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Challenge of Ductilization in Hexagonal Magnesium Based on the Platoon Concept

Research Project

Project/Area Number 18K18945
Research Category

Grant-in-Aid for Challenging Research (Exploratory)

Allocation TypeMulti-year Fund
Review Section Medium-sized Section 26:Materials engineering and related fields
Research InstitutionKyoto University

Principal Investigator

Tsuji Nobuhiro  京都大学, 工学研究科, 教授 (30263213)

Project Period (FY) 2018-06-29 – 2020-03-31
Project Status Completed (Fiscal Year 2019)
Budget Amount *help
¥6,240,000 (Direct Cost: ¥4,800,000、Indirect Cost: ¥1,440,000)
Fiscal Year 2019: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2018: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Keywords六方晶 / 粒界 / プラストン / 延性 / 塑性変形 / 加工硬化 / 変形双晶 / 粒界すべり
Outline of Final Research Achievements

We have succeeded in producing bulk nanostructured pure Mg and Mg-Zn-Zr-Ca alloy having fully recrystallized ultra fine grained structures with grain sizes ranging from several hundreds nm to 100 micrometers. In the bulk nanostructured Mg-Zn-Zr-Ca alloy, <c+a> dislocations that did not operate in conventional grain sizes were nucleated from grain boundaries, and they interacted with <a> dislocations to enhance the strain hardening of the material, leading to managing both high strength and large ductility. In case of the bulk nanostructured pure Mg, it was found for the first time that grain boundary sliding happened even during room temperature deformation. We could quantitatively explain the peculiar deformation behavior of the ultra fine grained Mg and Mg alloys in terms of the concept of "platon" we had proposed, and showed a fundamental guideline for realizing HCP Mg and Mg alloys with high strength and large tensile ductility.

Academic Significance and Societal Importance of the Research Achievements

Mgに代表される六方晶金属・合金は、軽量・高比強度などの優れた特性から構造材料としての応用が渇望されてきたが、乏しい遠征・加工性がその実用上の最大の障害となってきた。本研究は、プラストンという新しい概念に基づき、通常は活動しない変形モードを超微細粒Mgにおいて活性化し、強度と延性の両立を図ることが可能であることを実証したものである。本研究の成果は、構造材料の塑性変形に対する考え方を大きく転換するという学問的意味合いに加え、軽量金属として期待されつつも乏しい加工性が障害となっていた六方晶マグネシウム合金の構造材料としての応用可能性を拡大するという実用的・社会的観点からも、高い意義を有している。

Report

(3 results)
  • 2019 Annual Research Report   Final Research Report ( PDF )
  • 2018 Research-status Report
  • Research Products

    (30 results)

All 2020 2019 2018 Other

All Int'l Joint Research (3 results) Journal Article (11 results) (of which Int'l Joint Research: 8 results,  Peer Reviewed: 11 results,  Open Access: 3 results) Presentation (13 results) (of which Int'l Joint Research: 9 results,  Invited: 4 results) Remarks (3 results)

  • [Int'l Joint Research] 北京航空航天大学/重慶大学(中国)

    • Related Report
      2019 Annual Research Report
  • [Int'l Joint Research] デンマーク工科大学(デンマーク)

    • Related Report
      2019 Annual Research Report
  • [Int'l Joint Research] 北京航空航天大学(中国)

    • Related Report
      2018 Research-status Report
  • [Journal Article] Strategy for managing both high strength and large ductility in structural materials-sequential nucleation of different deformation modes based on a concept of plaston2020

    • Author(s)
      Tsuji Nobuhiro、Ogata Shigenobu、Inui Haruyuki、Tanaka Isao、Kishida Kyosuke、Gao Si、Mao Wenqi、Bai Yu、Zheng Ruixiao、Du Jun-Ping
    • Journal Title

      Scripta Materialia

      Volume: 181 Pages: 35-42

    • DOI

      10.1016/j.scriptamat.2020.02.001

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Formation Mechanism of Ultrafine Grained Microstructures: Various Possibilities for Fabricating Bulk Nanostructured Metals and Alloys2019

    • Author(s)
      Tsuji Nobuhiro、Gholizadeh Reza、Ueji Rintaro、Kamikawa Naoya、Zhao Lijia、Tian Yanzhong、Bai Yu、Shibata Akinobu
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 60 Issue: 8 Pages: 1518-1532

    • DOI

      10.2320/matertrans.MF201936

    • NAID

      130007683601

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2019-08-01
    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Change of Deformation Mechanisms Leading to High Strength and Large Ductility in Mg-Zn-Zr-Ca Alloy with Fully Recrystallized Ultrafine Grained Microstructures2019

