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Establishment of single grain boundary strength evaluation and atomistic mechanism investigation on grain boundary hydrogen embrittlement

Research Project

Project/Area Number 18H01344
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Review Section Basic Section 18010:Mechanics of materials and materials-related
Research InstitutionKansai University

Principal Investigator

TAKAHASHI Yoshimasa  関西大学, システム理工学部, 教授 (20611122)

Project Period (FY) 2018-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥13,130,000 (Direct Cost: ¥10,100,000、Indirect Cost: ¥3,030,000)
Fiscal Year 2020: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Fiscal Year 2019: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Fiscal Year 2018: ¥7,150,000 (Direct Cost: ¥5,500,000、Indirect Cost: ¥1,650,000)
Keywords水素脆性 / 結晶粒界 / 電子顕微鏡 / 強度評価 / 破壊 / 粒界
Outline of Final Research Achievements

The fracture along grain boundaries (GBs), which is frequently observed in high-strength poly-crystalline materials subjected to hydrogen environments, has been qualitatively attributed to the hydrogen embrittlement (HE) of the GBs. Is the GB-HE theory correct? Motivated by this fundamental question, a quantitative GB-HE measurement method using a micro-specimen containing a single GB is studied in detail. The key point of the study is the hard coating layer attached locally to the specimen surface. With this procedure, it is confirmed that the amount of plastic deformation before the onset of GB fracture is effectively reduced. Further, an in-situ STEM-EELS analysis of GB hydrogen using a nano electron probe is conducted under a hydrogen environment.

Academic Significance and Societal Importance of the Research Achievements

水素インフラの爆発的な普及は,水素による金属材料の脆化(水素脆性)に起因する不具合・事故案件の増大を必然的に招く.一方,水素脆性の基礎的研究は質・量の面においてまだまだ多くの余地がある.本課題で取り上げた多結晶材料中の結晶粒界における水素脆性もその典型例であり,詳細な破壊メカニズムを精密な実験により直接的に評価する,という試みは少ない.本研究の成果は,粒界そのものを対象とした破壊実験方法の確立や,粒界における水素の物理化学的解析手法の確立へ向けた大きな前進である.

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Annual Research Report
  • 2018 Annual Research Report
  • Research Products

    (17 results)

All 2020 2019 2018

All Journal Article (5 results) (of which Peer Reviewed: 5 results,  Open Access: 1 results) Presentation (12 results) (of which Int'l Joint Research: 3 results,  Invited: 1 results)

  • [Journal Article] Distinct fatigue limit of a 6XXX series aluminum alloy in relation to crack tip strain-aging2020

    • Author(s)
      Takahashi Yoshimasa、Kuriki Ryosuke、Kurihara Jun、Kozawa Tomoyuki、Shikama Takahiro、Noguchi Hiroshi
    • Journal Title

      Materials Science and Engineering: A

      Volume: 785 Pages: 139378-139378

    • DOI

      10.1016/j.msea.2020.139378

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Electron-microscopic analyses on high-temperature fatigue crack growth mechanism in a Ni-based single crystal superalloy2020

    • Author(s)
      Takahashi Yoshimasa、Kobayashi Daisuke、Kashihara Masaki、Kozawa Tomoyuki、Arai Shigeo
    • Journal Title

      Materials Science and Engineering: A

      Volume: 793 Pages: 139821-139821

    • DOI

      10.1016/j.msea.2020.139821

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Measurement of nanoscale local stress distribution in phase-separated glass using scanning transmission electron microscopy-cathodoluminescence2020

    • Author(s)
      Yamada Taiki、Ohtsuka Masahiro、Takahashi Yoshimasa、Yoshino Haruhiko、Amma Shin-ichi、Muto Shunsuke
    • Journal Title

      Materialia

      Volume: 9 Pages: 100578-100578

    • DOI

      10.1016/j.mtla.2019.100578

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] FE-SEM in situ Observation of Damage Evolution in Tension-compression Fatigue of Micro-sized Single-crystal Copper2019

    • Author(s)
      Takashi Sumigawa, Shin Uegaki, Tetsuya Yukishita, Shigeo Arai, Yoshimasa Takahashi, and Takayuki Kitamura
    • Journal Title

