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Evaluation model of lipid oxidation stability for spray-dried powder of functional lipid powder imparted oxidation stability with antioxidant.

Research Project

Project/Area Number 18K05517
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 38050:Food sciences-related
Research InstitutionSetsunan University (2020)
Kagawa University (2018-2019)

Principal Investigator

Yoshii Hidefumi  摂南大学, 農学部, 教授 (60174885)

Project Period (FY) 2018-04-01 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2020: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2019: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2018: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywordsイサダオイル / 高度不飽和脂肪酸 / エイコサペンタエン酸 / ドコサヘキサエン酸 / 噴霧乾燥 / 粉末 / 乳化 / 貯蔵安定性 / EPA / DHA / アブラミの式 / 魚油 / 油滴径 / 保存安定性 / 機能性脂質 / キラヤニン
Outline of Final Research Achievements

Krill oil (KO) is rich in polyunsaturated fatty acids, especially eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA), which have many health benefits. However, the oil is unstable owing to its high degree of unsaturation. The oil was microencapsulated using maltodextrin with a dextrose equivalent of 19 as a wall material to improve its stability. A saponin (Quillayanin) and sodium caseinate were also used as emulsifiers, and rosemary oil (RO) extract or sodium ascorbate was used as an antioxidant. The microencapsulated KO samples were stored at 25, 50, or 70℃ to examine the stability of EPA and DHA in the KO. For the microcapsules prepared from emulsions with smaller oil droplets, the surface oil ratios of EPA and DHA were higher, but the fatty acids were less stable at 50 and 70 °C. On the other hand, both EPA and DHA in the microcapsules prepared from emulsions with small oil droplets were stable at 25℃.

Academic Significance and Societal Importance of the Research Achievements

健康な生活を維持していく上で機能性食品の役割は非常に重要となってきている.血液の粘度や血圧の維持に重要であると考えられているエイコサペンタエン酸(EPA)、ドコサヘキサエン酸(DHA)等のω-3系高度不飽和脂肪酸(PUFA)を高含有する魚油やクリル油は、その生理機能から非常に注目されている。この魚油を安定な状態で食品に使用するため、魚油を乳化剤によりエマルションを作製し、その溶液を噴霧乾燥することにより乳化魚油噴霧乾燥粉末を得る。この粉末中魚油中の機能性成分であるEPA, DHAの安定性に及ぼす油滴径、粉末径の影響を検討し、安定な機能性脂質粉末作製のための工学的指針を確立させた。

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (28 results)

All 2021 2020 2019 2018

All Journal Article (6 results) (of which Int'l Joint Research: 4 results,  Peer Reviewed: 4 results,  Open Access: 2 results) Presentation (19 results) (of which Int'l Joint Research: 7 results,  Invited: 2 results) Book (2 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Stability of eicosapentaenoic acid and docosahexaenoic acid in spray-dried powder of emulsified krill oil2021

    • Author(s)
      Afroza Sultana, Yui Maki , Antonio Fermin, Shuji Adachi , Hidefumi Yoshii
    • Journal Title

      Future Foods

      Volume: 3 Pages: 1-6

    • DOI

      10.1016/j.fufo.2020.100009

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Effect of Antioxidant and Pro-oxidant on the Stability of Microencapsulated Squalene by Spray Drying2021

    • Author(s)
      Dwi Ayuni, Joko Nugroho Wahyu Karyadi, Arifin Dwi Saputro, Hidefumi Yoshii
    • Journal Title

      Agritech

      Volume: 41 Issue: 1 Pages: 49-57

    • DOI

      10.22146/agritech.52741

    • Related Report
      2020 Annual Research Report
  • [Journal Article] Crystallisation properties of amorphous cyclodextrin powders and their complexation with fish oil.2019

    • Author(s)
      Frierler, L., Ho, T.M.., Anthony, A., Yoshii, H., Yago A.J.E., Bhandari, B.
    • Journal Title

      Journal of Food Science and Technology

      Volume: 56 Issue: 3 Pages: 1519-1529

    • DOI

      10.1007/s13197-019-03643-7

    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] 機能性物質を閉じ込める~機能性食品粉末の製造と特性~2018

    • Author(s)
      吉井 英文、高重 至成、四日 洋和、安達 修二
    • Journal Title

      化学工学

      Volume: 82 Pages: 362-365

    • Related Report
      2018 Research-status Report
  • [Journal Article] Measuring method of glass transition temperature using aroma sensor.2018

    • Author(s)
      Chantanuson,R., Zhu, J., Shiga, H., Adachi, S., Soottitantawat, A., Yoshii, H.
    • Journal Title

      Food and Applied Bioscience Journal

      Volume: 6 Pages: 253-261

    • Related Report
      2018 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Encapsulation of krill oil by spray drying2018

    • Author(s)
      Takashige, S., Hermawan, A.D., Sultana, A., Shiga, H., Adachi, S., Yoshii, H.
    • Journal Title

      Proceeding of 21st International Drying Symposium

      Volume: 1 Pages: 587-594

    • Related Report
      2018 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Presentation] 乳化イサダオイル噴霧乾燥粉末中のエイコサペンタエン 酸,およびドコサヘキサエン酸の安定性2021

    • Author(s)
      フェルミン アントニオ, 高重至成 , アフロザ スルタナ, 安達修二, 吉井英文
    • Organizer
      日本農芸化学会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 乳化イサダオイルの噴霧乾燥粉末化と作製粉末の特質2020

    • Author(s)
      牧由惟, 安達修二, 吉井英文
    • Organizer
      日本食品工学会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 噴霧乾燥を用いた機能性食品粉末の作製2019

