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Interfacial control of Co-based superalloy for new forging process

Research Project

Project/Area Number 18H01742
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionTohoku University

Principal Investigator

Oikawa Katsunari  東北大学, 工学研究科, 教授 (70356608)

Co-Investigator(Kenkyū-buntansha) 上島 伸文  東北大学, 工学研究科, 助教 (10733131)
Project Period (FY) 2018-04-01 – 2023-03-31
Project Status Completed (Fiscal Year 2022)
Budget Amount *help
¥17,810,000 (Direct Cost: ¥13,700,000、Indirect Cost: ¥4,110,000)
Fiscal Year 2022: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2021: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2020: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2019: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2018: ¥11,050,000 (Direct Cost: ¥8,500,000、Indirect Cost: ¥2,550,000)
Keywords熱間加工 / 超合金 / 動的再結晶 / ミクロ組織 / 析出強化 / Co基超合金 / 熱間鍛造 / 鍛造 / 再結晶 / 析出 / Co -Al-W / 組織制御 / シミュレーション / 粒成長 / Co基合金 / 塑性加工 / ミクロ組織制御
Outline of Final Research Achievements

The effect of microstructure on the hot workability of Co-based superalloys, which are expected as new heat-resistant alloys, was investigated. We prepared samples in which different size of the γ' phase particles was precipitated for the hot compression. The smaller the γ' phase particles, the smaller the compressive load in Co-Al-W-based alloys, and the larger the γ' phase particles, the smaller the compressive load in Co-Al-W-Ni-Ti-Ta-B alloys. This suggests that the precipitation strengthening mechanism varies with the alloy system. The size of the residual γ' phase particles after compression was became significantly larger. This suggest that the γ' phase particles grow during the forging process. It is also clear that the γ' phase particles became incoherent with the matrix phase.

Academic Significance and Societal Importance of the Research Achievements

Co基超合金は,次世代の耐熱合金として期待されている.強化粒子であるγ'相が析出しているときの,熱間変形挙動やその後のミクロ組織変化については,殆ど研究されてこなかった.本研究では,母相粒径やγ'相粒子サイズが加工荷重に大きな影響があることを明らかにし,かつ,加工中に析出粒子が粗大化し非整合化することを見出している.以上の知見は,最適加工条件を明らかにすること役立つ.

Report

(6 results)
  • 2022 Annual Research Report   Final Research Report ( PDF )
  • 2021 Annual Research Report
  • 2020 Annual Research Report
  • 2019 Annual Research Report
  • 2018 Annual Research Report
  • Research Products

    (37 results)

All 2022 2021 2020 2019 Other

All Journal Article (8 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 8 results,  Open Access: 1 results) Presentation (28 results) (of which Int'l Joint Research: 6 results,  Invited: 3 results) Remarks (1 results)

  • [Journal Article] Thermodynamic and atomic mobility assessment of the Co-Fe-Mn system2022

    • Author(s)
      Pendem Sri Pragna、Ueshima Nobufumi、Oikawa Katsunari、Tsukada Yuhki、Koyama Toshiyuki
    • Journal Title

      Journal of Materials Science

      Volume: 57 Issue: 33 Pages: 15999-16015

    • DOI

      10.1007/s10853-022-07612-y

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Experimental Investigation and Thermodynamic Assessment of Ni-B and Ni-B-C Systems2022

    • Author(s)
      Oikawa Katsunari、Ueshima Nobufumi
    • Journal Title

      Journal of Phase Equilibria and Diffusion

      Volume: 43 Issue: 6 Pages: 814-826

    • DOI

      10.1007/s11669-022-00995-0

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Investigations on the Phase Transformations, Equilibria and Athermal ω in Ni-Ga-Cr Ternary System2022

    • Author(s)
      Ruan Jingjing、Chen Yuyuan、Kobayashi Kosei、Ueshima Nobufumi、Oikawa Katsunari
    • Journal Title

      Materials

      Volume: 15 Issue: 21 Pages: 7617-7617

    • DOI

      10.3390/ma15217617

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Phase equilibria, martensitic transformations and deformation behaviors of the subsystem of Cantor alloy?low-cost Fe-Mn-Cr alloys2021

    • Author(s)
      Ruan Jingjing、Ueshima Nobufumi、Li Haoge、Oikawa Katsunari
    • Journal Title

