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Topological analysis of 3D pore distribution in sintered metals-Elucidation of a fatigue failure process of porous materials.

Research Project

Project/Area Number 18K04779
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionKyushu University

Principal Investigator

Ozaki Yukiko  九州大学, 工学研究院, 教授 (20637946)

Co-Investigator(Kenkyū-buntansha) 品川 一成  九州大学, 工学研究院, 教授 (30215983)
平山 恭介  京都大学, 工学研究科, 助教 (70717743)
Project Period (FY) 2018-04-01 – 2023-03-31
Project Status Completed (Fiscal Year 2022)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2020: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2019: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2018: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords焼結金属 / 疲労破壊機構 / 3次元気孔配置 / 位相幾何解析 / パーシステント・ホモロジー / 金属射出成形 / Ti合金 / 3次元気孔配置 / X線CT / 弾性FEM / 有限要素解析 / 位相解析 / パーシステント / 疲労破壊 / 金属疲労機構 / 気孔配置 / パーシステントホモロジー / X線CT測定 / トポロジー / 気孔3D分布
Outline of Final Research Achievements

The purpose of this study was to elucidate the role of pores inside the sintered metal in fatigue fracture. First, the residual pore configuration inside the sintered body was visualized using X-ray CT, and the morphological parameters for all pore configurations were quantified using image analysis and topology. At the same time, based on the CT images, the stress distribution in the material under fatigue testing was estimated, and it was found that the edges of the largest pores were the maximum stress concentration points and possible crack initiation sources. Fracture mechanics analysis using the pore morphology parameters showed that the fatigue strength decreases with increasing cross-sectional area of the largest pore, and that the fatigue fracture mechanism of sintered metals can be explained by the same fatigue fracture model as that of metals made from dissolved metals.

Academic Significance and Societal Importance of the Research Achievements

機械部品は,使用環境下で繰返し応力が負荷され、疲労強度の向上は全ての素材における永遠の課題であり、内部欠陥との関係において解析が進んできた。粉末を原料とする焼結金属では、粉末粒子間隙由来の多数の気孔が残存するため、疲労破壊に関わる欠陥の特定が困難であった。そこで、残存気孔配置を放射光の高輝度X線を用いたイメージングにより可視化し、さらに位相幾何学(パーシステント・ホモロジー)の厳密解として、その気孔群の3D配置を定量化することによって、破壊機構を定量的に解析した。この手法は、積層造形等で創造される粉末原料の素材開発において有用な手法となることが期待される。

Report

(6 results)
  • 2022 Annual Research Report   Final Research Report ( PDF )
  • 2021 Research-status Report
  • 2020 Research-status Report
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (12 results)

All 2023 2022 2021 2019 2018 Other

All Journal Article (2 results) (of which Peer Reviewed: 1 results) Presentation (9 results) (of which Int'l Joint Research: 4 results,  Invited: 1 results) Remarks (1 results)

  • [Journal Article] Quantitative estimation of contribution of pore size and the distance between nearest neighbour pores on high cycle fatigue (HCF) crack initiation in Ti-6Al-4V MIM-sintered materials2023

    • Author(s)
      I. Ando, K. Kudo, K. Hirayama, Y. Shigeta, K.Shinagawa, A. Takeuchi, M. Uesugi, Y.Ozaki
    • Journal Title

      International Journal of Fatigue

      Volume: 171 Pages: 107557-107557

    • DOI

      10.1016/j.ijfatigue.2023.107557

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Four-dimensional observation of ductile fracture in sintered iron using synchrotron X-ray laminography2019

    • Author(s)
      Y. Ozaki, Y. Mugita, M. Aramaki, O. Furukimi, S. Oue, F. Jiang, T. Tsuji, A. Takeuchi, M. Uesugi & K. Ashizuka
    • Journal Title

      Powdwe Metallurgy

      Volume: 62 Issue: 2 Pages: 146-154

    • DOI

      10.1080/00325899.2019.1585032

    • Related Report
      2019 Research-status Report 2018 Research-status Report
  • [Presentation] Understanding the effect of process parameters on three-dimensional pore configurations and mechanical properties of laser additive manufactured Ti using synchrotron X-ray computed tomography and homology2023

    • Author(s)
      Y. Shigeta, A. Masatoshi, K. Kudo, K. Shinagawa, N.Nomura, K. Kondoh, M.Hoshino, K.Uesugi, Y. Ozaki
    • Organizer
      The International Conference on Sintering 2023, Gifu, Japan
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Application of Persistent Homology to Pore Configurations in Sintered Bodies2022

    • Author(s)
      Y. Ozaki, I. Ando, R. Kusunoki, Y. Shigeta, F. Jiang, T. Tsuji
    • Organizer
      WorldPM 2022, Lyon, France
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] X線CTによって可視化されたTi6Al4V-MIM材の残留気孔の数値化2021

    • Author(s)
      安東壱進,工藤健太郎,平山恭介,重田雄二,品川一成,尾﨑由紀子
    • Organizer
      日本鉄鋼協会第182回講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] 多孔質材料中の気孔配置に対するパーシステント・ホモロジー解析-モデル配置による検証2021

    • Author(s)
      安東壱進,重田雄二,尾﨑由紀子
    • Organizer
      日本鉄鋼協会第182回講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] Four-dimensional observation of ductile fracture in sintered iron using synchrotron X-ray laminography2019

    • Author(s)
      Y. Ozaki, Y. Mugita, M. Aramaki, O. Furukimi, S. Oue, F. Jiang, T. Tsuji, A. Takeuchi, M. Uesugi & K. Ashizuka
    • Organizer
      EuroPM2018
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] 高密度純鉄焼結体中の気孔配置が引張変形における亀裂発生に及ぼす影響2019

    • Author(s)
      中村公二、尾﨑由紀子、荒牧正俊、平山恭介、辻 健、蒋 飛
    • Organizer
      日本金属学会
    • Related Report
      2019 Research-status Report
  • [Presentation] 等方圧加圧処理により閉気孔を閉塞させた高密度純鉄焼結体の延性破壊機構の解析2019

    • Author(s)
      鴨川知誉, 芦塚康佑, 荒牧正俊, 尾﨑由紀子
    • Organizer
      日本鉄鋼協会
    • Related Report
      2019 Research-status Report
  • [Presentation] Four-dimensional Observation of Ductile Fracture in Sintered Iron using Synchrotron X-ray Laminography2019

    • Author(s)
      Y. Ozaki, Y. Mugita, M. Aramaki, S. Ooue, K. Ashizuka, A. Takeuchi, M. Uesugi and O. Furukimi
    • Organizer
      Euro PM2018 Congress, Birbao, Spain
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research
  • [Presentation] 閉気孔からなる高密度純鉄焼結体の延性破壊過程における 閉気孔の形態および気孔間距離の影響―閉気孔の切欠き効果の検証2018

    • Author(s)
      中村 公二, 鴨川 知誉,麦田 康敬 , 荒牧 正俊,芦塚 康佑,尾﨑 由紀子
    • Organizer
      粉体粉末冶金協会平成30年度秋季講演大会
    • Related Report
      2018 Research-status Report
  • [Remarks] 研究者情報

    • URL

      https://hyoka.ofc.kyushu-u.ac.jp/search/details/K006419/index.html

    • Related Report
      2022 Annual Research Report

URL: 

Published: 2018-04-23   Modified: 2024-01-30  

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