    • Author(s)
      吉井英文
    • Organizer
      中国地区化学工学懇話会記念講演会
    • Related Report
      2019 Research-status Report
    • Invited
  • [Presentation] Release from Spray-Dried Powders with Various Wall Materials.2019

    • Author(s)
      Takashige, S., Ariyanto, H,D., Adachi, S., Yoshii, H.
    • Organizer
      Third Nordic Baltic Drying Conference
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] イサダオイルの酵母への包括による安定化2019

    • Author(s)
      Sultana, A., Fermin, A., 安達修二, 吉井英文
    • Organizer
      食品工学会第20回大会
    • Related Report
      2019 Research-status Report
  • [Presentation] Oxidation stability of krill oil in emulsified spray-dried powder.2019

    • Author(s)
      Fermin, A., 安達修二, 吉井英文
    • Organizer
      食品工学会第20回大会
    • Related Report
      2019 Research-status Report
  • [Presentation] Effect of storage temperature and oil-droplet diameter to the stability of squalene oil2019

    • Author(s)
      Ayuni, D., 吉井英文
    • Organizer
      食品工学会第20回大会
    • Related Report
      2019 Research-status Report
  • [Presentation] Release rates of emulsified d-limonene encapsulated in spray-dried powders.2019

    • Author(s)
      Takashige, S., Ariyanto, H,D., Adachi, S., Yoshii, H.
    • Organizer
      Asian Pacific Confederation of Chemical Engineering (APCChE) Congress
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] Stability of DHA and EPA in encapsulated krill oil in spray-dried encapsulated yeast powder.2019

    • Author(s)
      Sultana, A.,Ferimin A., Adachi, S., Yoshii, H.
    • Organizer
      Asian Pacific Confederation of Chemical Engineering (APCChE) Congress
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] Oxidative stability of microencapsulated krill oil by spray drying.2019

    • Author(s)
      Fermin, A., Adachi, S., Yoshii, H
    • Organizer
      Asian Pacific Confederation of Chemical Engineering (APCChE) Congress.
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] Flavor release analysis from corn starch-coated spray-dried powders with ramping method of humidity at a constant temperature.2019

    • Author(s)
      Takashige, S, Ariyanto H.D., Yoshii, H.
    • Organizer
      The 10th Asia Pacific Drying Conference (ADC)
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] イサダオイルの乳化特性と粉末化.2019

    • Author(s)
      Fermin,A. 高重至成,Hermawan, A.D.,Sultana S., 安達修二,吉井英文
    • Organizer
      日本農芸化学会2019年度大会
    • Related Report
      2018 Research-status Report
  • [Presentation] Formation inclusion complex of cyclodextrin and allyl sulfide and their stability.2018

    • Author(s)
      Nguyen, T.V.A., Yoshii, H.
    • Organizer
      The 19th International Cyclodextrin Symposium
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research
  • [Presentation] Encapsulation and stability of allyl sulfide in cyclodextrin with and without the presence of medium chain triglycerides.2018

    • Author(s)
      Nguyen T.V.A., Yoshii, H.
    • Organizer
      日本食品工学会第18回(2018年度)年次大会
    • Related Report
      2018 Research-status Report
  • [Presentation] Dynamic flavor release from spray-dried encapsulated yeast cells.2018

    • Author(s)
      Afroza, S., Yoshii, H.
    • Organizer
      日本食品工学会第18回(2018年度)年次大会
    • Related Report
      2018 Research-status Report
  • [Presentation] トランスグルタミナーゼ処理によるコラーゲンペプチド・カゼイン含有エマルションの物理的特性2018

    • Author(s)
      泉秀明,御器谷友美,津田信治,吉井英文
    • Organizer
      日本食品科学工学会第65回大会
    • Related Report
      2018 Research-status Report
  • [Presentation] 乳化剤蛋白質のトランスグルタミナーゼ処理による乳化魚油粉末の酸化安定性.2018

    • Author(s)
      山内惇生,高重至成,泉秀明,御器谷友美,津田信治,吉井英文
    • Organizer
      日本食品科学工学会第65回大会
    • Related Report
      2018 Research-status Report
  • [Presentation] 中鎖脂肪酸トリグリセリドを用いたフレーバー包括シクロデキストリン粉末の噴霧乾燥法による作製2018

    • Author(s)
      Nguyen, T.V.A., Yoshii, H.
    • Organizer
      第35回シクロデキストリンシンポジウム
    • Related Report
      2018 Research-status Report
  • [Presentation] Encapsulation of krill oil by spray drying.2018

    • Author(s)
      Takashige, S., Hermawan, A.D., Sultana, A., Shiga, H., Adachi, S., Yoshii, H.
    • Organizer
      21st International Drying Symposium,
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research
  • [Book] 脂質・脂肪酸関連物質の使いこなし方-素材開発・機能創生・応用技術ー2020

    • Author(s)
      吉井英文、高重至成
    • Total Pages
      592
    • Publisher
      テクノシステム
    • ISBN
      9784924728868
    • Related Report
      2020 Annual Research Report
  • [Book] Nano-food Engineering2020

    • Author(s)
      Afroza Sultana, Asmaliza Ghani, Shuji Adachi, Hidefumi Yoshii
    • Total Pages
      616
    • Publisher
      Springer International Publishing
    • ISBN
      9783030445515
    • Related Report
      2020 Annual Research Report
  • [Patent(Industrial Property Rights)] 乳化イサダオイル2018

    • Inventor(s)
      吉井英文、高森吉守
    • Industrial Property Rights Holder
      吉井英文、高森吉守
    • Industrial Property Rights Type
      特許
    • Patent Publication Number
      2020-022387
    • Filing Date
      2018
    • Acquisition Date
      2020
    • Related Report
      2019 Research-status Report

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Published: 2018-04-23   Modified: 2022-01-27  

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