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Nanostructure control by forced nucleation mechanism during container-less rapid solidification process

Research Project

Project/Area Number 18K04767
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionTohoku University

Principal Investigator

Yodoshi Noriharu  東北大学, 金属材料研究所, 助教 (60586494)

Project Period (FY) 2018-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2020: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2019: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2018: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywords無容器凝固 / 急冷凝固 / アモルファス / 軟磁気特性 / ナノ組織制御 / 超音波照射 / 鉄系アモルファス / 単分散粒子 / ナノ結晶 / 軟磁性材料
Outline of Final Research Achievements

Ultrasonic irradiation was applied to a supercooled droplet (FeSiBP(Cu) alloy) to induce intentional forced nucleation during the drop-tube quenching, resulting in the success of fabrication of iron-based rapid solidification particles with uniformly dispersed nanocrystalline nuclei in the amorphous matrix (nanohetero-structure). The nanostructure of the obtained particles after heat treatment was observed by transmission electron microscopy (TEM), and it was confirmed that a nanostructure with uniformly dispersed nanocrystalline phases of several nm grain size (less than 5 nm) was obtained. The magnetic properties of the single particles showed that the saturation magnetic flux density of iron-based amorphous particles quenched under ultrasonic irradiation was significantly higher than that without irradiation.

Academic Significance and Societal Importance of the Research Achievements

非晶質相を得るための急冷凝固プロセスにおいて,超音波照射による選択的なエネルギー投入により,ナノ結晶組織を制御できる可能性を示すことができた.本研究で用いた鉄系非晶質合金は優れた軟磁気特性を示し,そのナノ組織制御により低損失な軟磁性材料として工業的に応用することが期待されており,省エネルギーな磁気デバイスの実現に向けた有用な基礎研究結果を得ることができた.

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (16 results)

All 2021 2020 2019 2018 Other

All Int'l Joint Research (3 results) Journal Article (3 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 3 results,  Open Access: 2 results) Presentation (9 results) (of which Int'l Joint Research: 2 results,  Invited: 3 results) Patent(Industrial Property Rights) (1 results)

  • [Int'l Joint Research] IWT Bremen/University of Bremen(ドイツ)

    • Related Report
      2020 Annual Research Report
  • [Int'l Joint Research] University of Bremen/IWT(ドイツ)

    • Related Report
      2019 Research-status Report
  • [Int'l Joint Research] Bremen University(ドイツ)

    • Related Report
      2018 Research-status Report
  • [Journal Article] Processing soft ferromagnetic metallic glasses: on novel cooling strategies in gas atomization, hydrogen enhancement, and consolidation2020

    • Author(s)
      Ciftci N.、Yodoshi N.、Armstrong S.、M?dler L.、Uhlenwinkel V.
    • Journal Title

      Journal of Materials Science & Technology

      Volume: 59 Pages: 26-36

    • DOI

      10.1016/j.jmst.2020.03.077

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Uniformity of the glassy state of iron-based metallic glassy particles and reproducibility of fabricating microparts2020

    • Author(s)
      Yamada Rui、Yodoshi Noriharu、Nomura Naoyuki、Saida Junji、Kawasaki Akira
    • Journal Title

      Materials & Design

      Volume: 191 Pages: 108667-108667

    • DOI

      10.1016/j.matdes.2020.108667

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Processing soft ferromagnetic metallic glasses: on novel cooling strategies in gas atmization, hydrogen enhancement, and cosolidation2020

    • Author(s)
      N.Ciftci, N. Yodoshi, S. Armstrong, L. Madler, V. Uhlenwinkel
    • Journal Title

      Journal of Materials Science & Technology

      Volume: 印刷中

    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Presentation] Fe-based metallic glassy mono-dispersed particles prepared by container-free solidification process and their nanocrystallization behavior.2021

    • Author(s)
      Noriharu Yodoshi, Rui Yamada, Akira Kawasaki
    • Organizer
      THERMEC 2021 International Conference on PROCESSING & MANUFACTURING OF ADVANCED MATERIALS Processing, Fabrication, Properties, Applications (THERMEC'2020)
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 高品位ガスアトマイズ粉末の作製の研究(2)2020

    • Author(s)
      吉年規治、遠藤 嵩英、正橋 直哉
    • Organizer
      日本金属学会春季大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 高品位ガスアトマイズ粉末の作製の研究2020

    • Author(s)
      吉年規治、遠藤 嵩英、正橋 直哉
    • Organizer
      日本金属学会春季大会
    • Related Report
      2019 Research-status Report
  • [Presentation] Pd系金属ガラス粒子を用いた粘性流動成形加工による微小部品の作製2019

    • Author(s)
      吉年規治、伊佐野はる香、山田類、菊池圭子、野村直之、川崎亮
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Related Report
      2019 Research-status Report
  • [Presentation] 単粒子圧縮試験法によるFe系金属ガラス過冷却液体の粘性係数測定とその組成依存性2019

    • Author(s)
      吉年規治、青栁慶真、山田類、菊池圭子、野村直之、川崎亮
    • Organizer
      日本金属学会春季講演大会
    • Related Report
      2018 Research-status Report
  • [Presentation] Fe-based metallic glassy mono-dispersed particles prepared by container-free solidification process and their applications.2018

    • Author(s)
      Noriharu Yodoshi, Rui Yamada, Akira Kawasaki
    • Organizer
      THERMEC 2018 International Conference on PROCESSING & MANUFACTURING OF ADVANCED MATERIALS
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Fe系非晶質単粒子のナノ組織制御と磁気特性評価2018

    • Author(s)
      峯岸剛太、菊池圭子、野村直之、山田類、吉年規治、川崎亮
    • Organizer
      粉体粉末冶金協会秋季大会
    • Related Report
      2018 Research-status Report
  • [Presentation] 鉄系金属ガラス単分散粒子の作製とその応用2018

    • Author(s)
      吉年規治
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Related Report
      2018 Research-status Report
    • Invited
  • [Presentation] 無容器凝固法で作製した鉄系非晶質粒子のナノ結晶化挙動と磁気特性評価2018

    • Author(s)
      吉年規治、山田類、川崎亮
    • Organizer
      日本材料学会 第4回材料WEEK
    • Related Report
      2018 Research-status Report
  • [Patent(Industrial Property Rights)] ガスアトマイズ法による金属合金粉末及びその製造方法2020

    • Inventor(s)
      吉年規治、正橋直哉
    • Industrial Property Rights Holder
      吉年規治、正橋直哉
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2020-033235
    • Filing Date
      2020
    • Related Report
      2019 Research-status Report

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Published: 2018-04-23   Modified: 2022-01-27  

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