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Synthesis of oxide-sugar alcohol nanocomplex structure by cooperative hydrolysis reaction and its application

Research Project

Project/Area Number 18550177
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Inorganic industrial materials
Research InstitutionChiba University

Principal Investigator

UEKAWA Naofumi  Chiba University, 大学院・工学研究科, 准教授 (60282448)

Project Period (FY) 2006 – 2008
Project Status Completed (Fiscal Year 2008)
Budget Amount *help
¥4,180,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥480,000)
Fiscal Year 2008: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2007: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2006: ¥2,100,000 (Direct Cost: ¥2,100,000)
Keywords酸化チタン / 溶液法 / ナノ粒子 / 糖アルコール / 蛍光 / グリコール / ナノ複合体 / 二次粒子 / 安定分散系
Research Abstract

酸化物ナノ粒子のナノレベルでの分散および集合構造を制御することでその多様な電子・光物性および触媒活性を制御することが可能になる。本研究では高い親水性と生体親和性を有するだけでなく遷移金属イオンへ強く配位子しその加水分解反応を制御することが可能であるグリコール類などの多価アルコールおよび糖アルコールに着目し、酸化物ナノ粒子-糖アルコール複合体の作成方法とその複合体ナノ粒子の物性の検討を行った。

Report

(4 results)
  • 2008 Annual Research Report   Final Research Report ( PDF )
  • 2007 Annual Research Report
  • 2006 Annual Research Report
  • Research Products

    (43 results)

All 2009 2008 2007 2006

All Journal Article (18 results) (of which Peer Reviewed: 8 results) Presentation (25 results)

  • [Journal Article] Synthesis of nitrogen-doped zinc oxide particles by thermal decomposition of mixture between zinc peroxide and ammonium salts2009

    • Author(s)
      N. Uekawa, Y. Mitani, T. Kojima, K. Kakegawa
    • Journal Title

      J. Ceram. Soc. Jpn. 117

      Pages: 283-288

    • Related Report
      2008 Final Research Report
  • [Journal Article] Synthesis of nitrogen-doped zinc oxide particles by thermal decomposition of mixture between zinc peroxide and ammonium salts2009

    • Author(s)
      N. Uekawa, Y. Mitani, T. Kojima, K. Kakegawa
    • Journal Title

      Journal of Ceramic Society of Japan 117

      Pages: 283-288

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of treatment conditions and titanium source on the hy drothermal synthesis of bismuth titanate particles2009

    • Author(s)
      T. Kojima, I. Yoshida, N. Uekawa, K. Kakegawa,
    • Journal Title

      Journal of the European Ceramic Society 29

      Pages: 431-437

    • NAID

      130006970861

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation of GdAlO_3-Al_2O_3 composite having fine pseudo-eutectic microstructure2008

    • Author(s)
      Y. Harada, K. Ayabe, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      J. Eurp. Ceram. Soc. 28

      Pages: 2941-2946

    • Related Report
      2008 Final Research Report
  • [Journal Article] Comparative examination of titania nanocrystals synthesized by peroxotitanic acid approach from different precursors2008

    • Author(s)
      Y. J. Liu, M. Aizawa, W. Q. Peng, Z. M. Wang, H. Hattori, N. Uekawa, H. Kanoh
    • Journal Title

      J. Colloid Inter. Sci. 322

      Pages: 497-504

    • NAID

      130006978602

    • Related Report
      2008 Final Research Report
  • [Journal Article] Formation of ultrafine eutectic-like microstructures of various rare earth oxide-Al_2O_3 systems by use of amorphous phases2008

    • Author(s)
      Y. Harada, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      J. Mater. Res. 29

      Pages: 3396-3402

    • Related Report
      2008 Final Research Report
  • [Journal Article] Formation of GdAI03-AI203 composite having fine pseudo-eut ectic microstructure2008

    • Author(s)
      Y. Harada, K. Ayabe, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      Journal of European Ceramic Society 28

      Pages: 2941-2946

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Comparative examination of titania nanocrystals synthesized by peroxotitanic acid approach from different precursors2008

    • Author(s)
      Y. J. Liu, M. Aizawa, W. Q. Peng, Z. M. Wang, H. Hattori, N. Uekawa, H. Kanoh
    • Journal Title

      Journal of Colloid and Interface Science 322

      Pages: 497-504

    • NAID

      130006978602

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation of ultrafine eutectic-like microstructures of various rare earth oxide-Al203 systems by use of amorphous phases2008

