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Fatigue of nano-metals

Research Project

Project/Area Number 18H03753
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Review Section Medium-sized Section 18:Mechanics of materials, production engineering, design engineering, and related fields
Research InstitutionKyoto University

Principal Investigator

Sumigawa Takashi  京都大学, エネルギー科学研究科, 教授 (80403989)

Co-Investigator(Kenkyū-buntansha) 中村 篤智  名古屋大学, 工学研究科, 准教授 (20419675)
嶋田 隆広  京都大学, 工学研究科, 准教授 (20534259)
Project Period (FY) 2018-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥45,500,000 (Direct Cost: ¥35,000,000、Indirect Cost: ¥10,500,000)
Fiscal Year 2020: ¥8,190,000 (Direct Cost: ¥6,300,000、Indirect Cost: ¥1,890,000)
Fiscal Year 2019: ¥10,140,000 (Direct Cost: ¥7,800,000、Indirect Cost: ¥2,340,000)
Fiscal Year 2018: ¥27,170,000 (Direct Cost: ¥20,900,000、Indirect Cost: ¥6,270,000)
KeywordsFatigue / Micro-sized metals / Tension-compression / In situ observation / Single crystal / ナノ疲労 / 引張圧縮疲労試験 / その場観察 / 電子顕微鏡 / 転位構造 / 電視顕微鏡
Outline of Final Research Achievements

The purpose of this study is to investigate the mechanism of tension-compression fatigue in micro- to nano-sized pure metals. In micro-sized single-crystal copper (Cu) specimens, it was confirmed that the extrusions/intrusions grew with the increase in the number of cycles and that fatigue cracks appeared at the bottom of the intrusion. On the other hand, cyclic work hardening did not occur, and the appearance of the extrusions/intrusions was different from that of Cu bulk counterpart. Low stress amplitude tests using micro-sized single-crystal nickel (Ni) specimens showed that fatigue damage occurred even below the fatigue limit of the bulk. Experiments on specimens with different dimensions showed that the fatigue behavior changed with the change in material dimensions. Transmission electron microscopy revealed that the internal dislocation structure was strongly influenced by the surfaces of material.

Academic Significance and Societal Importance of the Research Achievements

各種半導体デバイスの内部には、ナノ~マイクロサイズの金属素子が多数存在する。これらのデバイスは、近年では自動車等の厳しい環境下で使用されるようになり、内部の金属素子の疲労破壊が問題となっている。ナノ~マイクロサイズの金属では、疲労破壊の発生原因とされる下部組織の寸法の観点から従来の金属疲労とは異なる挙動を示すことが予測されるが、その学理自体が存在しなかった。本研究では、その学理の基礎基盤の礎を構築することに成功しており、学術的意義や社会的意義は極めて大きい。

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Annual Research Report
  • 2018 Annual Research Report
  • Research Products

    (49 results)

All 2021 2020 2019 2018 2017 Other

All Int'l Joint Research (4 results) Journal Article (25 results) (of which Int'l Joint Research: 17 results,  Peer Reviewed: 25 results,  Open Access: 2 results) Presentation (19 results) (of which Int'l Joint Research: 3 results,  Invited: 8 results) Remarks (1 results)

  • [Int'l Joint Research] ハルピン工業大学/浙江大学(中国)

    • Related Report
      2020 Annual Research Report
  • [Int'l Joint Research] ハルピン工業大学/浙江大学/天津大学(中国)

    • Related Report
      2018 Annual Research Report
  • [Int'l Joint Research] ノルウェー科学技術大学(ノルウェー)

    • Related Report
      2018 Annual Research Report
  • [Int'l Joint Research] アールト大学(フィンランド)

    • Related Report
      2018 Annual Research Report
  • [Journal Article] Experimental evaluation of loading mode effect on plasticity of microscale single-crystal copper2021

    • Author(s)
      Kai Huang, Takashi Sumigawa, Takayuki Kitamura
    • Journal Title

      Materials Science and Engineering: A

      Volume: 806 Pages: 140822-140822

    • DOI

      10.1016/j.msea.2021.140822

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Fatigue curve of microscale single-crystal copper: An in situ SEM tension-compression study2020

    • Author(s)
      Yabin Yan, Takashi Sumigawa, Xiaoyuan Wang, Wufan Chen, Fuzhen Xuan, Takayuki Kitamura
    • Journal Title

      International Journal of Mechanical Sciences

      Volume: 71 Pages: 105361-105361

    • DOI

      10.1016/j.ijmecsci.2019.105361

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Notch sensitivity of metamaterial with snapping microstructure2020

    • Author(s)
      日笠 健,澄川 貴志,田中 秀平,金子 遼太,北村 隆行
    • Journal Title

      Transactions of the JSME (in Japanese)

