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Mechanisms of strain-induced grain structure formation-Reconsideration of recrystallization

Research Project

Project/Area Number 18560689
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionThe University of Electro-Communications

Principal Investigator

SAKAI Taku  The University of Electro-Communications, Faculty of EC, Professor (40017364)

Project Period (FY) 2006 – 2007
Project Status Completed (Fiscal Year 2007)
Budget Amount *help
¥3,840,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥240,000)
Fiscal Year 2007: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2006: ¥2,800,000 (Direct Cost: ¥2,800,000)
KeywordsSevere plastic deformation / Multi-directional forging / Fine-grained structure / Microshear band / Kink band / Continuous dynamic recrystallization / Grain fragmentation / Anneasling / 温間,冷間加工 / ミクロシアバンド / 焼なまし / 連続再結晶
Research Abstract

The process and mechanisms of fine-grained structure formation during severe large deformation was studied in multi-Directional forging (MDF) and a single pass compression at low and high temperatures by using Cu and Al, Mg and Fe alloys. The relationships between deformation characteristics and evolution process of microstructures were systematically analyzed, and the main results obtained were summarized as follows.
1. Several kinds of deformation bands such as microshear and kink bands are generated in grain interiors in above a critical strain. The density and the misorientations of their boundaries increase with straining, leading to fragmentation of original grain interiors and finally formation of new fine-grains. The process of such strain-induced grain formation is concluded to be controlled by in-situ or continuous dynamic recrystallization.
2. Deformation bands are developed in various directions in three-dimensional space during MDF, leading to formation of fine-grained structures in large strain. This means that MDF is one of effective methods for fine-grained structure formation.
3. The process of new fine grain formation in a wide temperature interval can be classified into the three stages : (1) formation of conventional dislocation substructures accompanied with embryos of deformation bands (DBs) in stage 1 (ε<2) ; (2) development of large scale DBs followed by grain fragmentation, leading to new grain formation along DBs at moderate strains in stage 2 (2<ε<4) ; (3) development of new grained structures at high strains in stage 3 (ε>4).
4. Annealing of such strain-induced grain structure can not be controlled by conventional discontinuous recrystallization including nucleation and growth of new grains, but also by in-situ or continuous static recrystallization, in which grain growth takes place accompanied with recovery.

Report

(3 results)
  • 2007 Annual Research Report   Final Research Report Summary
  • 2006 Annual Research Report
  • Research Products

    (25 results)

All 2008 2007

All Journal Article (23 results) (of which Peer Reviewed: 4 results) Presentation (2 results)

  • [Journal Article] Mechanical Properties of Magnesium Alloy AZ31 after Sever Plastic Deformation2008

    • Author(s)
      J. Xing, X. Yang, H. Miura and T. Sakai
    • Journal Title

      Materials Transaction 49

      Pages: 69-75

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Grain refinement in aluminum alloy 2219 during ECAP at 250℃2008

    • Author(s)
      I.Mazurina, T., Sakai, H., Miura, 0., Sitdikov, R., Kaibyshev
    • Journal Title

      Mater. Sci. Eng. A 473

      Pages: 287-305

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Microstructural Behavior of Al-Mg-Sc Alloy Processed by ECAP at Elevated Temperatures2008

    • Author(s)
      O., Sitdikov, T., Sakai, E., Avtokratova, R., Kaibyshev, K., Tsuzaki, Y., Watanabe
    • Journal Title

      Acta Mater 56

      Pages: 821-834

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] 銅の冷間,高温加工中と加工後の連続・不連続再結晶(基調講演論文)2007

    • Author(s)
      酒井 拓
    • Journal Title

      銅と銅合金 46

      Pages: 1-6

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Ultra-Fine Grain Development in Copper during Multi-Directional forging at 195K2007

    • Author(s)
      C. Kobayashi, T. Sakai, A. Belyakov, X. Yang and H. Miura
    • Journal Title

      Phil. Mag. Letters 87

      Pages: 751-766

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Grain Refinement in a Commercial Al-Mg-Sc Alloy under Hot ECAP Conditions2007

    • Author(s)
      O., Sitdikov, T., Sakai, E., Avtokratova, R. Kaibyshev, Y., Kimra, K., Tsuzaki
    • Journal Title

      Mater. Sci. Engin. A 444

      Pages: 18-30

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Effect of Initial Grain Size and Strain Path on Grain Refinement in Magnesium Alloy AZ312007

    • Author(s)
      X., Yang, H., Miura, T., Sakai
    • Journal Title

      Materials Science Forum 539-543

      Pages: 1632-1637

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Microstructural Changes in As-Cast 7475 Al Alloy during Warm Severe Forging2007

    • Author(s)
      A., Goloborodko, T., Sakai, O., Sitdikov, H., Miura
    • Journal Title

      Materials Science Forum 539-543

      Pages: 2922-2927

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Microstructural Evolution and Recrystallization Behavior in Copper Multi-Directionally Forged at 77K2007