    • Author(s)
      Y. Harada, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      Journal of Material Research 23

      Pages: 3396-3402

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation of porous spherical aggregated structure of ZnO nanoparticles by low-temperature heating of Zn(OH)_2 in diol solution2007

    • Author(s)
      N. Uekawa, S. Ishii, T. Kojima, K. Kakegawa
    • Journal Title

      Mater. Lett. 61

      Pages: 1729-1734

    • Related Report
      2008 Final Research Report
  • [Journal Article] Formation process of BaTiO_3 particles by reaction between barium hydroxide aqueous solution and titania obtained by hydrolysis of titanium alkoxide2007

    • Author(s)
      Z. Min, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      J. Mater. Res. 22

      Pages: 2631-2638

    • Related Report
      2008 Final Research Report
  • [Journal Article] Synthesis of Titania Particles by Low-Temperature Hydrolysis Reaction of Titanium Alkoxide and Their Surface Characteristics2007

    • Author(s)
      Z. Min, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      J. Ceram. Soc. Jpn. 115

      Pages: 840-845

    • Related Report
      2008 Final Research Report
  • [Journal Article] Formation of porous spherical aggregated structure of ZnO nanoarticles by low-temerature heating of Zn(OH)_2 in diol solution2007

    • Author(s)
      N. Uekawa, S. Ishii, T. Kojima, K. Kakegawa
    • Journal Title

      Materials Letters 61

      Pages: 1729-1734

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation process of BaTiO3 particles by reaction between barium hydroxide aqueous solution and titania obtained by hydrolysis of titanium alkoxide2007

    • Author(s)
      Z. Min, N. Uekawa, T. Kojima, K. Kakegawa
    • Journal Title

      Journal of Materials Research 22

      Pages: 2631-2638

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis of Titania Particles by Low-Temperature Hydrolysis Reaction of Titanium Alkoxide and Their Surface Characteristics2007

    • Author(s)
      Z. Min, N. Uekawa, T. Kojma, K. Kakegawa
    • Journal Title

      Journal of Ceramic Society of Japan 115

      Pages: 840-845

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation of porous spherical aggregated structre of ZnO nanoparticles by low-temperature heating of Zn(OH)_2 in diol solution2007

    • Author(s)
      N.Uekawa, S.Ishii, T.Kojima, K.Kakegawa
    • Journal Title

      Materials Letters 61巻

      Pages: 1729-1734

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Synthesis and Characterization of Titania-Sugar Alcohol Complex Nanoparticles2006

    • Author(s)
      N. Uekawa, M. Suzuki, F. Mori, T. Kojima, K. Kakegawa
    • Journal Title

      J. Ceram. Soc. Jpn. 114

      Pages: 807-813

    • NAID

      110004839573

    • Related Report
      2008 Final Research Report
  • [Journal Article] Synthesis and Characterization of Titania-Sugar Alcohol Complex Nanoparticles2006

    • Author(s)
      N.Uekawa, m.Suzuki, F.Mori, T.Kojima, K.Kakegawa
    • Journal Title

      Journal of Ceramics Society of Japan 114巻・10号

      Pages: 807-813

    • NAID

      110004839573

    • Related Report
      2006 Annual Research Report
  • [Presentation] 硫化亜鉛沈殿の溶液中での解膠による硫化亜鉛ナノ粒子分散ゾルの調製2009

    • Author(s)
      上川直文, 松本貴彬, 小島隆, 掛川一幸
    • Organizer
      (社)日本セラミックス協会2009年年会
    • Place of Presentation
      千葉県
    • Year and Date
      2009-03-17
    • Related Report
      2008 Final Research Report
  • [Presentation] 硫化亜鉛沈殿の溶液中での解膠による硫化亜鉛ナノ粒子分散ゾルの調製2009

    • Author(s)
      上川直文、松本貴彬、小島隆、掛川一幸
    • Organizer
      (社)日本セラミックス協会2009年年会
    • Place of Presentation
      千葉
    • Year and Date
      2009-03-17
    • Related Report
      2008 Annual Research Report
  • [Presentation] アンモニウム塩と硝酸塩の混合融体中での反応によるNドープZnO粒子の合成2009

