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Anisotropic thick film magnets prepared by high-speed PLD method and their application to an advanced and small motor

Research Project

Project/Area Number 19360147
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Electronic materials/Electric materials
Research InstitutionNagasaki University

Principal Investigator

NAKANO Masaki  Nagasaki University, 工学部, 准教授 (20274623)

Co-Investigator(Kenkyū-buntansha) 福永 博俊  長崎大学, 工学部, 教授 (10136533)
Project Period (FY) 2007 – 2009
Project Status Completed (Fiscal Year 2009)
Budget Amount *help
¥18,980,000 (Direct Cost: ¥14,600,000、Indirect Cost: ¥4,380,000)
Fiscal Year 2009: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2008: ¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2007: ¥13,910,000 (Direct Cost: ¥10,700,000、Indirect Cost: ¥3,210,000)
Keywords電気 / 電子材料 / 磁性 / PLD法 / 厚膜磁石 / 高速成膜 / エネルギー積 / マイクロモータ / ドロップレット / YAGレーザ / 異方性磁石膜 / 保磁力 / 添加物 / 小型モータ / 高成膜速度 / 基板加熱 / 異方性 / ミリサイズモータ
Research Abstract

In the study, an improvement in magnetic properties of anisotropic and isotropic Nd-Fe-B film magnets was carried out by using additives. In addition, several applications comprising the films were investigated. The obtained results are as followed.
(1) Anisotropic Nd-Fe-B films
An obtained film prepared from the Nd_<2.4>Fe_<14>B+Ga_<0.5at.%> target had the coercivity, remanence and (BH)_<max> values of approximately 850 kA/m, 0.95 T and 150 kJ/m^3, respectively. These magnetic properties are superior compared with those for the anisotropic PLD-made Nd-Fe-B films without additives. We also confirmed that the intensities of a X-ray diffraction peaks corresponding to the c-planes such as (004), (006) and (008) of the film were stronger than those of the additive-free film.
(2) Isotropic film magnets
PLD-made isotroipic Nd-Fe-B thick film magnets were prepared from targets with Zr, Nb and Ga, respectively. They were crystallized by two annealing methods of conventional annealing (CA) and pulse annealing (PA), respectively. In the case of using Nd_<2.6>Fe_<14>B targets, 0.5 at.% Zr, Nb and Ga addition increased the coercivity of the film by approximately 100~300 kA/m compared with that of additive-free samples prepared by CA method. We also confirmed further increase in coercivity of the film by PA method and the obtained film prepared from a Nd_<2.6>Fe_<14>B+Ga_<0.5at.%> target had large coercivity of approximately 1700 kA/m.
(3) Applications
We applied the above-mentioned films to a friction-drive motor and a milli-size motor.

Report

(4 results)
  • 2009 Annual Research Report   Final Research Report ( PDF )
  • 2008 Annual Research Report
  • 2007 Annual Research Report
  • Research Products

    (35 results)

All 2010 2009 2008 2007 Other

All Journal Article (18 results) (of which Peer Reviewed: 12 results) Presentation (13 results) Remarks (3 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Yamashita, Anisotropic Nd-Fe-B thick film magnets prepared on various substrates2010

    • Author(s)
      M. Nakano, S. Sato, T. Yanai, H. Fukunaga, F. Yamashita
    • Journal Title

      Journal of Physics: Conference Series

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Preparation of ring-shaped composite bonded magnets with continuously controlled anisotropy distribution for internal space2010

    • Author(s)
      F. Yamashita, O. Yamada, S. Ohya, O. Kobayashi, M. Nakano, H. Fukunaga
    • Journal Title

      Journal of Physics: Conference Series

    • NAID

      120006984785

    • Related Report
      2009 Final Research Report
  • [Journal Article] PLD-fabricated anisotropic Nd-Fe-B thick films with Ga additive2009

    • Author(s)
      M. Nakano, S. Tsutsumi, T. Yanai, H. Fukunaga, F. Yamashita
    • Journal Title

      Journal of Applied Physics vol.105,No.7

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Change in the direction of anisotropy in PLD-fabricated Sm-Co thick film magnets2009

    • Author(s)
      M. Nakano, K. Yamaguchi, T. Yanai, F. Yamashita, H. Fukunaga
    • Journal Title

      Journal of Applied Physics vol.105,No.7

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] PLD-fabricated anisotropic Nd-Fe-B thick films with Ga additive2009

    • Author(s)
      M.Nakano, S.Tsutsumi, T.Yanai, F.Yamashita, H.Fukunaga
    • Journal Title

      Journal of Applied Physics 105-7

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Change in the direction of anisotropy in PLD-fabricated Sm-Co thick film magnets2009

    • Author(s)
      M.Nakano, K.Yamaguchi, T.Yanai, F.Yamashita, H.Fukunaga
    • Journal Title

      Journal of Applied Physics 105-7

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Anisotropic properties in Fe-Pt thick film magnets2009