    • Author(s)
      Zheng Ruixiao、Bhattacharjee Tilak、Gao Si、Gong Wu、Shibata Akinobu、Sasaki Taisuke、Hono Kazuhiro、Tsuji Nobuhiro
    • Journal Title

      Scientific Reports

      Volume: 9 Issue: 1 Pages: 11702-11702

    • DOI

      10.1038/s41598-019-48271-5

    • NAID

      120007006236

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] 圧延工程の違いによる素材の性質の変化とその影響:巨大ひずみ加工を中心に2019

    • Author(s)
      辻 伸泰
    • Journal Title

      砥粒加工学会誌

      Volume: 63 Pages: 456-459

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Bi-lamellar microstructure in Ti?6Al?4V: Microstructure evolution and mechanical properties2019

    • Author(s)
      Chong Yan、Bhattacharjee Tilak、Tsuji Nobuhiro
    • Journal Title

      Materials Science and Engineering: A

      Volume: 762 Pages: 138077-138077

    • DOI

      10.1016/j.msea.2019.138077

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Yielding nature and Hall-Petch relationships in Ti-6Al-4V alloy with fully equiaxed and bimodal microstructures2019

    • Author(s)
      Chong Yan、Deng Guanyu、Gao Si、Yi Jangho、Shibata Akinobu、Tsuji Nobuhiro
    • Journal Title

      Scripta Materialia

      Volume: 172 Pages: 77-82

    • DOI

      10.1016/j.scriptamat.2019.07.015

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] On the strain hardening abilities of α+β titanium alloys: The roles of strain partitioning and interface length density2019

    • Author(s)
      Chong Yan、Deng Guanyu、Yi Jangho、Shibata Akinobu、Tsuji Nobuhiro
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 811 Pages: 152040-152040

    • DOI

      10.1016/j.jallcom.2019.152040

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Achieving bi-lamellar microstructure with both high tensile strength and large ductility in Ti?6Al?4V alloy by novel thermomechanical processing2019

    • Author(s)
      Chong Yan、Bhattacharjee Tilak、Yi Jangho、Zhao Shiteng、Tsuji Nobuhiro
    • Journal Title

      Materialia

      Volume: 8 Pages: 100479-100479

    • DOI

      10.1016/j.mtla.2019.100479

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Factors determining room temperature mechanical properties of bimodal microstructures in Ti-6Al-4V alloy2018

    • Author(s)
      Chong Yan、Bhattacharjee Tilak、Park Myeong-Heom、Shibata Akinobu、Tsuji Nobuhiro
    • Journal Title

      Materials Science and Engineering: A

      Volume: 730 Pages: 217-222

    • DOI

      10.1016/j.msea.2018.06.019

    • Related Report
      2018 Research-status Report
    • Peer Reviewed
  • [Journal Article] Deformation behavior of as-cast and as-extruded Mg97Zn1Y2 alloys during compression, as tracked by in situ neutron diffraction2018

    • Author(s)
      Gong Wu、Aizawa Kazuya、Harjo Stefanus、Zheng Ruixiao、Kawasaki Takuro、Abe Jun、Kamiyama Takashi、Tsuji Nobuhiro
    • Journal Title

      International Journal of Plasticity

      Volume: 111 Pages: 288-306

    • DOI

      10.1016/j.ijplas.2018.08.001

    • Related Report
      2018 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effect of Grain Size on Mechanical Properties of Mg-0.3at.%Y Dilute Alloy2018

    • Author(s)
      Zheng Rui Xiao、Kawarada Ichiro、Gong Wu、Shibata Akinobu、Somekawa Hidetoshi、Ogata Shigenobu、Tsuji Nobuhiro
    • Journal Title

      Materials Science Forum

      Volume: 941 Pages: 790-795

    • DOI

      10.4028/www.scientific.net/msf.941.790

    • Related Report
      2018 Research-status Report
    • Peer Reviewed
  • [Presentation] Effect of Grain Size on Mechanical Properties of Mg-0.3at.%Y Dilute Alloy2019

    • Author(s)
      Ruixiao Zheng, Chaoli Ma, Nobuhiro Tsuji
    • Organizer
      10th Pacific Rim International Conference on Advance Materials and Processing (PRICM 10)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of Temperature on Deformation Behaviors of Mg-0.1at.%Y Alloy Having Various Grain Sizes2019

    • Author(s)
      Kazuhiro Oki, Akinobu Shibata, Nobuhiro Tsuji, Ruixiao Zheng
    • Organizer
      10th Pacific Rim International Conference on Advance Materials and Processing (PRICM 10)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 種々の粒径を有する希薄Mg-Y二元系合金の低温力学特性2019