      Materialia

      Volume: 20 Pages: 101231-101231

    • DOI

      10.1016/j.mtla.2021.101231

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Investigation on the σ-phase-related equilibria in Cr-Mn-Co system2021

    • Author(s)
      Li Haoge、Ruan Jingjing、Ueshima Nobufumi、Oikawa Katsunari
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 867 Pages: 159024-159024

    • DOI

      10.1016/j.jallcom.2021.159024

    • Related Report
      2021 Annual Research Report 2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Experimental investigations of fcc/bcc phase equilibria in the Cr-Mn-Ni ternary system2020

    • Author(s)
      Li Haoge、Ruan Jingjing、Ueshima Nobufumi、Oikawa Katsunari
    • Journal Title

      Intermetallics

      Volume: 127 Pages: 106994-106994

    • DOI

      10.1016/j.intermet.2020.106994

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Generation and Progress Behavior of Strain-Induced Abnormally Large Grains in Superalloy 7182020

    • Author(s)
      Aoki Chuya、Date Masayoshi、Ueno Tomonori、Ohno Takehiro、Oikawa Katsunari
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 51 Issue: 8 Pages: 4022-4032

    • DOI

      10.1007/s11661-020-05838-6

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Growth behavior of the δ-Ni3Nb phase in superalloy 718 and modified KJMA modeling for the transformation-time-temperature diagram2020

    • Author(s)
      Ruan J.J.、Ueshima N.、Oikawa K.
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 814 Pages: 152289-152289

    • DOI

      10.1016/j.jallcom.2019.152289

    • Related Report
      2020 Annual Research Report 2019 Annual Research Report
    • Peer Reviewed
  • [Presentation] Atomic mobility assessment in ternary fcc Co-Cr-Mn system2022

    • Author(s)
      S.P. Pendem, N. Ueshima, K. Oikawa
    • Organizer
      MS&T2022
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Kinetic and thermodynamic assessment in ternary fcc Co-Cr-Mn alloy2022

    • Author(s)
      S. P. Pendem, N. Ueshima, K. Oikawa, Y. Tsukada, T. Koyama
    • Organizer
      日本金属学会2022年秋期(第171回)講演大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] CrMnFeCoNi合金系の熱力学データベース構築2022

    • Author(s)
      及川勝成、上島伸文
    • Organizer
      日本金属学会2022年秋期(第171回)講演大会
    • Related Report
      2022 Annual Research Report
    • Invited
  • [Presentation] Fe-Mn-Ni系合金における相互拡散係数の決定2022

    • Author(s)
      庄子智明、上島伸文、及川勝成
    • Organizer
      日本金属学会2022年秋期(第171回)講演大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] Co-Mn-Ni系合金の相互拡散係数の決定2022

    • Author(s)
      宮崎紘平、上島伸文、及川勝成
    • Organizer
      日本金属学会2022年秋期(第171回)講演大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] Determination of Mobility parameters in FCC Co-Fe-Mn Ternary System2022

    • Author(s)
      P. S. Pragna, N. Ueshima, K. Oikawa, T. Koyama, Y. Tsukada
    • Organizer
      日本金属学会2022年春期(第170回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Cr-MnおよびCr-Mn-Co系の熱力学的解析2022

    • Author(s)
      李 浩歌、上島伸文、〇及川 勝成、韓 光植、阿部 太一、大沼 郁雄
    • Organizer
      日本金属学会2022年春期(第170回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Phase equilibria and Diffusion kinetics in Fe-Co-Mn ternary system2021

    • Author(s)
      S.P. Pendem, N. Ueshima, K. Oikawa
    • Organizer
      MRM2021
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Phase equilibria of the subsystem of Cantor alloy-Cr-Co-Mn alloys2021

    • Author(s)
      H.G. Li, N. Ueshima, K. Oikawa
    • Organizer
      MRM2021
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Development of a prediction model and process-microstructure-property database on forging and heat treatment of superalloy 720Li2021

    • Author(s)
      N.Ueshima, C. Aoki, T. Osada, S. Horikoshi, A. Yanagida, H. Murakami, T. Ishida, Y. Yamabe-Mitarai, K. Oikawa, N. Yukawa, J. Yanagimoto
    • Organizer
      The 14th International Symposium on Superalloys (Superalloys 2021)
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Grain growth behavior and dissolution behavior of δ-phase near solvus temperature of superalloy 7182021