    • Author(s)
      上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第47回セラミックス基礎科学討論会
    • Place of Presentation
      大阪府
    • Year and Date
      2009-01-09
    • Related Report
      2008 Final Research Report
  • [Presentation] アンモニウム塩と硝酸塩の混合融体中での反応によるNドープZnO粒子の合成2009

    • Author(s)
      上川直文、小島隆、掛川一幸
    • Organizer
      (社)日本セラミックス協会第47回セラミックス基礎科学討論会
    • Place of Presentation
      大阪国際会議場
    • Year and Date
      2009-01-09
    • Related Report
      2008 Annual Research Report
  • [Presentation] 水酸化物の低温解膠による蛍光発光性ZnOナノ粒子安定分散ゾルの調製と共存陽イオンが蛍光発光特性に与える影響2008

    • Author(s)
      上川直文、山崎晃典、小島隆、掛川一幸
    • Organizer
      日本セラミックス協会第21回秋季シンポジウム
    • Place of Presentation
      福岡県
    • Year and Date
      2008-09-18
    • Related Report
      2008 Final Research Report
  • [Presentation] 低温溶液プロセスによるCeO_2ナノ粒子-高分子複合体膜の調製と光吸収特性の検討2008

    • Author(s)
      若松和哉, 上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第21回秋季シンポジウム
    • Place of Presentation
      福岡県
    • Year and Date
      2008-09-18
    • Related Report
      2008 Final Research Report
  • [Presentation] 水酸化物の低温解膠による蛍光発光性ZnOナノ粒子安定分散ゾルの調製と共存陽イオンが蛍光発光特性に与える影響2008

    • Author(s)
      上川直文、山崎晃典、小島隆、掛川一幸
    • Organizer
      (社)日本セラミックス協会第21回秋季シンポジウム
    • Place of Presentation
      北九州
    • Year and Date
      2008-09-18
    • Related Report
      2008 Annual Research Report
  • [Presentation] 低温溶液プロセスによるCeO2ナノ粒子-高分子複合体膜の調製と光吸収特性の検討2008

    • Author(s)
      若松和哉、上川直文、小島隆、掛川一幸
    • Organizer
      (社)日本セラミックス協会第21回秋季シンポジウム
    • Place of Presentation
      北九州
    • Year and Date
      2008-09-18
    • Related Report
      2008 Annual Research Report
  • [Presentation] Synthesis of TiO_2 Photocatalyst Particles by Low Temperature Hydrolysis Reaction of Alkoxides and Their Surface Characteristics2008

    • Author(s)
      N. Uekawa, M. Zeng, T. Kojima, K. Kakegawa
    • Organizer
      14^<th> International Congress on Catalysis
    • Place of Presentation
      Korea
    • Year and Date
      2008-07-17
    • Related Report
      2008 Final Research Report
  • [Presentation] Synthesis of TiO2 Photocatalyst Particles by Low Temperature Hydrolysis Reaction of Alkoxides and Their Surface Characteristics2008

    • Author(s)
      N. Uekawa, M. Zeng, T. Kojima, K. Kakegawa
    • Organizer
      14th International Congress on Catalysis
    • Place of Presentation
      ソウル・韓国
    • Year and Date
      2008-07-17
    • Related Report
      2008 Annual Research Report
  • [Presentation] 水酸化亜鉛の低温加熱処理による酸化亜鉛ナノ粒子の合成と蛍光発光特性の検討2008

    • Author(s)
      上川直文, 山崎晃範, 小島隆, 掛川一幸
    • Organizer
      第46回日本セラミックス協会基礎討論会
    • Place of Presentation
      愛知県
    • Year and Date
      2008-01-10
    • Related Report
      2008 Final Research Report
  • [Presentation] Photocatalytic activity of titanium oxide-sugar alcohol complex nanoparticles2007

    • Author(s)
      N. Uekawa, T. Kojima, K. Kakegawa
    • Organizer
      ISETS07
    • Place of Presentation
      Japan
    • Year and Date
      2007-11-24
    • Related Report
      2008 Final Research Report
  • [Presentation] Characterization of TiO_2 photocatalist nanoparticles prepared by low temperature hydrolysis reaction of alkoxides2007

    • Author(s)
      M. Zeng, N. Uekawa, T. Kojima, K. Kakegawa
    • Organizer
      ISETS07
    • Place of Presentation
      Japan
    • Year and Date
      2007-11-24
    • Related Report
      2008 Final Research Report
  • [Presentation] ペルオキシ化合物水溶液を用いたNbドープTiO_2の合成と物性の検討2007