      Materials Science and Engineering A

      Volume: A764 Pages: 138218-138218

    • DOI

      10.1016/j.msea.2019.138218

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microscopic analysis of non-propagating fatigue crack tips2019

    • Author(s)
      Yukihiko Kimura, Yoshimasa Takahashi, Taizo Makino, Takanori Kato, Shigeo Arai
    • Journal Title

      International Journal of Fatigue

      Volume: 125 Pages: 122-127

    • DOI

      10.1016/j.ijfatigue.2019.03.043

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Presentation] Si/Cuマイクロ要素の界面剥離き裂発生強度則-界面端形状の影響-2020

    • Author(s)
      森井裕介,高橋可昌,宅間正則,齋藤賢一,佐藤知広
    • Organizer
      日本機械学会2020年度年次大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 7000系アルミニウム合金の高サイクル疲労特性に及ぼすMg添加の影響2020

    • Author(s)
      川端優典,高橋可昌,宅間正則,齋藤賢一,佐藤知広
    • Organizer
      日本機械学会2020年度年次大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Ni基超合金における高温クリープき裂先端の詳細観察2020

    • Author(s)
      小澤知之,高橋可昌,小林大輔
    • Organizer
      日本機械学会関西支部第96期定時総会講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Epoxy/SUS界面端からの時間依存型剥離き裂発生強度則の検討2020

    • Author(s)
      阪本和駿,高橋可昌,宅間正則,齋藤賢一,佐藤知広
    • Organizer
      日本機械学会関西支部第96期定時総会講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] STEM-CLによるナノ分相ガラスの局所応力分布測定2020

    • Author(s)
      武藤俊介,山田泰希,大塚正弘,高橋可昌,吉野晴彦,安間伸一
    • Organizer
      日本顕微鏡学会第76回学術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Direct observation of fatigue crack tips in a single-crystalline Ni-based superalloy2019

    • Author(s)
      Yoshimasa Takahashi, Daisuke Kobayashi, Masaki Kashihara, Tomohiro Kozawa, Shigeo Arai
    • Organizer
      International Conference on Materials and Systems for Sustainability (ICMaSS) 2019
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] その場ETEM/ナノインデント法を用いたマイクロ要素界面の剥離強度評価2019

    • Author(s)
      高橋可昌,岸本要,樋口公孝,山本悠太,荒井重勇,武藤俊介
    • Organizer
      日本顕微鏡学会第75回学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Al-Cu T4合金の高サイクル疲労強度特性に及ぼす温度の影響2019

    • Author(s)
      中野裕貴,辻田捷,高橋可昌,宅間正則,齋藤賢一,佐藤知広
    • Organizer
      日本機械学会M&M2019材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 小澤知之,高橋可昌,宅間正則,齋藤賢一,佐藤知広,野口博司,志鎌隆広2019

    • Author(s)
      ひずみ時効能を持つAl-Mg-Si 系合金の微小疲労き裂進展特性
    • Organizer
      日本機械学会M&M2019材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] マイクロ要素界面端からの剥離き裂発生強度評価における試験方法の検討2019

    • Author(s)
      岸本要,高橋可昌,宅間正則,齋藤賢一,佐藤知広
    • Organizer
      日本機械学会関西支部第94期定時総会講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Emergence of distinct fatigue limit: impact of excess solute magnesium in 6061-T6 alloy2018

    • Author(s)
      Yoshimasa Takahashi, Ryosuke Kuriki, Masaki Kashihara, Takahiro Shikama, Hiroshi Noguchi
    • Organizer
      The 22nd European Conference on Fracture (ECF22)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Evaluation of delamination strength of bonded micro-components: a nano-indenter technique combined with environmental microscopy2018

    • Author(s)
      Yoshimasa Takahashi, Kaname Kishimoto, Kimitaka Higuchi, Yuta Yamamoto,Shigeo Arai, Shunsuke Muto
    • Organizer
      29th International Symposium on Micro-Nano Mechatronics and Human Science
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited

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Published: 2018-04-23   Modified: 2022-01-27  

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