    • Author(s)
      Y., Nakao, H., Miura, T., Sakai
    • Journal Title

      Advanced Materials Research 15-17

      Pages: 649-654

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Stimulated Grain Refine-ment of Ni-Fe Alloy by Coarse Precipitates during Hot Multi-Directional Forging2007

    • Author(s)
      H., Miura, T., Sakai, T., Ueno, N., Fujita, Y., Yoshinaga
    • Journal Title

      Materials Science Forum 550

      Pages: 271-276

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Annealing of Deformed Materials Developed by Continuous/ Discontinuous Dynamic Recrystallization2007

    • Author(s)
      T., Sakai, H., Miura
    • Journal Title

      Materials Science Forum 550

      Pages: 327-332

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Effect of Defor-mation Temperature on Microstructure Evolution in 2219 Aluminum Alloy during ECAP2007

    • Author(s)
      I.Mazurina, O., Sitdikov, R. O., Kaibyshev, H., Miura, T., Sakai
    • Journal Title

      Materials Science Forum 558-559

      Pages: 545-550

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Microstructural Evolution in a Commercial Al-Mg-Sc Alloy during ECAP at 300C2007

    • Author(s)
      O., Sitdikov, T., Sakai, E., Avtokratova, R. Kaibyshev, T., Tsuzaki, Y., Watanabe
    • Journal Title

      Materials Science Forum 558-559

      Pages: 569-574

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Recrystallization Behavior of Ultra Fine-Grained Structure Induced by Mechanical Twinning in Cu-Zn Alloy2007

    • Author(s)
      Y., Nakao, H., Miura, T., Sakai
    • Journal Title

      Materials Science Forum 558-559

      Pages: 1329-1334

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Superplasticity of Magnesium Alloy AZ31 Processed by Multi-Directional Forging2007

    • Author(s)
      J., Xing, X.,. Yang, H., Miura, T., Sakai
    • Journal Title

      Mater. Trans 48

      Pages: 1406-1411

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] UltraFine Grain Development in Copper during Multidirectional forging at 195K2007

    • Author(s)
      C., Kobayashi, T., Sakai, A., Belyakov, H., Miura
    • Journal Title

      Phil. Mag. Letters 87

      Pages: 751-766

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Enhanced Grain Refinement Induced by Deformation Twining during Multi-Directional Forging of Cu and Cu-Zn Alloy2007

    • Author(s)
      H., Miura, H., Nakao, T., Sakai
    • Journal Title

      Trans Mater 48

      Pages: 2539-2541

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Microstructural Evolution at Grain Boundary in a Copper Bicrystal during Multi-Directional Forging2007

    • Author(s)
      H., Miura, Y., Yoshida, T., Sakai
    • Journal Title

      Voprosy Materialo Lovedenija (Problems of Materials Science) N4 52)

      Pages: 24-29

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary
  • [Journal Article] Ultra-Fine Grain Development in Copper during Multi-Directional forging at 195K2007

    • Author(s)
      C. Kobayashi, T. Sakai, A. Belakov, X. Yang and H. Miura
    • Journal Title

      Phil. Mag. Letters 87

      Pages: 751-766

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Stimulated Grain Refinement of Ni-Fe Alloy by Coarse Precipitates during Hot Multi-Directional Forging2007

    • Author(s)
      H.Miura, T.Sakai, T.Ueno, N.Fujita, Y.Yoshinaga
    • Journal Title

      Materials Science Forum 550

      Pages: 271-276

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Annealing of Deformed Materials Developed by Continuous/Discontinuous Dynamic Recrystallization2007

    • Author(s)
      T.Sakai, H.Miura
    • Journal Title

      Materials Science Forum 550

      Pages: 327-332

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Superplasticity of Magnesium Alloy AZ31 Processed by Multi-Directional Forging2007

    • Author(s)
      J.Xing, X.Yang, H.Miura, T.Sakai
    • Journal Title

      Materials Transactions 48(in press)

    • Related Report
      2006 Annual Research Report
  • [Journal Article] マグネシウム合金AZ31の多軸鍛造による大ひずみ加工と機械的特性2007

    • Author(s)
      刑 剋, 楊続躍, 三浦博己, 酒井拓
    • Journal Title

      塑性と加工 48(5)(in press)

    • Related Report
      2006 Annual Research Report
  • [Presentation] Ultrafine Grain Formation during Severe Plastic Deformation(Plenary invited)2007

    • Author(s)
      T. Sakai
    • Organizer
      The 5th International Conference on Physical and Numerical Simulation of Materials Processing
    • Place of Presentation
      Zhengzhou, China
    • Year and Date
      2007-10-23
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2007 Annual Research Report 2007 Final Research Report Summary
  • [Presentation] Ultrafine Grain Formation during Severe Plastic Deformation (Keynote invited)2007

    • Author(s)
      T., Sakai
    • Organizer
      A plenary lecture in the 5th International Conference on Physical and Numerical Simulation of Materials Processing (ICPNS'2007)
    • Place of Presentation
      Zhengzhou, China
    • Year and Date
      2007-10-06
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2007 Final Research Report Summary

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Published: 2006-04-01   Modified: 2016-04-21  

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