトの逆変態挙動に及ぼす合金元素添加の影響2018

    • Author(s)
      佐藤充孝,松本宗,宮本吾郎,古原忠
    • Organizer
      日本鉄鋼協会第175回春季講演大会
    • Related Report
      2017 Research-status Report
  • [Presentation] Fe-1M-0.3mass%N(M : Si, Cr, Mo)のベイナイト変態挙動2018

    • Author(s)
      佐藤充孝,島谷将太,宮本吾郎,古原忠
    • Organizer
      日本鉄鋼協会第175回春季講演大会
    • Related Report
      2017 Research-status Report
  • [Presentation] 鉄-窒素マルテンサイト組織からのオーステナイト逆変態挙動2017

    • Author(s)
      松本宗,佐藤充孝,宮本吾郎,古原忠
    • Organizer
      日本鉄鋼協会第174回秋季講演大会
    • Related Report
      2017 Research-status Report
  • [Presentation] 低窒素鋼のベイナイト変態に及ぼす合金元素の影響2017

    • Author(s)
      島谷将太,佐藤充孝,宮本吾郎,古原忠
    • Organizer
      日本鉄鋼協会第174回秋季講演大会
    • Related Report
      2017 Research-status Report
  • [Presentation] Fe-1M-0.3mass%N (M : Si, Cr, Mn, Mo)マルテンサイトの焼戻し挙動2017

    • Author(s)
      佐藤充孝,古原忠
    • Organizer
      日本鉄鋼協会第174回秋季講演大会
    • Related Report
      2017 Research-status Report
  • [Presentation] Tempering behavior of iron-nitrogen-based matensite2017

    • Author(s)
      Mitsutaka Sato,Tadashi Furuhara
    • Organizer
      The 5th International Symposium on Steel Science
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] Fe-0.3mass%N-1M(M : Mn,Mo)マルテンサイト組織からのオーステナイト逆変態挙動2017

    • Author(s)
      松本宗,佐藤充孝,宮本吾郎,古原忠
    • Organizer
      日本熱処理技術協会 第84回秋季講演大会
    • Related Report
      2017 Research-status Report

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Published: 2017-04-28   Modified: 2020-03-30  

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