      Volume: 86 Issue: 886 Pages: 19-00398-19-00398

    • DOI

      10.1299/transjsme.19-00398

    • NAID

      130007864396

    • ISSN
      2187-9761
    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] In-Situ TEM Observation of Nanodomain Mechanics in Barium Titanate under External Loads2020

    • Author(s)
      Takashi Sumigawa, Ken Hikasa, Akihiro Kusunose, Hiroki Unno, Kairi Masuda, Takahiro Shimada, and Takayuki Kitamura
    • Journal Title

      Physical Review Materials

      Volume: 4 Issue: 5 Pages: 054415-054415

    • DOI

      10.1103/physrevmaterials.4.054415

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A Quantitative In Situ SEM Bending Method for Stress Relaxation of Microscale Materials at Room Temperature2020

    • Author(s)
      Yabin Yan, Wufan Chen, Takashi Sumigawa, Xiaoyuan Wang, Takayuki Kitamura, Fuzhen Xuan
    • Journal Title

      Experimental Mechanics

      Volume: 60 Issue: 7 Pages: 937-947

    • DOI

      10.1007/s11340-020-00611-7

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] An experimental study on atomic-level unified criterion for brittle fracture2020

    • Author(s)
      Kai Huang, Takashi Sumigawa, Takahiro Shimada, Shuhei Tanaka, Youhei Hagiwara, Licheng Guo, Takayuki Kitamura
    • Journal Title

      International Journal of Solids and Structures

      Volume: 206 Pages: 1-8

    • DOI

      10.1016/j.ijsolstr.2020.08.006

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Nonlinear Elasticity in Meta-Film Comprising of Nano-Helices2020

    • Author(s)
      Ryota Kaneko, Tetsuya Yukishita, Takashi Sumigawa, Takayuki Kitamura
    • Journal Title

      Thin Solid Films

      Volume: 695 Pages: 137749-137749

    • DOI

      10.1016/j.tsf.2019.137749

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Load-dependence of Damage Process in Tension-compression Fatigue of Microscale Single-crystal Copper2020

    • Author(s)
      Kai Huang, Takashi Sumigawa, Takayuki Kitamura
    • Journal Title

      International Journal of Fatigue

      Volume: 133 Pages: 105415-105415

    • DOI

      10.1016/j.ijfatigue.2019.105415

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Contact Area Measurement of Micron-sized Metal-coated Polymer Particles under Compression2020

    • Author(s)
      Molly Bazilchuk, Takashi Sumigawa, Takayuki Kitamura, Zhiliang Zhang, Helge Kristiansen, Jianying He
    • Journal Title

      nternational Journal of Mechanical Sciences

      Volume: 165 Pages: 105214-105214

    • DOI

      10.1016/j.ijmecsci.2019.105214

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Outstanding Property in Fatigue Strength of Thin Film Comprising of Copper Helical Nano-Elements Grown by Glancing Angle Deposition2019

    • Author(s)
      金子遼太,山本幹也,澄川貴志,北村隆行
    • Journal Title

      Journal of the Society of Materials Science, Japan

      Volume: 68 Issue: 11 Pages: 845-851

    • DOI

      10.2472/jsms.68.845

    • NAID

      130007748601

    • ISSN
      0514-5163, 1880-7488
    • Year and Date
      2019-11-15
    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Novel Experimental Contrivance on Competitive Cracking in Multilayered Nano-structures2019

    • Author(s)
      Takayuki Kitamura, Takashi Sumigawa, Kai Huang, Yabin Yan, Li-cheng Guo
    • Journal Title

      Theoretical and Applied Fracture Mechanics

      Volume: 100 Pages: 319-327

    • DOI

      10.1016/j.tafmec.2019.01.033

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] FE-SEM in situ Observation of Damage Evolution in Tension-compression Fatigue of Micro-sized Single-crystal Copper2019

    • Author(s)
      Takashi Sumigawa, Shin Uegaki, Tetsuya Yukishita, Shigeo Arai, Yoshimasa Takahashi, and Takayuki Kitamura
    • Journal Title

      Materials Science and Engineering A

      Volume: A764 Pages: 138218-138218

    • DOI

      10.1016/j.msea.2019.138218

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of Experimental Methodology on Fracture Toughness of Micro-Scale Polymer Resins under In Situ Observation2019

    • Author(s)
      Ryota Kaneko, Eiichi Kaneko, Takashi Sumigawa, Takayuki Kitamura
    • Journal Title

      Material Design & Processing Communications

      Volume: 2(1) Issue: 1

    • DOI

      10.1002/mdp2.102

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Electron engineering of metallic multiferroic polarons in epitaxial BaTiO32019

