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Application of X-ray Photoelectron Spectroscopy to Characterization of Nano-and Subnano-particles Embedded in Dielectric Matrices

Research Project

Project/Area Number 19510116
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Nanomaterials/Nanobioscience
Research InstitutionKyoto Institute of Technology

Principal Investigator

TAKAHIRO Katsumi  Kyoto Institute of Technology, 工芸科学研究科, 教授 (80236348)

Co-Investigator(Kenkyū-buntansha) NAGATA Shinji  東北大学, 金属材料研究所, 准教授 (40208012)
Co-Investigator(Renkei-kenkyūsha) NAGATA Shinji  東北大学, 金属材料研究所, 准教授 (40208012)
Project Period (FY) 2007 – 2008
Project Status Completed (Fiscal Year 2008)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2008: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2007: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Keywordsナノ材料 / 光電子分光 / イオン注入 / 量子ビーム / サイズ評価 / イオン照射 / 状態分析 / ナノ粒子 / サブナノ粒子
Research Abstract

本研究では, X線光電子分光法を用いて, マトリックス中に埋め込まれたナノメートルサイズさらにはサブナノメートルサイズの超微粒子のサイズ評価と存在状態の分析を目指して, 基礎研究を行った。まず, 基板上にAuナノ粒子を生成し, 広い粒子サイズ範囲において, サイズと価電子帯幅の関係を見出した。次に, 得られた関係を用いて, マトリックス中に埋め込まれたAuクラスター・超微粒子のサイズ評価を行い, 透過型電子顕微鏡の結果と良く一致することを確認し, 本手法の有用性を示すことができた。

Report

(3 results)
  • 2008 Annual Research Report   Final Research Report ( PDF )
  • 2007 Annual Research Report
  • Research Products

    (21 results)

All 2009 2008 2007

All Journal Article (4 results) (of which Peer Reviewed: 4 results) Presentation (17 results)

  • [Journal Article] Application of X-ray Photoelectron Spectroscopy to Characterization of Au Nanoparticles Formed by Ion Implantation into SiO_22009

    • Author(s)
      K. Takahiro, S. Oizumi, K. Morimoto, K. Kawatsura, T. Isshiki, K. Nishio, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Journal Title

      Applied Surface Science (掲載確定)

    • Related Report
      2008 Final Research Report
    • Peer Reviewed
  • [Journal Article] Ion-induce Self-organized Ripple Patterns on Graphite and Diamond Surfaces2009

    • Author(s)
      K. Takahiro, K. Ozaki, K. Kawatsura, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Journal Title

      Applied Surface Science (掲載確定)

    • Related Report
      2008 Final Research Report
    • Peer Reviewed
  • [Journal Article] Application of X-ray Photoelectron Spectroscopy to Characterization of Au Nanoparticles Formed by Ion Implantation into SiO_22009

    • Author(s)
      高廣克己, 他
    • Journal Title

      Applied Surface Science (掲載確定)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ion-induced Self-organized Ripple Patterns on Graphite and Diamond Surfaces2009

    • Author(s)
      高廣克己, 他
    • Journal Title

      Applied Surface Science (掲載確定)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] イオン注入によるAuナノ粒子生成とX線光電子分光を用いた粒径測定2009

    • Author(s)
      高廣克己, 森本圭一, 大泉信之助, 一色俊之, 西尾弘司, 永田晋二
    • Organizer
      第56回応用物理学関係連合講演会
    • Place of Presentation
      筑波大学(茨城県つくば市)
    • Year and Date
      2009-03-30
    • Related Report
      2008 Final Research Report
  • [Presentation] イオン照射炭素表面上へのAuおよびPtナノ粒子生成2009

    • Author(s)
      森本圭一, 安田賢司, 高廣克己, 永田晋二
    • Organizer
      第56回応用物理学関係連合講演会
    • Place of Presentation
      筑波大学(茨城県つくば市)
    • Year and Date
      2009-03-30
    • Related Report
      2008 Final Research Report
  • [Presentation] イオン照射炭素表面上へのAuおよびPtナノ粒子生成2009

    • Author(s)
      森本圭一, 高廣克己, 他
    • Organizer
      第56回応用物理学関係連合講0330
    • Place of Presentation
      茨城県つくば市
    • Year and Date
      2009-03-30
    • Related Report
      2008 Annual Research Report
  • [Presentation] イオン注入によるAuナノ粒子生成とX線光電子分光を用いた粒径測定2009

    • Author(s)
      高廣克己, 他
    • Organizer
      第56回応用物理学関係連合講演会
    • Place of Presentation
      茨城県つくば市
    • Year and Date
      2009-03-30
    • Related Report
      2008 Annual Research Report
  • [Presentation] XPS Study on Au and Pt Clusters Deposited on Graphite with and without Ion Irradiation2008

    • Author(s)
      K. Morimoto, S. Yasuda, K. Takahiro, S. Nagata
    • Organizer
      International Symposium on Surface Science and Nanotechnology
    • Place of Presentation
      早稲田大学(東京都新宿区)
    • Year and Date
      2008-11-11
    • Related Report
      2008 Final Research Report
  • [Presentation] Auger Parameter Analysis of Ag and Cu Nanoparticles Formed by Sputter Deposition on Non-conductive Substrates2008

