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Interface tailoring of eutectic composites for ultra-high temperature structural applications

Research Project

Project/Area Number 18H01735
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Review Section Basic Section 26040:Structural materials and functional materials-related
Research InstitutionKyoto University

Principal Investigator

Kishida Kyosuke  京都大学, 工学研究科, 准教授 (20354178)

Project Period (FY) 2018-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥17,420,000 (Direct Cost: ¥13,400,000、Indirect Cost: ¥4,020,000)
Fiscal Year 2020: ¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2019: ¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2018: ¥8,060,000 (Direct Cost: ¥6,200,000、Indirect Cost: ¥1,860,000)
Keywords界面特性制御 / 共晶複相材料 / 構造・機能材料 / 力学特性
Outline of Final Research Achievements

We have recently found a possibility to endow a new class of ultra-high temperature structural materials with high strength and high toughness simultaneously by utilizing interphase boundaries in directionally solidified in-situ eutectic composites. In the present study, we have systematically investigated microstructure - mechanical property relationship in various transition-metal silicide based eutectic composites in order to verify the strategy and to clarify the requirement for applying the strategy. In addition, deformation behaviors of various transition-metal silicides have been investigated by mechanical tests of micrometer-sized single crystals to
elucidate the deformation mechanism of the component phases in the eutectic composites.

Academic Significance and Societal Importance of the Research Achievements

本研究により脆性的な複数の構成相からなる超耐熱共晶合金の異相界面特性制御と組織微細さの制御により,高い高温強度特性と高い破壊靭性値の同時賦与が可能であることを明らかにしたとともに,これまで十分に解明されていなかった超高融点金属間化合物材料の塑性変形の基礎を明らかにしたことは学術的に非常に意義がある.また得られた成果は新規超高融点材料の実用化に向けた基礎としても重要であり,将来的な発電用ガスタービンをはじめとする熱機関の熱効率の向上と,それによる化石燃料の消費量ならびに温室効果ガスの排出量削減に大きく寄与することが期待されるため,社会的意義も高い.

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Annual Research Report
  • 2018 Annual Research Report
  • Research Products

    (49 results)

All 2021 2020 2019 2018 Other

All Journal Article (14 results) (of which Int'l Joint Research: 4 results,  Peer Reviewed: 13 results,  Open Access: 5 results) Presentation (30 results) (of which Int'l Joint Research: 11 results,  Invited: 11 results) Remarks (3 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Plastic deformation of single crystals of the equiatomic Cr-Mn-Fe-Co-Ni high-entropy alloy in tension and compression from 10 K to 1273 K2021

    • Author(s)
      Kawamura Marino、Asakura Makoto、Okamoto Norihiko L.、Kishida Kyosuke、Inui Haruyuki、George Easo P.
    • Journal Title

      Acta Materialia

      Volume: 203 Pages: 116454-116454

    • DOI

      10.1016/j.actamat.2020.10.073

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Comprehensive Phase Field Study on Directionally-Solidified MoSi2/Mo5Si3Eutectic Alloy2021

    • Author(s)
      Zhu Chuan Qi、Yamamoto Jimpei、Koizumi Yuichiro、Yuge Koretaka、Kishida Kyosuke、Inui Haruyuki
    • Journal Title

      Materials Science Forum

      Volume: 1016 Pages: 749-754

    • DOI

      10.4028/www.scientific.net/msf.1016.749

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Plastic deformation of single crystals of CrB2, TiB2 and ZrB2 with the hexagonal AlB2 structure2021

    • Author(s)
      Paul Bhaskar、Okamoto Norihiko L.、Kusakari Misato、Chen Zhenghao、Kishida Kyosuke、Inui Haruyuki、Otani Shigeki
    • Journal Title

      Acta Materialia

      Volume: 211 Pages: 116857-116857

    • DOI

      10.1016/j.actamat.2021.116857

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Experimental evaluation of critical resolved shear stress for the first-order pyramidal c+a slip in commercially pure Ti by micropillar compression method2020

    • Author(s)
      K. Kishida, J. Kim, T. Nagae, H. Inui
    • Journal Title

      Acta Materialia

      Volume: 96 Pages: 168-174

    • DOI

      10.1016/j.actamat.2020.06.043

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Room temperature deformation of single crystals of Ti5Si3 with the hexagonal D88 structure investigated by micropillar compression tests2020

    • Author(s)
      Kishida Kyosuke、Fukuyama Takayoshi、Maruyama Takuto、Inui Haruyuki
    • Journal Title