    • Author(s)
      M.Nakano, S.Shibata, T.Yanai, H.Fukunaga
    • Journal Title

      Journal of Applied Physics 105-7

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] PLD-fabricated anisotropic Nd-Fe-B thick films with Ga additive2009

    • Author(s)
      M. Nakano, S. Tsutsumi, T. Yanai, H. Fukunaga, F. Yamashita
    • Journal Title

      J. Appl. Phys. VOl. 105, No. 7

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Magnetic Properties of Multi-Layered Nanocomposite Film-Magnets2008

    • Author(s)
      H. Fukunaga, H. Nakayama, M. Nakano, F. Yamashita, Y. Okada, K. Kawamura, H. Murakami, M. Ogushi, T. Yanai
    • Journal Title

      Proceedings of the 10th Joint Symposium of Nagasaki University and Cheju National University on Science and Technology

      Pages: 11-14

    • Related Report
      2009 Final Research Report
  • [Journal Article] Preparation of ring-shaped rare earth bonded magnets with continuously controlled anisotropy directions2008

    • Author(s)
      M. Nakano, H. Fukunaga
    • Journal Title

      Proceedings 20th Workshop on Rare Earth Permanent Magnets and Applications, Creta Greece

      Pages: 91-94

    • Related Report
      2009 Final Research Report
  • [Journal Article] mprovement in magnetic properties of anisotropic Nd-Fe-B film magnets2008

    • Author(s)
      M. Nakano, S. Tsutsumi, H. Takeda, T. Yanai, H. Fukuaga, F. Yamashita
    • Journal Title

      Proceedings 20th Workshop on Rare Earth Permanent Magnets and Applications, Creta Greece

      Pages: 231-232

    • Related Report
      2009 Final Research Report
  • [Journal Article] Improvement in magnetic properties of PLD-made Nd-Fe-B thick film magnets2008

    • Author(s)
      M. Nakano, H. Takeda, F. Yamashita, T. Yanai, H. Fukunaga
    • Journal Title

      IEEE Trans. Magn. vol.44,No.11

      Pages: 4199-4201

    • NAID

      120006984190

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Magnetic Properties of Multi-Layered Nanocomposite Film-Magnets2008

    • Author(s)
      H. Fukunaga, H. Nakayama, M. Nakano, T. Yanai
    • Journal Title

      Proceedings of the 10th Joint Symposium of Nagasaki University and Cheju National University on Science and Technology

      Pages: 11-14

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Preparation of ring-shaped rare earth bonded magnets with continuously controlled anisotropy directions2008

    • Author(s)
      F. Yamashita, Y. Okada, K. Kawamura, H. Murakami, M. Ogushi, M. Nakano, H. Fukunaga
    • Journal Title

      Proceedings 20^<th> Workshop on Rare Earth Permanent Magnets and Applications, Creta Greece

      Pages: 91-94

    • Related Report
      2008 Annual Research Report
  • [Journal Article] Improvement in magnetic properties of anisotropic Nd-Fe-B film magnets2008

    • Author(s)
      M. Nakano, S. Tsutsumi, H. Takeda, T. Yanai, H. Fukuaga, F. Yamashita
    • Journal Title

      Proceedings 20^<th> Workshop on Rare Earth Permanent Magnets and Applications, Creta Greece

      Pages: 231-232

    • Related Report
      2008 Annual Research Report
  • [Journal Article] Improvement in magnetic properties of PLD-made Nd-Fe-B thick film magnets2008

    • Author(s)
      M. Nakano, H. Takeda, F. Yamashita, T. Yanai, H. Fukunaga
    • Journal Title

      IEEE Trans. Magn. Vol. 44, No. 11

      Pages: 4199-4201

    • NAID

      120006984190

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microstructure of Anisotropic Nd-Fe-B Film Magnets Prepared by Pulsed Laser Deposition2007

    • Author(s)
      M Ishimaru, M. Itakura, N. Kuwano, S. Sato, M. Nakano, H. Fukunaga
    • Journal Title

      Materials Science Forum vol.561-565

      Pages: 1131-1134

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Microstructure of Anisotropic Nd-Fe-B Film Magnets Preared by Pulsed aser Deposition2007

    • Author(s)
      M Ishimaru, M.Itakura, N.Kuwano, S.Sato, M.Nakano, and H.Fukunaga
    • Journal Title

      Materials Science Forum 561-565

      Pages: 1131-1134

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Presentation] PLD法を用い作製したNd-Fe-B系等方性磁石膜の磁気特性と微細構造2010

    • Author(s)
      中野正基
    • Organizer
      平成22年電気学会全国大会
    • Place of Presentation
      明治大学(東京)
    • Year and Date
      2010-03-17
    • Related Report
      2009 Annual Research Report
  • [Presentation] Ga添加Nd-Fe-B系異方性厚膜磁石2009

    • Author(s)
      堤卓
    • Organizer
      日本磁気学会第33回学術講演会
    • Place of Presentation
      長崎大学(長崎)
    • Year and Date
      2009-09-12
    • Related Report
      2009 Annual Research Report
  • [Presentation] Cu添加を施した等方性Nd-Fe-B系厚膜磁石の磁気特性2009

