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Development and application of crystal structure analysis technology with polarized X-ray multiple wave method

Research Project

Project/Area Number 18540310
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Condensed matter physics I
Research InstitutionThe University of Tokyo

Principal Investigator

OKITSU Kouhei  The University of Tokyo, Graduate School of engineering, Research Associate (50323506)

Co-Investigator(Kenkyū-buntansha) IMAI Yasuhiko  The University of Tokyo, SPring-8, Researcher (30416375)
YODA Yoshitaka  The University of Tokyo, SPring-8, Researcher (90240366)
上エ地 義徳  東京大学, 大学院新領域創成科学研究科, 助手 (10312985)
Project Period (FY) 2006 – 2007
Project Status Completed (Fiscal Year 2007)
Budget Amount *help
¥2,840,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥240,000)
Fiscal Year 2007: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2006: ¥1,800,000 (Direct Cost: ¥1,800,000)
KeywordsX-ray diffraction / Dynamical diffraction thoery / Simultaneous diffraction / Polarization / Phase problem / Computer simulation / Takagi-Taupin equation / Refraction imaging / X線動力学的回折理論 / X線結晶構造解析 / シンクロトロン放射光
Research Abstract

Takagi-Taupin equation (T-T theory) has been widely known since its derivation by Takagi as an X-ray dynamical diffraction theory that can deal with wave fields in a deformed crystal. The Ewald-Laue dynamical theory (E-L theory) has been considered as an principle X-ray dynamical diffraction theory while the T-T theory has been considered to be a special theory However, it should be noted that the E-L and T-T theories are equivalent to each other. The T-T theory describes the X-ray wave fields in a crystal in the real space while the E-L theory describes those in the reciprocal space. The E-L theory was extended to three-beam case in the late 1969's and a numerical method to solve it was given by Colella in 1974. However, the T-T theory has been considered not able to be solved for multiple wave condition until the present author gave a numerical method to solve it for multiple wave cases.
Furthermore, the T-T theory can be solved numerically but only for plane-wave and spherical wave X-ray incidence condition but also for an arbitrary X-ray incidence condition. Recently Ando and his coworkers studies on refraction contrast imaging using an analyzer crystal that can obtain clear images even when normal absorption images cannot be obtained at all due to the faint absorption inhomogeneity of object. In 2007 fiscal year, the present author made a study focusing on computer simulation of refraction contrast imaging. The computer-simulated refraction contrast images well agreed with practical images obtained by experiments. Therefore, it has come to be able to evaluate favorable condition required to the analyzer crystal. Further, X-ray refraction computed tomography (CT) and tomothynthes images that can be obtained by rotating the object, can be expected before experiment. This simulation was performed by taking advantage of the feature of T-T equation that can deal with an arbitrary incidence condition of X-rays.

Report

(3 results)
  • 2007 Annual Research Report   Final Research Report Summary
  • 2006 Annual Research Report
  • Research Products

    (6 results)

All 2006 Other

All Journal Article (3 results) (of which Peer Reviewed: 1 results) Remarks (3 results)

  • [Journal Article] Polarization-dependent six-beam X-ray pinhole topographs2006

    • Author(s)
      Kouhei Okitsu, Yoshitaka Yoda, Yasuhiko Imai, Yoshinori Ueji, Yuta Urano and Xiao Wei Zhang
    • Journal Title

      Acta Cryst. A 62

      Pages: 237-247

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Polarization-dependent six-beam X-ray pinhole topographs2006

    • Author(s)
      K. Okitsu, Y. Yoda, Y. Imai, Y. Ueji, Y. Urano and X. -W. Zhang
    • Journal Title

      Acta Cryst A62

      Pages: 237-247

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Poloarization-dependent six-beam X-ray pinhole topographs2006

    • Author(s)
      K.Okitsu, et al.
    • Journal Title

      Acta Crystallographica Sction A 62

      Pages: 237-247

    • Related Report
      2006 Annual Research Report
  • [Remarks] 「研究成果報告書概要(和文)」より

    • URL

      http://park.itc.u-tokyo.ac.jp/hpx/

    • Related Report
      2007 Final Research Report Summary
  • [Remarks]

    • URL

      http://park.itc.u-tokyo.ac.jp/hpx/Takagi-Taupin_equation/index.html

    • Related Report
      2007 Annual Research Report
  • [Remarks] このURLには、研究遂行上秘匿すべき事項が含まれるため、IDとパスワードを公表できない。

    • URL

      http://park.itc.u-tokyo.ac.jp/hpx/RefractionImageSimulation/RefractionImages.html

    • Related Report
      2007 Annual Research Report

URL: 

Published: 2006-04-01   Modified: 2020-05-15  

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