    • Author(s)
      Tao Xu, Takahiro Shimada, Yasumitsu Araki, Masataka Mori, Gen Fujimoto, Jie Wang, Tong-Yi Zhang, and Takayuki Kitamura
    • Journal Title

      npj Computational Materials

      Volume: 5 Issue: 1 Pages: 23-23

    • DOI

      10.1038/s41524-019-0163-6

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] In situ observation on formation process of nanoscale cracking during tension-compression fatigue of single crystal copper micron-scale specimen2018

    • Author(s)
      Takashi Sumigawa, Kim Byungwoon, Yuki Mizuno, Takuma Morimura, and Takayuki Kitamura
    • Journal Title

      Acta Materialia

      Volume: 153 Pages: 270-278

    • DOI

      10.1016/j.actamat.2018.04.061

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Challenge toward nanometer scale fracture mechanics2018

    • Author(s)
      Takayuki Kitamura, Takashi Sumigawa, Takahiro Shimada
    • Journal Title

      Engineering Fracture Mechanics

      Volume: 187 Pages: 33-44

    • DOI

      10.1016/j.engfracmech.2017.10.009

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Static assessment of nanoscale notched silicon beams using the averaged strain energy density method2018

    • Author(s)
      Pasquale Gallo, Takashi Sumigawa, Takayuki Kitamura, Filippo Berto
    • Journal Title

      Theoretical and Applied Fracture Mechanics

      Volume: 95 Pages: 261-269

    • DOI

      10.1016/j.tafmec.2018.03.007

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Deformation and fracture of micron-sized metal-coated polymer spheres : an in-situ study2018

    • Author(s)
      Molly Bazilchuk, Takashi Sumigawa, Takayuki Kitamura, Zhiliang Zhang, Helge Kristiansen and Jianying He
    • Journal Title

      Advanced Engineering Materials

      Volume: - Issue: 7

    • DOI

      10.1002/adem.201800049

    • Description
      印刷中
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Unstable cracking behavior in nanoscale single crystal silicon: Initiation, unstable propagation and arrest2018

    • Author(s)
      Li-cheng Guo, Kai Huang, Takashi Sumigawa, Yabin Yan, Takayuki Kitamura
    • Journal Title

      Engineering Fracture Mechanics

      Volume: 196 Pages: 113-122

    • DOI

      10.1016/j.engfracmech.2018.04.014

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Continuum thermodynamics of unusual domain evolution-induced toughening effect in nanocracked strontium titanate2018

    • Author(s)
      Le Van Lich, Takahiro Shimada, Jie Wang, Kairi Masuda, Tinh Quoc Bui, Van-Hai Dinh, Takayuki Kitamura
    • Journal Title

      Engineering Fracture Mechanics

      Volume: 190 Pages: 232-244

    • DOI

      10.1016/j.engfracmech.2017.12.030

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Effect of geometric configuration on the electrocaloric properties of nanoscale ferroelectric materials2018

    • Author(s)
      Xu Hou, Huiyu Li, Takahiro Shimada, Takayuki Kitamura, Jie Wang
    • Journal Title

      Journal of Applied Physics

      Volume: 123 Issue: 12 Pages: 124103-124103

    • DOI

      10.1063/1.5020584

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Ferroelectric critical size and vortex domain structures of PbTiO_3 nanodots : A density functional theory study2018

    • Author(s)
      Xiaoyuan Wang, Yabin Yan, Takahiro Shimada, Jie Wang, Takayuki Kitamura
    • Journal Title

      Journal of Applied Physics

      Volume: 123 Issue: 11 Pages: 114101-114101

    • DOI

      10.1063/1.5013049

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Giant magnetoelectric effect at the graphone/ferroelectric interface2018

    • Author(s)
      Jie Wang, Yajun Zhang, Mohapatra Prakash Kumar Sahoo, Takahiro Shimada, Takayuki Kitamura, and Tong-Yi Zhang
    • Journal Title

      Scientific Reports

      Volume: 8 Issue: 1 Pages: 12448-12448

    • DOI

      10.1038/s41598-018-30010-x

    • NAID

      120006534641

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Electronic and Atomic Structures of Edge and Screw Dislocations in Rock Salt Structured Ionic Crystals2018

    • Author(s)
      Masaya Ukita, Atsutomo Nakamura, Tatsuya Yokoi, Katsuyuki Matsunaga
    • Journal Title

      Philosophical Magazine

      Volume: 98 Issue: 24 Pages: 2189-2204

    • DOI

      10.1080/14786435.2018.1478146

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fracture criterion of mixed-mode crack propagation along the interface in nanoscale components2017

    • Author(s)
      Yabin Yan, Kai Huang, Takashi Sumigawa, Takayuki Kitamura
    • Journal Title