    • Author(s)
      K. Oikawa, N. Ueshima, J. J. Ruan
    • Organizer
      Thermec’2021
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Interdiffusion in Co-Fe-Mn alloys2021

    • Author(s)
      スリ プラグナ ペンデム、上島伸文、及川勝成
    • Organizer
      粉体粉末冶金協会2021年度秋季大会(第128回講演大会)
    • Related Report
      2021 Annual Research Report
  • [Presentation] Alloy 720Liの熱間圧縮における動的再結晶と流動応力の内部変数モデルの構築2021

    • Author(s)
      中村丞、上島伸文、及川勝成
    • Organizer
      第72回塑性加工連合講演会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Cr-Mn系とCr-Mn-Co系状態図の熱力学アセスメント2021

    • Author(s)
      李浩歌、上島伸文、及川勝成
    • Organizer
      日本金属学会2021年秋期(第169回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] γ'相の影響を考慮したAlloy720Liの流動応力モデリング2021

    • Author(s)
      中村丞、上島伸文、及川勝成
    • Organizer
      日本金属学会2021年秋期(第169回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Diffusion Kinetics in Ternary Co-Fe-Mn Alloy2021

    • Author(s)
      スリ プラグナ ペンデム、上島伸文、及川勝成
    • Organizer
      日本金属学会2021年秋期(第169回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Ni-Nb二元系及びNi-Cr-Nb三元系合金の実験状態図2021

    • Author(s)
      三川陸、荻野勇人、上島伸文、及川勝成
    • Organizer
      日本金属学会2021年秋期(第169回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Experimental investigations on Cr-Co-Mn ternary phase diagram2020

    • Author(s)
      H. G. Li, N. Ueshima, K. Oikawa,
    • Organizer
      日本金属学会2020年秋期(第167回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Phase equilibria in Mn rich corner in Mn Fe Cr ternary system2020

    • Author(s)
      J. J. Ruan, N. Ueshima, K. Oikawa
    • Organizer
      日本金属学会2020年秋期(第167回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Internal State Variablesモデルを用いたAlloy 720Liの流動応力モデリング2020

    • Author(s)
      中村丞、 上島 伸文、及川 勝成
    • Organizer
      日本鉄鋼協会第180回秋季講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 転位密度ベースモデルを用いたAlloy 720Liの流動応力モデリング2020

    • Author(s)
      中村丞、上島伸文、及川勝成
    • Organizer
      日本塑性加工学会第71回塑性加工連合講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Co基超合金の熱間鍛造によるγ’相の析出形態への影響2020

    • Author(s)
      廣川大樹, 上島伸文, 及川勝成
    • Organizer
      第19回 日本金属学会東北支部研究発表大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Phase Equilibria in Ternary Fe-Co-Mn System at 900℃2020

    • Author(s)
      Sri Pragna Pendem, N. Ueshima, K. Oikawa
    • Organizer
      第19回 日本金属学会東北支部研究発表大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Investigation and thermodynamic assessment on the σ-phase-related equilibria in Cr-Mn-Co system2020

    • Author(s)
      H. G. Li, N. Ueshima、K. Oikawa
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Phase equilibria and diffusion kinetics in Fe-Co-Mn ternary system2020

    • Author(s)
      S. P. Pendem, N. Ueshima、K. Oikawa
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Microstructure evolution during dynamic recrystallization and meta-dynamic recrystallization in superalloy7182019

    • Author(s)
      N. Ueshima, D.X. Wen, J.J. Ruan, K. Oikawa
    • Organizer
      FiMPART'19
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Ni基超合金の加工組織モデリングと予測2019

    • Author(s)
      上島伸文,J.J. Ruan, 温東旭,及川勝成
    • Organizer
      日本金属学会第165回講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 時効熱処理中のCo-9Al-10Wのγ'相成長挙動2019

    • Author(s)
      廣川大樹,上島伸文,及川勝成
    • Organizer
      日本金属学会第165回講演大会
    • Related Report
      2019 Annual Research Report
  • [Remarks] http://www.material.tohoku.ac.jp/~koso/lab.html

    • Related Report
      2022 Annual Research Report

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Published: 2018-04-23   Modified: 2024-01-30  

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