    • Author(s)
      上川直文, 柿沼亮太, 大澤佑介, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第20回秋季シンポジウム
    • Place of Presentation
      愛知県
    • Year and Date
      2007-09-21
    • Related Report
      2008 Final Research Report
  • [Presentation] アルコキシドの低温加水分解によるTiO_2粒子の合成と表面特性の評価2007

    • Author(s)
      曾敏, 上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第20回秋季シンポジウム
    • Place of Presentation
      愛知県
    • Year and Date
      2007-09-21
    • Related Report
      2008 Final Research Report
  • [Presentation] チタンアルコキシドの低温加水分解反応による高表面積酸化チタンの合成と光触媒活性の検討2007

    • Author(s)
      曾 敏, 上川 直文, 小島 隆, 掛川 一幸
    • Organizer
      日本セラミックス協会
    • Place of Presentation
      名古屋工業大学
    • Year and Date
      2007-09-13
    • Related Report
      2007 Annual Research Report
  • [Presentation] 水酸化亜鉛のグリコール溶液中低温加熱処理による蛍光発光性ZnOナノ粒子の生成挙動2007

    • Author(s)
      山崎晃範, 上川直文, 小島隆, 掛川一幸
    • Organizer
      第23回日本セラミックス協会関東支部研究発表会
    • Place of Presentation
      東京都
    • Year and Date
      2007-08-31
    • Related Report
      2008 Final Research Report
  • [Presentation] 過酸化亜鉛ナノ粒子を前駆体として用いた窒素ドープZnOの調製法の検討2007

    • Author(s)
      上川直文, 三谷知裕, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会2007年年会
    • Place of Presentation
      東京都
    • Year and Date
      2007-03-23
    • Related Report
      2008 Final Research Report
  • [Presentation] 水酸化亜鉛のエチレングリコール中低温加熱処理による酸化亜鉛ナノ粒子の合成と蛍光発光特性の検討2007

    • Author(s)
      山崎晃範, 上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会2007年年会
    • Place of Presentation
      東京都
    • Year and Date
      2007-03-23
    • Related Report
      2008 Final Research Report
  • [Presentation] チタンアルコキシドの低温加水分解による高表面積酸化チタンの合成と光触媒活性の検討2007

    • Author(s)
      曾敏, 上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会2007年年会
    • Place of Presentation
      東京都
    • Year and Date
      2007-03-23
    • Related Report
      2008 Final Research Report
  • [Presentation] アンモニウム塩低温融体中での硝酸塩の分解によるZnO粒子の合成とキャラクタリゼーション2007

    • Author(s)
      上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会2008年年会
    • Place of Presentation
      新潟県
    • Year and Date
      2007-03-21
    • Related Report
      2008 Final Research Report
  • [Presentation] 溶液法による酸化物ナノ粒子安定分散ゾルの合成とナノ凝集構造制御2006

    • Author(s)
      上川直, 山崎晃範, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第19回秋季シンポジウム
    • Place of Presentation
      山梨県
    • Year and Date
      2006-09-21
    • Related Report
      2008 Final Research Report
  • [Presentation] 溶液を用いたCeO_2-TiO_2ナノ粒子複合体の合成と光還元反応の検討2006

    • Author(s)
      鈴木一也, 上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第19回秋季シンポジウム
    • Place of Presentation
      山梨県
    • Year and Date
      2006-09-21
    • Related Report
      2008 Final Research Report
  • [Presentation] チタンアルコキシドの直接加水分解反応によるBaTiO_3粒子の合成と粒子生成過程の検討2006

    • Author(s)
      曾敏, 上川直文, 小島隆, 掛川一幸
    • Organizer
      日本セラミックス協会第19回秋季シンポジウム
    • Place of Presentation
      山梨県
    • Year and Date
      2006-09-20
    • Related Report
      2008 Final Research Report
  • [Presentation] Preparation of Nanoporous Aggregated structure of ZnO nanoparticles by heating Zn(OH)_2 in a diol solution and their characterization2006

    • Author(s)
      N. Uekawa, S. Ishii, T. Kojima, K. Kakegawa
    • Organizer
      IUMRS-ICA-2006
    • Place of Presentation
      Korea
    • Year and Date
      2006-09-13
    • Related Report
      2008 Final Research Report

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Published: 2006-04-01   Modified: 2016-04-21  

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