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Measurement of temeprature dependence of heat capacity on high temeprature melts using an electrostatic levitation method

Research Project

Project/Area Number 18K04002
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 19020:Thermal engineering-related
Research InstitutionJapan Aerospace EXploration Agency

Principal Investigator

Ishikawa Takehiko  国立研究開発法人宇宙航空研究開発機構, 宇宙科学研究所, 教授 (00371138)

Project Period (FY) 2018-04-01 – 2022-03-31
Project Status Completed (Fiscal Year 2021)
Budget Amount *help
¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
Fiscal Year 2020: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2019: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2018: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywords無容器プロセッシング / 高温融体 / 熱物性計測 / 定圧比熱 / 輻射率 / 偏光計測 / 浮遊
Outline of Final Research Achievements

This research tries to establish a method to measure the emissivity of electrostatically levitated sample with polarimetry over wide temperature ranges. By combining this technique with the heat capacity measurement technique, temperature dependence of heat capacity can be obtained. A commercial polarimeter used to measure thin film thickness was combined with electrostatic levitators to validate the method. Since the levitated sample is too small (2 mm in diameter) and its curvature was too steep to reflect the incident laser properly, good SN could not be obtained at the polarimeter. One possible solution is to rotate the sample and get oblate shape, and this will be perused.

Academic Significance and Societal Importance of the Research Achievements

鉄など融点の高い金属について、液体状態の物性値は鋳造など融体を用いた製造プロセスの高度化に必要です。しかし、高温で容器と反応する等の問題で測定が困難です。試料を浮遊させる無容器法によってこの問題が解決され、密度など多くの物性値が測定可能になりました。比熱も工業的・学術的に重要な物性値で、本研究ではその温度依存性の測定に挑戦しています。

Report

(5 results)
  • 2021 Annual Research Report   Final Research Report ( PDF )
  • 2020 Research-status Report
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (10 results)

All 2021 2020 2019 2018

All Journal Article (3 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 3 results) Presentation (7 results)

  • [Journal Article] Spectral emissivity, hemispherical total emissivity, and constant pressure heat capacity of liquid vanadium measured by an electrostatic levitator2021

    • Author(s)
      Ishikawa Takehiko、Koyama Chihiro、Nakata Yui、Watanabe Yuki、Paradis Paul-Fran?ois
    • Journal Title

      The Journal of Chemical Thermodynamics

      Volume: 163 Pages: 106598-106598

    • DOI

      10.1016/j.jct.2021.106598

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Measurement of thermophysical properties of molten Si-Cr and Si-Fe alloys for design of solution growth of SiC2020

    • Author(s)
      S. Kawanishi, M. Abe, C. Koyama, T. Ishikawa, H. Shibata
    • Journal Title

      Journal of Crystal Growth

      Volume: 541 Pages: 125658-125658

    • DOI

      10.1016/j.jcrysgro.2020.125658

    • Related Report
      2019 Research-status Report
    • Peer Reviewed
  • [Journal Article] Spectral emissivity and constant pressure heat capacity of liquid titanium measured by an electrostatic levitator2019

    • Author(s)
      Ishikawa Takehiko、Koyama Chihiro、Nakata Yui、Watanabe Yuki、Paradis Paul-Francois
    • Journal Title

      The Journal of Chemical Thermodynamics

      Volume: 131 Pages: 557-562

    • DOI

      10.1016/j.jct.2018.12.002

    • Related Report
      2018 Research-status Report
    • Peer Reviewed
  • [Presentation] 静電浮遊炉におけるバナジウム融体の放射率測 定および比熱の算出(第2 報)2021

    • Author(s)
      渡邊 勇基, 小山 千尋, 石川 毅彦
    • Organizer
      第42回日本熱物性シンポジウム
    • Related Report
      2021 Annual Research Report
  • [Presentation] 静電浮遊炉におけるバナジウム融体の放射率測定および比熱の算出2020

    • Author(s)
      仲田結衣、小山千尋、石川毅彦
    • Organizer
      第41回熱物性シンポジウム
    • Related Report
      2020 Research-status Report
  • [Presentation] 静電浮遊炉におけるCr-Si融体の放射率および比熱の測定2019

    • Author(s)
      仲田結衣、小山千尋、石川毅彦、川西咲子、柴田浩幸、吉川健
    • Organizer
      第40回日本熱物性シンポジウム
    • Related Report
      2019 Research-status Report
  • [Presentation] 静電浮遊炉によるTi融体の放射率および比熱測定法2018

    • Author(s)
      (251)仲田結衣、渡邊勇基、織田裕久、田丸晴香、小山千尋、石川毅彦
    • Organizer
      日本マイクログラビティ応用学会第30回学術講演会
    • Related Report
      2018 Research-status Report
  • [Presentation] 静電浮遊炉を用いたY3Al5O12融体の熱物性測定2018

    • Author(s)
      小山千尋、渡邊勇基、仲田結衣、石川毅彦
    • Organizer
      第47回結晶成長国内会議
    • Related Report
      2018 Research-status Report
  • [Presentation] 静電浮遊炉におけるTi融体の放射率測定2018

    • Author(s)
      (254)仲田結衣、渡邊勇基、織田裕久、田丸晴香、小山千尋、石川毅彦
    • Organizer
      第39回日本熱物性シンポジウム
    • Related Report
      2018 Research-status Report
  • [Presentation] 静電浮遊法を用いたY3Al5O12融体の輻射率および比熱測定2018

    • Author(s)
      小山千尋、渡邊勇基、仲田結衣、石川毅彦
    • Organizer
      第39回日本熱物性シンポジウム
    • Related Report
      2018 Research-status Report

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Published: 2018-04-23   Modified: 2023-01-30  

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