    • Author(s)
      寺田皓祐
    • Organizer
      日本磁気学会第33回学術講演会
    • Place of Presentation
      長崎大学(長崎)
    • Year and Date
      2009-09-12
    • Related Report
      2009 Annual Research Report
  • [Presentation] 添加物を施したNd-Fe-B系磁性膜の磁気特性2009

    • Author(s)
      寺田皓祐
    • Organizer
      電気学会マグネティクス研究会
    • Place of Presentation
      宇都宮大学(栃木)
    • Year and Date
      2009-08-06
    • Related Report
      2009 Annual Research Report
  • [Presentation] Anisotropic Nd-Fe-B thick film magnets prepared on various substrates2009

    • Author(s)
      中野正基
    • Organizer
      ICM(International Conference on Magnetics)
    • Place of Presentation
      カールスルーエ(ドイツ)
    • Year and Date
      2009-07-27
    • Related Report
      2009 Annual Research Report
  • [Presentation] Dyコーティングを施したNd-Fe-B系厚膜磁石2009

    • Author(s)
      伊東啓太
    • Organizer
      平成21年電気学会全国大会
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2009-03-19
    • Related Report
      2009 Annual Research Report
  • [Presentation] Anisotropic Nd-Fe-B-(Ga) Thick Film Magnets2008

    • Author(s)
      M. Nakano
    • Organizer
      The IUMRS International Conference in Asia 2008
    • Place of Presentation
      名古屋(愛知)
    • Year and Date
      2008-12-11
    • Related Report
      2008 Annual Research Report
  • [Presentation] Improvement in magnetic properties of anisotropic Nd-Fe-B film magnets2008

    • Author(s)
      M. Nakano
    • Organizer
      20th Workshop on Rare Earth Permanent Magnets
    • Place of Presentation
      クノソス(ギリシヤ)
    • Year and Date
      2008-09-10
    • Related Report
      2008 Annual Research Report
  • [Presentation] Anisotropic Nd-Fe-B thick film magnets with Ga additive2008

    • Author(s)
      M. Nakano
    • Organizer
      Moscow International Symposium on Magnetism
    • Place of Presentation
      モスクワ(ロシア)
    • Year and Date
      2008-06-21
    • Related Report
      2008 Annual Research Report
  • [Presentation] Nd-Fe-B 系厚膜磁石の保磁力に及ぼす添加物の影響2008

    • Author(s)
      武田 浩之, 柳井 武志, 中野 正基, 福永 博俊, 山下 文敏
    • Organizer
      日本金属学会2008年春季大会
    • Place of Presentation
      武蔵工業大学(東京都)
    • Year and Date
      2008-03-27
    • Related Report
      2007 Annual Research Report
  • [Presentation] 異方性厚膜磁石の磁気特性向上に関する検討2008

    • Author(s)
      武田 浩之, 柳井 武志, 中野 正基, 福永 博俊, 山下 文敏
    • Organizer
      平成20年 電気学会全国大会
    • Place of Presentation
      福岡工業大学(福岡県)
    • Year and Date
      2008-03-19
    • Related Report
      2007 Annual Research Report
  • [Presentation] Nd-Fe-B磁石膜の磁気特性改善に関する検討2007

    • Author(s)
      武田 浩之, 柳井 武志, 中野 正基, 福永 博俊, 山下 文敏
    • Organizer
      平成19年度粉体粉末冶金協会秋季大会
    • Place of Presentation
      京都工芸繊維大学 (京都)
    • Year and Date
      2007-11-20
    • Related Report
      2007 Annual Research Report
  • [Presentation] PLD-fabricated Nd-Fe-B thick films with additives2007

    • Author(s)
      H.Takeda, T.Yanai, M.Nakano, F.Yamashita, H.Fukunaga
    • Organizer
      52nd Annual Conference on Magnetism and Magnetic Materials
    • Place of Presentation
      Tampa,Florida,USA
    • Year and Date
      2007-11-09
    • Related Report
      2007 Annual Research Report
  • [Remarks]

    • URL

      http://www.eee.nagasaki-u.ac.jp/~magnet/index.html

    • Related Report
      2009 Final Research Report
  • [Remarks]

    • URL

      http://www.eee.nagasaki-u.ac.jp/~magnet/index.html

    • Related Report
      2009 Annual Research Report
  • [Remarks]

    • URL

      http://www.eee.nagasaki-u.ac.jp/~magnet/paper/frame_paper.htm

    • Related Report
      2007 Annual Research Report
  • [Patent(Industrial Property Rights)] Nd-Fe-B系磁石,及びその製造方法2009

    • Inventor(s)
      中野正基, 福永博俊
    • Industrial Property Rights Holder
      長崎大学
    • Industrial Property Number
      2009-152023
    • Filing Date
      2009-06-26
    • Related Report
      2009 Final Research Report

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Published: 2007-04-01   Modified: 2016-04-21  

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