    • Author(s)
      Y. Minakuchi, K. Takahiro, F. Nishiyama, S. Yamamoto, K. Narumi, H. Naramoto
    • Organizer
      International Symposium on Surface Science and Nanotechnology
    • Place of Presentation
      早稲田大学(東京都新宿区)
    • Year and Date
      2008-11-11
    • Related Report
      2008 Final Research Report
  • [Presentation] Auger Parameter Analysis of Ag and Cu Nanoparticles Formed by Sputter Deposition on Non-conductive Substrates2008

    • Author(s)
      水口友貴, 高廣克己, 他
    • Organizer
      International Symposium on Surface Science and Nanoechnology
    • Place of Presentation
      東京都新宿区
    • Year and Date
      2008-11-11
    • Related Report
      2008 Annual Research Report
  • [Presentation] XPS Study on Au and Pt Clusters Deposited on Gr aphite with and without Ion Irradiation2008

    • Author(s)
      森本圭一, 高廣克己, 他
    • Organizer
      International Symposium on Surface Science and Nanotechnology
    • Place of Presentation
      東京都新宿区
    • Year and Date
      2008-11-11
    • Related Report
      2008 Annual Research Report
  • [Presentation] Ion-induce Self-organized Ripple Patterns on Graphite and Diamond Surfaces2008

    • Author(s)
      K. Takahiro, K. Ozaki, K. Kawatsura, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Organizer
      4th Vacuum and Surface Sciences Conference of Asia and Australia(VASSCAA-4)
    • Place of Presentation
      島根県松江市
    • Year and Date
      2008-10-28
    • Related Report
      2008 Final Research Report
  • [Presentation] Application of X-ray Photoelectron Spectroscopy to Characterization of Au Nanoparticles Formed by Ion Implantation into SiO_22008

    • Author(s)
      K. Takahiro, S. Oizumi, K. Morimoto, K. Kawatsura, T. Isshiki, K. Nishio, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Organizer
      4th Vacuum and Surface Sciences Conference of Asia and Australia(VASSCAA-4)
    • Place of Presentation
      島根県松江市
    • Year and Date
      2008-10-28
    • Related Report
      2008 Final Research Report
  • [Presentation] Application of X-ray Photoelectron Spectroscopy to Characterization of Au Nanoparticles Formed by Ion Implantation into SiO_22008

    • Author(s)
      高廣克己, 他
    • Organizer
      4th Vacuum and Surface Sciences Conference of Asia and Australia (VASSCAA-4)
    • Place of Presentation
      島根県松江市
    • Year and Date
      2008-10-28
    • Related Report
      2008 Annual Research Report
  • [Presentation] Ion-induced Self-organized Ripple Patterns on Graphite and Diamond Surfaces2008

    • Author(s)
      高廣克己, 他
    • Organizer
      4th Vacuum and Surface Sciences Conference of Asia and Australia (VASSCAA-4)
    • Place of Presentation
      島根県松江市
    • Year and Date
      2008-10-28
    • Related Report
      2008 Annual Research Report
  • [Presentation] Ripple Formation on Graphite and Diamond Surfaces by Ion Irradiation2007

    • Author(s)
      K. Takahiro, K. Ozaki, K. Kawatsura, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Organizer
      第18回日本MRS学術シンポジウム, 国際セッション
    • Place of Presentation
      日本大学駿河台キャンパス(東京都千代田区)
    • Year and Date
      2007-12-09
    • Related Report
      2008 Final Research Report
  • [Presentation] Ripple Formation on Graphite and Diamond Surfaces by Ion Irradiation2007

    • Author(s)
      高廣克己, 他
    • Organizer
      第18回日本MRS学術シンポジウム国際セッション
    • Place of Presentation
      日本大学駿河台キャンパス(東京都千代田区)
    • Year and Date
      2007-12-09
    • Related Report
      2007 Annual Research Report
  • [Presentation] Ion-induced Self-organized Ripple Patterns on Graphite and Diamond Surfaces2007

    • Author(s)
      K. Takahiro, K. Ozaki, K. Kawatsura, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Organizer
      9^<th> Int. Conf. on Atomically Controlled Surfaces, Interfaces and Nanostructures
    • Place of Presentation
      東京大学駒場キャンパス(東京都目黒区)
    • Year and Date
      2007-11-14
    • Related Report
      2008 Final Research Report 2007 Annual Research Report
  • [Presentation] Application of X-ray Photoelectron Spectroscopy Characterization of Au Nanoparticles Formed by Ion Implantation into Al_2O_3 and SiO_22007

    • Author(s)
      K. Takahiro, S. Oizumi, K. Kawatsura, T. Isshiki, K. Nishio, S. Nagata, S. Yamamoto, K. Narumi, H. Naramoto
    • Organizer
      9^<th> Int. Conf. on Atomically Controlled Surfaces, Interfaces and Nanostructures
    • Place of Presentation
      東京大学駒場キャンパス(東京都目黒区)
    • Year and Date
      2007-11-14
    • Related Report
      2008 Final Research Report
  • [Presentation] Application of X-ray Photoelectron Spectroscopy to Characterization of Au Nanoparticles Formed by Ion Implantation into Al_2O_3 and SiO_22007

    • Author(s)
      高廣克己, 他
    • Organizer
      9^<th> Int. Conf. on Atomically Controlled Surfaces, Interfaces and Nanostructures
    • Place of Presentation
      東京大学駒場キャンパス(東京都目黒区)
    • Year and Date
      2007-11-14
    • Related Report
      2007 Annual Research Report

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Published: 2007-04-01   Modified: 2016-04-21  

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