      Scientific Reports

      Volume: 10 Issue: 1 Pages: 17983-17983

    • DOI

      10.1038/s41598-020-75007-7

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Micropillar compression deformation of single crystals of α-Nb5Si3 with the tetragonal D8l structure2020

    • Author(s)
      Kishida Kyosuke、Maruyama Takuto、Fukuyama Takayoshi、Inui Haruyuki
    • Journal Title

      Science and Technology of Advanced Materials

      Volume: 21 Issue: 1 Pages: 805-816

    • DOI

      10.1080/14686996.2020.1855065

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] MoSi2基Brittle/Brittle複相単結晶超耐熱材料の開発2020

    • Author(s)
      岸田恭輔、乾晴行
    • Journal Title

      金属

      Volume: 90 Pages: 556-562

    • Related Report
      2020 Annual Research Report
  • [Journal Article] Pattern formation mechanism of directionally-solidified MoSi2/Mo5Si3 eutectic by phase-field simulation2020

    • Author(s)
      Zhu Chuanqi、Koizumi Yuichiro、Chiba Akihiko、Yuge Koretaka、Kishida Kyosuke、Inui Haruyuki
    • Journal Title

      Intermetallics

      Volume: 116 Pages: 106590-106590

    • DOI

      10.1016/j.intermet.2019.106590

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Room temperature deformation of 6H-SiC single crystals investigated by micropillar compression2020

    • Author(s)
      Kishida Kyosuke、Shinkai Yasuharu、Inui Haruyuki
    • Journal Title

      Acta Materialia

      Volume: 187 Pages: 19-28

    • DOI

      10.1016/j.actamat.2020.01.027

    • NAID

      120006796464

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Strategy for managing both high strength and large ductility in structural materials-sequential nucleation of different deformation modes based on a concept of plaston2020

    • Author(s)
      Tsuji Nobuhiro、Ogata Shigenobu、Inui Haruyuki、Tanaka Isao、Kishida Kyosuke、Gao Si、Mao Wenqi、Bai Yu、Zheng Ruixiao、Du Jun-Ping
    • Journal Title

      Scripta Materialia

      Volume: 181 Pages: 35-42

    • DOI

      10.1016/j.scriptamat.2020.02.001

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructure and mechanical properties of a MoSi2-Mo5Si3 eutectic composite processed by laser surface melting2019

    • Author(s)
      Vega Farje Juan A.、Matsunoshita Hirotaka、Kishida Kyosuke、Inui Haruyuki
    • Journal Title

      Materials Characterization

      Volume: 148 Pages: 162-170

    • DOI

      10.1016/j.matchar.2018.12.016

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Anisotropic plastic deformation of single crystals of the MAX phase compound Ti3SiC2 investigated by micropillar compression2018

    • Author(s)
      Higashi Masaya、Momono Shogo、Kishida Kyosuke、Okamoto Norihiko L.、Inui Haruyuki
    • Journal Title

      Acta Materialia

      Volume: 161 Pages: 161-170

    • DOI

      10.1016/j.actamat.2018.09.024

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] On the influence of crystallography and dendritic microstructure on micro shear behavior of single crystal Ni-based superalloys2018

    • Author(s)
      Laplanche G.、Wieczorek N.、Fox F.、Berglund S.、Pfetzing-Micklich J.、Kishida K.、Inui H.、Eggeler G.
    • Journal Title

      Acta Materialia

      Volume: 160 Pages: 173-184

    • DOI

      10.1016/j.actamat.2018.08.052

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Micropillar compression deformation of single crystals of Mo5SiB2 with the tetragonal D8 structure2018

    • Author(s)
      Kishida Kyosuke、Maruyama Takuto、Matsunoshita Hirotaka、Fukuyama Takayoshi、Inui Haruyuki
    • Journal Title

      Acta Materialia

      Volume: 159 Pages: 416-428

    • DOI

      10.1016/j.actamat.2018.08.048

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Presentation] 6H-SiC単結晶の室温塑性変形挙動2021

    • Author(s)
      岸田恭輔, 乾 晴行
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Mo添加NbSi2/Nb5Si3共晶合金の微細組織と力学特性2021

    • Author(s)
      上村 遙, 岸田 恭輔, 乾 晴行
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Micropillar compression deformation of transition-metal disilicides with the C11b and C40 structures2021

    • Author(s)
      Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Thermec’2021
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] D8l型構造を有する遷移金属シリサイド単結晶の室温変形挙動2020

