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Application of nano-polycrystalline diamond to high-pressure technique using multi anvil apparatus

Research Project

Project/Area Number 17K18806
Research Category

Grant-in-Aid for Challenging Research (Exploratory)

Allocation TypeMulti-year Fund
Research Field Earth and planetary science and related fields
Research InstitutionEhime University

Principal Investigator

Kunimoto Takehiro  愛媛大学, 地球深部ダイナミクス研究センター, 特定研究員 (20543169)

Project Period (FY) 2017-06-30 – 2020-03-31
Project Status Completed (Fiscal Year 2019)
Budget Amount *help
¥6,370,000 (Direct Cost: ¥4,900,000、Indirect Cost: ¥1,470,000)
Fiscal Year 2018: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2017: ¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Keywordsナノ多結晶ダイヤモンド / 高圧発生 / マルチアンビル装置 / 超高圧発生 / マントルー核境界 / 6-8-2式高圧セル / 地球マントル最下部 / マルチアンビル型高圧発生装置 / 核ーマントル境界
Outline of Final Research Achievements

The pressures available in Kawai-type multianvil apparatus (KMA), using tungsten carbide or sintered diamond, have been limited to about 30 GPa and 60 GPa, respectively. Recent efforts in introductions of new materials and improvements in cell assemblies significantly expanded these limits to 60 GPa for WC anvils and 120 GPa for SD anvils.
We have been trying to improve the cell for the 6-8-2 cell to generate the pressure equivalent to the Earth’s core-mantle boundary (CMB), for better understanding of this heterogeneous region.
Experiments were conducted using the KMA at SPring-8. Generated pressures were determined from the unit cell volumes of Au using adequate equation of state. We reached pressures of about 150 GPa in two independent runs, which are the highest pressure ever reported in KMA. The pressure achieved in these runs completely cover the entire D” region (approx. 125-135 GPa), and some attempts have also been made to produce high temperatures under such pressures.

Academic Significance and Societal Importance of the Research Achievements

地球内部、特にマントル最下部条件(CMB)の物質科学的研究は主にダイヤモンドアンビル装置(DAC)を用いて行われてきた。しかしながらDACの場合、高温発生や温度測定において大きな誤差を含むため、研究内容によっては信頼性に乏しい場合もある。
本研究ではマルチアンビル装置を用いてCMBに相当する圧力発生を可能とした。そのため、これまでDACで実施された相境界の決定などの再現実験や実際のマントルに近い組成の試料を用いた実験を行うことで、これまで明らかにされてきた地球内部環境を再確認し、さらに新たな知見を加える事が期待できる。

Report

(4 results)
  • 2019 Annual Research Report   Final Research Report ( PDF )
  • 2018 Research-status Report
  • 2017 Research-status Report
  • Research Products

    (5 results)

All 2020 2019 2018 2017

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (4 results) (of which Int'l Joint Research: 2 results)

  • [Journal Article] High pressure generation in Kawai-type multianvil apparatus using nano-polycrystalline diamond anvils2019

    • Author(s)
      T. Irifune, T. Kunimoto, T. Shinmei, Y. Tange
    • Journal Title

      Comptes Rendus Geoscience

      Volume: 351 Issue: 2-3 Pages: 260-260

    • DOI

      10.1016/j.crte.2018.07.005

    • Related Report
      2019 Annual Research Report 2018 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] High-pressure generation to 150 GPa in multianvil apparatus using the 6-8-2 system with nano-polycrystalline diamond anvils.2020

    • Author(s)
      Takehiro Kunimoto, and Tetsuo IRIFUNE
    • Organizer
      JpGU-AGU joint meeting 2020: Virtual
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] ナノ多結晶ダイヤモンドの圧縮挙動2018

    • Author(s)
      入舩徹男,上田千晶,境毅,國本健広,有本岳史,新名亨,門林宏和,大藤弘明,八木健彦,河口沙織,河口彰吾
    • Organizer
      第59回高圧討論会
    • Related Report
      2018 Research-status Report
  • [Presentation] X線その場観察実験と電気抵抗測定によるGaP,GaAs,ZnS, ZnTeの構造相転移と圧力誘起金属化の観察2018

    • Author(s)
      國本健広、入舩徹男
    • Organizer
      第59回高圧討論会
    • Related Report
      2018 Research-status Report
  • [Presentation] Generation of ~90 GPa in Kawai-type multianvil apparatus using nano-polycrystalline diamond anvils.2017

    • Author(s)
      Takehiro Kunimoto, and Tetsuo Irifune
    • Organizer
      JpGU-AGU joint meeting 2017
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research

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Published: 2017-07-21   Modified: 2021-02-19  

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