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Establishment of evaluation technique for thermo-viscoelastic property of glass using viscosity measurement

Research Project

Project/Area Number 18K03856
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 18010:Mechanics of materials and materials-related
Research InstitutionKindai University

Principal Investigator

ITO Hiroaki  近畿大学, 工学部, 准教授 (70534981)

Project Period (FY) 2018-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2020: ¥520,000 (Direct Cost: ¥400,000、Indirect Cost: ¥120,000)
Fiscal Year 2019: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2018: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Keywords熱粘弾性特性 / 応力緩和 / シフトファクタ / 粘度測定 / ネットワーク構造 / 光学ガラス / ガラス組成 / クリープ試験
Outline of Final Research Achievements

In this study, unidirectional compression creep tests were performed for various commercial optical glasses to investigate the effects of glass compositions or network structures on stress relaxation behavior. As a result, it was clarified that these two factors have little effect on the stress relaxation behavior and draw a master curve of shear relaxation modulus with almost the same shape in any glass. In addition, we tried to measure the viscosity by the parallel plate test and succeeded in calculating the shift factor from the estimated viscosity. In other words, it has become possible to significantly reduce the measurement time for the shift factor compared to the conventional creep test. Furthermore, the parallel plate tests with an extremely low loads using a thermomechanical analyzer were also performed, and it was clarified that the shift factors are not affected by the measured loads.

Academic Significance and Societal Importance of the Research Achievements

本研究では,ガラスの熱粘弾性特性を短時間かつ容易に同定する新たな手法を提案した.光学ガラスの応力緩和挙動はネットワーク構造やガラス組成の影響を受けずほぼ同一挙動を示すこと,また平行平板試験による粘度測定によってシフトファクタ(時間‐温度移動因子)を,従来のクリープ試験と同等の精度を有しつつ短時間で評価できることを明らかにした.特に粘度測定によるシフトファクタの決定手法は,ガラスのみならず各種高分子材料への適用も可能と考えられることから学術的にも価値がある成果と考えている.

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (7 results)

All 2021 2020 2019 2018

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (6 results)

  • [Journal Article] Derivation of Shift Factor for the Optical Glass Using Viscosity Measurement2020

    • Author(s)
      伊藤 寛明、百田 大地、前岡 勇輝、藤原 光紘、荒井 政大
    • Journal Title

      Journal of the Japanese Society for Experimental Mechanics

      Volume: 20 Issue: 1 Pages: 23-27

    • DOI

      10.11395/jjsem.20.23

    • NAID

      130007828522

    • ISSN
      1346-4930, 1884-4219
    • Year and Date
      2020-04-03
    • Related Report
      2019 Research-status Report
    • Peer Reviewed
  • [Presentation] 光学ガラスの熱粘弾性特性に及ぼすネットワーク構造の影響2021

    • Author(s)
      本田涼馬, 有岡直希, 前田祐, 伊藤寛明
    • Organizer
      日本機械学会中国四国支部第59期総会・講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 熱機械分析装置を用いた光学ガラスのシフトファクタの評価及び測定荷重の影響2020

    • Author(s)
      伊藤寛明,高橋直矢,中桐正貴
    • Organizer
      日本非破壊検査協会総合シンポジウム2020
    • Related Report
      2020 Annual Research Report
  • [Presentation] 応力緩和試験によるガラスの熱粘弾性特性評価2019

    • Author(s)
      伊藤寛明、中澤貴之
    • Organizer
      日本実験力学会2019年次講演会
    • Related Report
      2019 Research-status Report
  • [Presentation] ガラスの熱粘弾性特性に及ぼす測定荷重の影響2019

    • Author(s)
      伊藤寛明,前岡勇輝,中桐正貴
    • Organizer
      日本非破壊検査協会平成30年度第3回応力・ひずみ測定部門講演会
    • Related Report
      2018 Research-status Report
  • [Presentation] 光学ガラスの熱粘弾性特性に及ぼす化学組成の影響2018

    • Author(s)
      伊藤寛明, 吉崎康平, 百田大地
    • Organizer
      日本実験力学会2018年次講演会
    • Related Report
      2018 Research-status Report
  • [Presentation] 粘度測定に基づいた光学ガラスのシフトファクタの導出2018

    • Author(s)
      伊藤寛明, 百田大地, 笠村裕也
    • Organizer
      日本非破壊検査協会平成30年度秋季講演大会
    • Related Report
      2018 Research-status Report

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Published: 2018-04-23   Modified: 2022-01-27  

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