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Precise isotope analysis of ultra trace lead using high resistance amplifiers.

Research Project

Project/Area Number 18K14259
Research Category

Grant-in-Aid for Early-Career Scientists

Allocation TypeMulti-year Fund
Review Section Basic Section 34020:Analytical chemistry-related
Research InstitutionGakushuin University (2019-2022)
Japan Agency for Marine-Earth Science and Technology (2018)

Principal Investigator

Fukami Yusuke  学習院大学, 理学部, 助教 (10754418)

Project Period (FY) 2018-04-01 – 2023-03-31
Project Status Completed (Fiscal Year 2022)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2020: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2019: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2018: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywords鉛同位体 / 表面電離型質量分析計 / ダブルスパイク / トータルエバポレーション / 極微量分析 / TIMS / トータルエバポレーション法 / ダブルスパイク法 / 同位体分析 / 年代測定
Outline of Final Research Achievements

Improvements have been made to the measurement method for the high-precision analysis of lead isotope ratios at ultra trace amount. Using an amplifier with a higher resistance than conventional amplifiers connected to the detector improves the signal-to-noise ratio and provides precise measurement for signals of low intensity, but the differences in response to time variations in signal intensity are problematic. The influence of the different time response of the signal when using a high-resistance amplifier on the isotope ratio measurements was evaluated, and a high-precision isotope ratio analysis method for ultra trace amounts of lead was developed.

Academic Significance and Societal Importance of the Research Achievements

鉛同位体は年代測定を行うツールとして、宇宙地球化学のみならず考古学等の種々の分野の研究にも広く利用されている。隕石等の地球外試料や歴史的遺構等の希少性の高い試料等、限られた微量試料を用いて分析を行う必要がある試料は少なくない。本研究で確立した極微量鉛の高精度同位体分析手法は、分析に用いる試料量が限られた試料の分析へと適用することにより、これらの試料のより高精度な年代分析を可能にすることが期待できる。

Report

(6 results)
  • 2022 Annual Research Report   Final Research Report ( PDF )
  • 2021 Research-status Report
  • 2020 Research-status Report
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (6 results)

All 2023 2022 2020 2019 2018

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (5 results) (of which Int'l Joint Research: 1 results,  Invited: 2 results)

  • [Journal Article] Historical changes of 236U/238U and 235U/238U isotopic ratios in Tokyo Bay from the 1960s to the 2000s2022

    • Author(s)
      Yoshida Ami、Shikimori Junko、Ohno Takeshi、Ijichi Yuta、Fukami Yusuke、Sakata Masahiro、Hirata Takafumi
    • Journal Title

      Journal of Environmental Radioactivity

      Volume: 255 Pages: 107011-107011

    • DOI

      10.1016/j.jenvrad.2022.107011

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] 核スピンおよび分子の対称性に起因する非質量依存同位体分別の基本原理と地球化学への応用2023

    • Author(s)
      深海雄介
    • Organizer
      第20回同位体科学研究会
    • Related Report
      2022 Annual Research Report
    • Invited
  • [Presentation] 10^13Ω抵抗付増幅器を使用したTE-DS-TIMSによる極微量鉛同位体分析における時定数補正について2020

    • Author(s)
      深海雄介、飛田南斗、横山哲也、鈴木勝彦
    • Organizer
      日本地球化学会第67回オンライン年会
    • Related Report
      2020 Research-status Report
  • [Presentation] Lead Isotope Analysis for Picogram Size Samples by TE-DS-TIMS using Amplifier equipped with 1013 Ohm Resistor2020

    • Author(s)
      Y. Fukami, M. Tobita, T. Yokoyama, K. Suzuki
    • Organizer
      Goldschmidt Virtual 2020
    • Related Report
      2020 Research-status Report
    • Int'l Joint Research
  • [Presentation] 1013Ω抵抗付増幅器を使用したTE-DS-TIMSによる極微量鉛同位体分析手法の開発2019

    • Author(s)
      深海雄介、飛田南斗、横山哲也、鈴木勝彦
    • Organizer
      2019年度日本地球化学会第66回年会
    • Related Report
      2019 Research-status Report
  • [Presentation] 宇宙地球化学における高精度鉛同位体分析手法2018

    • Author(s)
      深海雄介、飛田南斗、横山哲也、森脇涼太、臼井寛裕
    • Organizer
      NINS分野融合型共同研究ワークショップ『量子ビームを用いた次世代非破壊分析技術とその応用 惑星物質科学との可能性』
    • Related Report
      2018 Research-status Report
    • Invited

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Published: 2018-04-23   Modified: 2024-01-30  

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