    • Author(s)
      沖 和洋,鄭 瑞暁,柴田 曉伸,辻 伸泰
    • Organizer
      日本金属学会 / 鉄鋼協会2019秋季講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 超微細粒純Mg及び希薄Mg-Y二元系合金の低温力学特性2019

    • Author(s)
      沖和洋, 鄭瑞暁, 柴田曉伸, 辻伸泰
    • Organizer
      軽金属学会 若手研究者・院生による研究発表会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Fully Recrystallized Bulk Nanostructured Metals for Managing Both High Strength and Large Ductility2019

    • Author(s)
      Nobuhiro Tsuji
    • Organizer
      Xi’an Jiaotong University, Frontier Institute of Science and Technology (FIST)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Relationship between Local Heterogeneous Deformation Behaviors and Global Deformation of Materials2019

    • Author(s)
      Nobuhiro TSUJI, Myeong-Heom PARK, Si GAO, Yu BAI, Wenqi MAO, Akinobu SHIBATA
    • Organizer
      中国科学院・金属研究所(IMR, CAS)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Relationship between Local Heterogeneous Deformation Behaviors and Global Deformation of Materials2019

    • Author(s)
      Nobuhiro TSUJI, Myeong-Heom PARK, Si GAO, Yu BAI, Wenqi MAO, Akinobu SHIBATA
    • Organizer
      Northeastern University(中国・東北大学)、School of Materials Science & Engineering
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 種々の粒径を有する希薄Mg-Y 二元系合金の低温力学特性2019

    • Author(s)
      ○沖 和洋,鄭 瑞暁,柴田 曉伸,辻 伸泰
    • Organizer
      日本金属学会2019春季講演大会
    • Related Report
      2018 Research-status Report
  • [Presentation] Effect of grain size on mechanical properties of Mg-0.3at.%Y dilute alloy2018

    • Author(s)
      ○Ruixiao Zheng, Ichiro Kawarada, Gong Wu, Akinobu Shibata, Hidetoshi Somekawa, Shigenobu Ogata, Nobuhiro Tsuji
    • Organizer
      10th International Conference on Processing & Manufacturing of Advanced Materials (THERMEC 2018)
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research
  • [Presentation] Fabricating Ti-1.0%Fe with Ultrafine Grained Microstructures by Thermomechanical Processes2018

    • Author(s)
      ○Yuan Zhang, Deng Guanyu, Chong Yan, Bai Yu, Shibata Akinobu, Tsuji Nobuhiro
    • Organizer
      10th International Conference on Processing & Manufacturing of Advanced Materials (THERMEC 2018)
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research
  • [Presentation] Orientation Dependence of Deformation Behaviors in Cyclic Deformation of AZ31 Magnesium Alloy Investigated by In-Situ Neutron Diffraction, EBSD and TEM2018

    • Author(s)
      ○Wu Gong, Ruixiao Zheng, Stefanus Harjo, Kazuya Aizawa, Akinobu Shibata, Nobuhiro Tsuji
    • Organizer
      18th International Conference on the Strength of Materials (ICSMA18)
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research
  • [Presentation] Investigation into Microstructure and Mechanical Properties of Titanium Processed by Severe Plastic Deformation2018

    • Author(s)
      ◯Guanyu Deng, Tilak Bhattacharjee, Yan Chong, Yu Bai, Akinobu Shibata, Nobuhiro Tsuji
    • Organizer
      The 9th Int. Con. on Advanced Materials Processing (ICAMP 9)
    • Related Report
      2018 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Investigation on the microstructure and mechanical properties of Ti-1.0 Fe alloy with equiaxed α+β microstructures2018

    • Author(s)
      ○Y. Chong,R. Zheng,N. Tsuji
    • Organizer
      日本金属学会/日本鉄鋼協会共同セッション2018秋期講演大会
    • Related Report
      2018 Research-status Report
  • [Remarks] 辻研究室のホームページ

    • URL

      http://www.tsujilab.mtl.kyoto-u.ac.jp

    • Related Report
      2019 Annual Research Report
  • [Remarks] 高強度・高延性マグネシウム合金を実現 -結晶粒サイズのナノ化による変形モード制御-

    • URL

      http://www.kyoto-u.ac.jp/ja/research/research_results/2019/190812_1.html

    • Related Report
      2019 Annual Research Report
  • [Remarks] 京都大学 辻研究室

    • URL

      http://www.tsujilab.mtl.kyoto-u.ac.jp/

    • Related Report
      2018 Research-status Report

URL: 

Published: 2018-07-25   Modified: 2021-02-19  

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