    • Author(s)
      岸田 恭輔,乾 晴行
    • Organizer
      日本金属学会2020年秋期(第167回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Mo添加NbSi2/Nb5Si3一方向凝固共晶合金の微細組織2020

    • Author(s)
      上村 遥,岸田 恭輔,乾 晴行
    • Organizer
      日本金属学会2020年秋期(第167回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Micropillar Compression Deformation of Transition-Metal Disilicides with the C40 Structure2020

    • Author(s)
      Kyosuke Kishida, Haruyuki Inui
    • Organizer
      2020 MRS Virtual Spring/Fall Meeting & Exhibit
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Microstructure and Crystallographic Orientation Relationships in Directionally Solidified NbSi2/Nb5Si3 Eutectic Composites with Mo Addition2020

    • Author(s)
      Haruka Uemura, Kosei Takeda, Kyosuke Kishida, Haruyuki Inui
    • Organizer
      2020 MRS Virtual Spring/Fall Meeting & Exhibit
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 遷移金属ダイシリサイド単結晶のマイクロピラー圧縮変形2020

    • Author(s)
      岸田 恭輔、乾 晴行
    • Organizer
      日本金属学会2020年春期(第166回)講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Mo添加NbSi2/Nb5Si3共晶合金の微細組織と力学特性2020

    • Author(s)
      上村 遙、武田 康誠、岸田 恭輔、乾 晴行
    • Organizer
      日本金属学会2020年春期(第166回)講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] フェーズフィールド法によるMoSi2基複相超高温耐熱構造材料における組織形成メカニズムの研究2020

    • Author(s)
      山本陣平,小泉雄一郎,弓削是貴,岸田恭輔,乾晴行, 朱 伝奇、奥川将行
    • Organizer
      日本金属学会2020年春期(第166回)講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Development of MoSi2/Mo5Si3-based in-situ composites for ultra-high temperature applications2019

    • Author(s)
      Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Beyond Nickel-Based Superalloys III
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Pattern Formation Mechanism of Script Lamellar Pattern in MoSi2/Mo5Si3 Eutectic Examined by Phase Field Method2019

    • Author(s)
      Chuanqi Zhu,Yuichiro Koizumi, Akihiko Chiba, Koretaka Yuge, Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Beyond Nickel-Based Superalloys III
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Influences of growth conditions on microstructures and mechanical properties of directionally solidified MoSi2/Mo5Si3-based eutectic composites2019

    • Author(s)
      Kosei Takeda, Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Beyond Nickel-Based Superalloys III
    • Related Report
      2019 Annual Research Report
  • [Presentation] Phase-field simulation of directional solidification in MoSi2/Mo5Si3 eutectic alloy with elastic anisotropy2019

    • Author(s)
      Jimpei Yamamoto, Yuichiro Koizumi, Koretaka Yuge, Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Beyond Nickel-Based Superalloys III
    • Related Report
      2019 Annual Research Report
  • [Presentation] 単結晶マイクロピラー圧縮試験で探る層状化合物の塑性変形機構2019

    • Author(s)
      岸田恭輔
    • Organizer
      日本金属学会2019年秋期(第165回)講演大会
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] MoSi2/Mo5Si3共晶一方向凝固材の微細組織と力学特性に及ぼす凝固条件の影響2019

    • Author(s)
      武田康誠、岸田恭輔、乾晴行
    • Organizer
      日本金属学会2019年秋期(第165回)講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Room-temperature deformaton behavior of D8l-type transiton-metal silicides investgated by micropillar compression2019

    • Author(s)
      Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Intermetallics 2019
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Microstructure optmisaton of directonally solidifed MoSi2/Mo5si3 eutectc composites2019

    • Author(s)
      Kosei Takeda, Kyosuke Kishida, Haruyuki Inui
    • Organizer
      Intermetallics 2019
    • Related Report
      2019 Annual Research Report
  • [Presentation] Room Temperature Deformation Behavior of Hard Intermetallic Compounds Investigated by Micropillar Compression Method2019

    • Author(s)
      Kyosuke KISHIDA, Haruyuki INUI
    • Organizer
      MATERIALS RESEARCH MEETING 2019(MRM 2019)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] MoSi2/Mo5Si3/Mo5Si3C三相共晶合金の微細組織と力学特性に及ぼすTaおよびNb添加の影響2019

