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New stage of astromaterial microanalysis with high-resolution X-ray spectrosocopy

Research Project

Project/Area Number 18K18794
Research Category

Grant-in-Aid for Challenging Research (Exploratory)

Allocation TypeMulti-year Fund
Review Section Medium-sized Section 17:Earth and planetary science and related fields
Research InstitutionNational Astronomical Observatory of Japan (2020)
Japan Aerospace EXploration Agency (2018-2019)

Principal Investigator

Mitsuda Kazuhisa  国立天文台, 先端技術センター, 特任教授 (80183961)

Co-Investigator(Kenkyū-buntansha) 野口 高明  九州大学, 基幹教育院, 教授 (40222195)
Project Period (FY) 2018-06-29 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2020: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2019: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2018: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Keywords宇宙物質 / 元素微量分析 / 透過型電子顕微鏡 / EDS / 超高エネルギー分解能 / X線マイクロカロリメータ / 超高エネルギー分解能X線分光 / 宇宙物質微量分析 / STEM-TES
Outline of Final Research Achievements

We developed a novel detector fabrication process in which energy resolution in a low energy range below about 1 keV is improved. We fabricated a new detector in house and validated the ability with experiments. The new detector can well separate low-energy emission lines from continuum, which is impossible with conventional semiconductor detectors. Using standard samples of minerals, we investigated damages of samples imposed by Scanning Transmission Electron Microscope with TES measurements. We confirmed that the effect of damage on the spectral measurements is negligibly small as far as the measurements were done within usual measurement time. We also investigated the stability of detector calibration data and the response function on time scale of a few days. We established the calibration strategy based on the results.

Academic Significance and Societal Importance of the Research Achievements

TES型X線マイクロカロリメータアレイ検出器は,従来の半導体検出器に比べると50倍程度優れたエネルギー分解能を持ち,物質分析への応用も期待されている。しかし,検出効率や最大計測率等の制限からが高い分解能を得るには注意が必要である。また性能の時間変化も懸念される。本研究は,今後重要になると予想されるボロンから酸素のK線を含む低エネルギー帯におけるエネルギー分解能を,10keVまでの高エネルギー帯の性能を犠牲にせずに高めることに成功し,計測による試料へのダメージを含めた実分析に向けた知見を取得した。本研究成果により,超高エネルギー分解能のX線マイクロ解析の実利用への道が拓くことが期待される。

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (7 results)

All 2021 2020 2019 2018

All Journal Article (2 results) (of which Peer Reviewed: 2 results) Presentation (5 results) (of which Int'l Joint Research: 2 results)

  • [Journal Article] A Concept Design of TES X-ray Microcalorimeter Array with Different Thickness Absorber Toward the Observation from 50 eV to 15 keV for STEM-EDS2020

    • Author(s)
      Hayashi, T, Muramatsu, H., Konno, R., Yamasaki, NY., Mitsuda, K., Takano, A., Maehata, K.,, Hara, T.
    • Journal Title

      JOURNAL OF LOW TEMPERATURE PHYSICS

      Volume: 199 Issue: 3-4 Pages: 908-915

    • DOI

      10.1007/s10909-019-02326-z

    • Related Report
      2019 Research-status Report
    • Peer Reviewed
  • [Journal Article] Construction of response function of TES X-ray microcalorimeter for STEM-EDS2019

    • Author(s)
      Tasuku Hayashi, Haruka Muramatsu, Keisei Maehisa, Noriko Y. Yamasaki, Kazuhisa Mitsuda, Keisuke Maehata and Toru Hara
    • Journal Title

      IEEE Transactions on Applied Superconductivity

      Volume: Vol.29 Issue 5 Issue: 5 Pages: 1-4

    • DOI

      10.1109/tasc.2019.2902304

    • NAID

      130008148508

    • Related Report
      2018 Research-status Report
    • Peer Reviewed
  • [Presentation] サブマイクロスケールでの地球外物質分析を目指した広帯域での検出効率向上を可能とするTES型X線マイクロカロリメータの開発2021

    • Author(s)
      林 佑, 八木 雄大, 山崎 典子, 満田 和久, 前畑 京介, 原 徹
    • Organizer
      第68回 応用物理学会 春季学術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Development of a 64-pixel TES-EDS system towards microanalysis of astromaterials2020

    • Author(s)
      T. Hayashi, N. Y. Yamasaki, K. Mitsuda, K. Maehata, T. Hara
    • Organizer
      Applied Superconductivity Conference 2020
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] A Concept Design of TES X-ray Microcalorimeter Array with Different Thickness Absorber Toward the Observation from 50 eV to 15 keV for STEM-EDS2019

    • Author(s)
      Hayashi, T, Muramatsu, H., Konno, R., Yamasaki, NY., Mitsuda, K., Takano, A., Maehata, K.,, Hara, T.
    • Organizer
      International Workshop on Low Temperature Detectors 18
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] X線高分光分析に向けたTESカロリメータの応答関数の構築2019

    • Author(s)
      林佑, 村松はるか, 満田和久, 山崎典子, 前畑京介, 原徹
    • Organizer
      日本物理学会 第74回年次大会(2019年)
    • Related Report
      2018 Research-status Report
  • [Presentation] Development of TES X-ray Microcalorimeters for Material Analysis and Tests Towards Micro Analysis of Astromaterial2018

    • Author(s)
      K. Mitsuda
    • Organizer
      The 14th International Workshop of. High-Temperature Superconductors in High Frequency Field (HTSHFF 2018)
    • Related Report
      2018 Research-status Report

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Published: 2018-07-25   Modified: 2022-01-27  

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