      Engineering Fracture Mechanics

      Volume: 193 Pages: 137-150

    • DOI

      10.1016/j.engfracmech.2018.02.014

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Presentation] 引張圧縮繰り返し負荷を受けるマイクロNi単結晶の疲労挙動とその寸法依存性2021

    • Author(s)
      川勝信貴
    • Organizer
      日本機械学会 関西支部第96期定時総会講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] VO2ナノ薄膜におけるモット転移温度の面内 単軸ひずみ負荷応答2021

    • Author(s)
      河村啓
    • Organizer
      日本機械学会 関西支部第96期定時総会講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 円孔欠陥を有する飛び移り座屈構造メカニカルメタマテリアルの力学応答2021

    • Author(s)
      大村知輝
    • Organizer
      日本材料学会 第6回材料WEEK
    • Related Report
      2020 Annual Research Report
  • [Presentation] [001]多重すべり方位を有するマイクロ銅単結晶の引張圧縮疲労挙動2021

    • Author(s)
      高田聡志
    • Organizer
      日本材料学会 第6回材料WEEK
    • Related Report
      2020 Annual Research Report
  • [Presentation] ナノ・マイクロ材料の力学特性評価実験2020

    • Author(s)
      澄川貴志
    • Organizer
      日本材料学会 第69期第1回マルチスケール材料力学部門委員会
    • Related Report
      2020 Annual Research Report
    • Invited
  • [Presentation] マイクロ金属の引張圧縮疲労特性2020

    • Author(s)
      澄川貴志
    • Organizer
      溶接学会 第131回マイクロ接合研究委員会
    • Related Report
      2020 Annual Research Report
    • Invited
  • [Presentation] Fatigue of Micro-sized Copper Single Crystal Specimen under Fully-reversed Axial Loading2019

    • Author(s)
      Takashi Sumigawa
    • Organizer
      5th International Conference on Materials and Reliability (ICMR-2019)
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] SEMピコインデンターを用いた微小材料の強度特性評価2019

    • Author(s)
      澄川貴志
    • Organizer
      ブルカージャパン株式会社京都大学ナノテクノロジーハブ拠点共催『試料最表面の形状・物性を探る』~ナノプローブ表面特性評価技術セ ミナー~
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] マイクロ金属の引張圧縮疲労2019

    • Author(s)
      澄川貴志
    • Organizer
      日本機械学会 マイクロ・ナノ工学部門主催 第10回マイクロ・ナノ工学シンポジウム
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] マイクロ金属の疲労挙動観察2019

    • Author(s)
      澄川貴志
    • Organizer
      日本金属学会 2019年 秋季(第165回)講演大会
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] 電子顕微鏡内での微小材料の強度評価実験2019

    • Author(s)
      澄川貴志
    • Organizer
      RC278「産業変革期の電子実装技術における信頼性設計と熱制御に関する研究分科会」
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] マイクロサイズの銅単結晶試験片の引張圧縮繰り返し変形挙動2019

    • Author(s)
      澄川貴志
    • Organizer
      M&M2019 材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 双晶境界を有するマイクロ銅の引張圧縮疲労過程その場観察2019

    • Author(s)
      安井千央
    • Organizer
      M&M2019 材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] ひずみ負荷を受ける微小強誘電体中のナノドメイン構造変化のその場観察2019

    • Author(s)
      日笠健
    • Organizer
      日本材料学会 第5回材料WEEK ワークショップ
    • Related Report
      2019 Annual Research Report
  • [Presentation] Siナノ非線形ばねの作製とその場観察引張試験2019

    • Author(s)
      金子遼太
    • Organizer
      日本材料学会 第4回マルチスケールシンポジウム
    • Related Report
      2019 Annual Research Report
  • [Presentation] 微小BaTiO3単結晶中のナノドメイン構造の引張負荷応答2019

    • Author(s)
      日笠健
    • Organizer
      日本材料学会 第4回マルチスケールシンポジウム
    • Related Report
      2019 Annual Research Report
  • [Presentation] Formation of Slip Bands in Nano-polycrystalline Copper sandwiched between Brittle Materials2018

    • Author(s)
      Takashi Sumigawa
    • Organizer
      European conference on fracture
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Fatigue of single-crystal gold micro-specimen by resonant vibration2018

    • Author(s)
      Takashi Sumigawa
    • Organizer
      1st International Conference on Theoretical, Applied, Experimental Mechanic
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Challenge toward Fracture Mechanics in Atomic Scale2018

    • Author(s)
      Takayuki Kitamura
    • Organizer
      European conference on fracture
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Remarks] 京都大学大学院工学研究科機械理工学専攻 材料物性学研究室

    • URL

      http://cyber.me.kyoto-u.ac.jp/

    • Related Report
      2019 Annual Research Report

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Published: 2018-04-23   Modified: 2022-01-27  

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