    • Author(s)
      武田康誠,神原佑季,松野下裕貴,岸田恭輔,乾晴行
    • Organizer
      社団法人日本鉄鋼協会・公益社団法人日本金属学会 関西支部 材料物性工学談話会平成30年度第2回講演会ならびにポスター発表会
    • Related Report
      2018 Annual Research Report
  • [Presentation] MoSi2/Mo5Si3共晶一方向合金の微細組織と力学特性に及ぼす結晶育成条件の影響2019

    • Author(s)
      武田康誠,岸田恭輔,乾晴行,出村雅彦
    • Organizer
      日本金属学会2019年春期(第164回)講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 層状結晶構造を有する金属間化合物の結晶構造と塑性変形2018

    • Author(s)
      岸田恭輔
    • Organizer
      東京大学大学院工学系研究科マテリアル工学専攻マテリアル工学セミナー「構造材料の新展開」
    • Related Report
      2018 Annual Research Report
    • Invited
  • [Presentation] Influences of ternary and quaternary additions on mechanical properties of MoSi2/Mo5Si3-based in-situ composites2018

    • Author(s)
      Kyosuke Kishida, Yuki Kambara, Haruyuki Inui
    • Organizer
      THERMEC’2018 International Conference on Processing & Manufacturing of Advanced Materials
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] マイクロピラー圧縮試験法を用いた塑性変形研究の最前線2018

    • Author(s)
      岸田恭輔
    • Organizer
      日本金属学会2018年秋期(第163回)講演大会
    • Related Report
      2018 Annual Research Report
    • Invited
  • [Presentation] MoSi2基共晶一方向凝固合金の組織と力学特性に及ぼす添加元素の影響2018

    • Author(s)
      武田康誠, 神原佑季,松野下裕貴,岸田恭輔,乾 晴行
    • Organizer
      日本金属学会2018年秋期(第163回)講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] TM5Si3型遷移金属シリサイドの室温変形挙動2018

    • Author(s)
      福山貴義,丸山拓仁,岸田恭輔,乾 晴行
    • Organizer
      日本金属学会2018年秋期(第163回)講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Plastic deformation of layered compounds studied by micropillar compression and scanning electron microscopy2018

    • Author(s)
      K. Kishida, H. Inui
    • Organizer
      International symposium on Atomistic Processes of Crystal Plasticity
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] マイクロピラー圧縮試験による結晶性材料の変形機構解析2018

    • Author(s)
      岸田恭輔, 乾 晴行
    • Organizer
      日本材料学会第67期第1回マルチスケール材料力学部門委員会
    • Related Report
      2018 Annual Research Report
    • Invited
  • [Presentation] Room temperature deformation of transition-metal silicides investigated by micropillar compression method2018

    • Author(s)
      K. Kishida, H. Inui
    • Organizer
      MRS 2018 Fall Meeting & Exhibit
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Effects of Ta and Nb Addition on the Microstructure and Mechanical Properties of MoSi2/Mo5Si3/Mo5Si3C Eutectic Composites2018

    • Author(s)
      Kosei Takeda, Yuki Kambara, Hirokata Matunoshita, Kyosuke Kishida, Haruyuki Inui
    • Organizer
      MRS 2018 Fall Meeting & Exhibit
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Remarks] 京都大学大学院工学研究科材料工学専攻 乾 研究室のページ

    • URL

      http://imc.mtl.kyoto-u.ac.jp/

    • Related Report
      2020 Annual Research Report 2019 Annual Research Report
  • [Remarks] Researchgate

    • URL

      https://www.researchgate.net/profile/Kyosuke_Kishida

    • Related Report
      2019 Annual Research Report
  • [Remarks] 京都大学大学院工学研究科材料工学専攻 乾 研究室

    • URL

      http://imc.mtl.kyoto-u.ac.jp/

    • Related Report
      2018 Annual Research Report
  • [Patent(Industrial Property Rights)] 金属積層成形体及びその製造方法2019

    • Inventor(s)
      乾 晴行,岸田恭輔,小岩井修二
    • Industrial Property Rights Holder
      乾 晴行,岸田恭輔,小岩井修二
    • Industrial Property Rights Type
      特許
    • Filing Date
      2019
    • Related Report
      2019 Annual Research Report
  • [Patent(Industrial Property Rights)] 金属積層成形体及びその製造方法2018

    • Inventor(s)
      乾 晴行,岸田恭輔,小岩井修二
    • Industrial Property Rights Holder
      乾 晴行,岸田恭輔,小岩井修二
    • Industrial Property Rights Type
      特許
    • Filing Date
      2018
    • Related Report
      2018 Annual Research Report

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Published: 2018-04-23   Modified: 2022-01-27  

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