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4D evaluation of damage in hetero-structured materials with high performance by multi-scale measurement

Research Project

Project/Area Number 19H02024
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Review Section Basic Section 18010:Mechanics of materials and materials-related
Research InstitutionShizuoka University

Principal Investigator

Kikuchi Shoichi  静岡大学, 工学部, 准教授 (80581579)

Co-Investigator(Kenkyū-buntansha) 岩田 太  静岡大学, 電子工学研究所, 教授 (30262794)
藤井 朋之  静岡大学, 工学部, 准教授 (30377840)
中澤 謙太  静岡大学, 工学部, 助教 (50824520)
塩澤 大輝  神戸大学, 工学研究科, 准教授 (60379336)
Project Period (FY) 2019-04-01 – 2022-03-31
Project Status Completed (Fiscal Year 2021)
Budget Amount *help
¥17,030,000 (Direct Cost: ¥13,100,000、Indirect Cost: ¥3,930,000)
Fiscal Year 2021: ¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2020: ¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2019: ¥8,970,000 (Direct Cost: ¥6,900,000、Indirect Cost: ¥2,070,000)
Keywords粉末冶金 / 表面改質 / 金属疲労 / 光計測 / 破壊力学 / 高輝度放射光
Outline of Research at the Start

本研究では,大きさの異なるミクロ組織をマクロに周期配置させた3次元ヘテロ構造材料の高機能化メカニズムを解明する.とくに「強さ」と「しなやかさ」の両立という特異な力学特性を解明するため,ヘテロ構造材料のミクロ・マクロ変形の双方を捉えるマルチスケール計測法を構築し,3次元ヘテロ構造における材料損傷挙動の時間的変化を評価(4次元材料損傷評価)する.

Outline of Final Research Achievements

Metallic materials having a heterogeneous structure (HS), which consists of a coarse-grained structure surrounded by a network structure of fine equiaxed grains, were fabricated to achieve high strength and ductility. 4D evaluation of damage was conducted for the HS materials with high performance by multi-scale measurement.
The fatigue limit was increased by the HS design due to the grain refinement. To improve their fatigue properties, thermomechanical processing (TMP) was performed. The average size of the grains in the fine-grained structures was preferentially decreased by TMP. Applying TMP to CP titanium having a HS increased its fatigue life due to greater resistance to the initiation of fatigue crack as a result of grain refinement. In contrast, the crack growth rates for the HS material for long cracks were constantly higher, and its threshold stress intensity range were lower compared to a material with a homogenous coarse-grained structure.

Academic Significance and Societal Importance of the Research Achievements

しなやかな粗大粒組織の周りに強い微細粒組織をネットワーク状に周期配置させた「3次元ヘテロ構造材料」の特異な力学特性を,ミクロ・マクロ変形の双方を捉えるマルチスケール計測法によって明らかにした.これまでは「いかに均一かつ微細な結晶粒を作るか」が常識とされていたが,このような3次元ヘテロ構造材料の実用化によって各種機械構造物の信頼性向上が期待される.さらに,3次元ヘテロ構造材料の多機能性は機械構造物の小型軽量化にも寄与し,省エネルギー化の促進が期待される.

Report

(4 results)
  • 2021 Annual Research Report   Final Research Report ( PDF )
  • 2020 Annual Research Report
  • 2019 Annual Research Report
  • Research Products

    (49 results)

All 2022 2021 2020 2019 Other

All Journal Article (9 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 9 results,  Open Access: 8 results) Presentation (33 results) (of which Int'l Joint Research: 9 results,  Invited: 4 results) Remarks (7 results)

  • [Journal Article] Effects of Grain Size and Grain Boundary Stability on Mechanical and Fatigue Properties of Nanocrystalline Nickel Thin Films2021

    • Author(s)
      Yoshikazu Nakai, Ryota Takeshige, Tsuyoshi Hirai, Shoichi Kikuchi
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 62 Issue: 9 Pages: 1320-1327

    • DOI

      10.2320/matertrans.Z-M2021837

    • NAID

      130008077630

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2021-09-01
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Bimodal Microstructure Design of CrMnFeCoNi High-Entropy Alloy Using Powder Metallurgy2021

    • Author(s)
      藤田佳佑,藤原弘,菊池将一
    • Journal Title

      Journal of the Society of Materials Science, Japan

      Volume: 70 Issue: 8 Pages: 648-655

    • DOI

      10.2472/jsms.70.648

    • NAID

      130008076294

    • ISSN
      0514-5163, 1880-7488
    • Year and Date
      2021-08-15
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of rolling reduction and direction on fatigue crack propagation in commercially pure titanium with harmonic structure2021

    • Author(s)
      Y. Nakai , S. Kikuchi, K. Osaki, M.O. Kawabata, and K. Ameyama
    • Journal Title

      International Journal of Fatigue

      Volume: 143 Pages: 106018-106018

    • DOI

      10.1016/j.ijfatigue.2020.106018

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Microstructural Characterization and Wear Behavior of Sintered Compacts Fabricated from Plasma-Nitrided Commercially Pure Titanium Powder2020

    • Author(s)
      S. Kikuchi, S. Suzuki and H. Akebono
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 61 Issue: 12 Pages: 2284-2291

    • DOI

      10.2320/matertrans.Z-M2020854

    • NAID

      130007942357

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2020-12-01
    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Investigation on the Durability of Ti-6Al-4V Alloy Designed in a Harmonic Structure via Powder Metallurgy: Fatigue Behavior and Specimen Size Parameter Issue2020

    • Author(s)
      Guennec Benjamin、Ishiguri Takayuki、Kawabata Mie Ota、Kikuchi Shoichi、Ueno Akira、Ameyama Kei
    • Journal Title

      Metals

      Volume: 10 Issue: 5 Pages: 636-658

    • DOI

      10.3390/met10050636

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Fabrication of high-strength Zr-based composites by spark plasma sintering2020

    • Author(s)
      Tomoyuki Fujii, Masaki Suzuki, Ryuki Matsubara, Keiichiro Tohgo and Yoshinobu Shimamura
    • Journal Title

      Journal of Materials Engineering and Performance

      Volume: 29 Issue: 12 Pages: 7883-7890

    • DOI

      10.1007/s11665-020-05308-5

    • NAID

      120006956829

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] The effects of thermo-mechanical processing on fatigue crack propagation in commercially pure titanium with a harmonic structure2020

    • Author(s)
      Osaki Kohei、Kikuchi Shoichi、Nakai Yoshikazu、Kawabata Mie Ota、Ameyama Kei
    • Journal Title

      Materials Science and Engineering: A

      Volume: 773 Pages: 138892-138892

    • DOI

      10.1016/j.msea.2019.138892

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Evaluation of Fatigue Properties under Four-point Bending and Fatigue Crack Propagation in Austenitic Stainless Steel with a Bimodal Harmonic Structure2019

    • Author(s)
      Shoichi Kikuchi, Yuta Nakatsuka, Yoshikazu Nakai, Masashi Nakatani, Mie Ota Kawabata, Kei Ameyama
    • Journal Title

      Frattura ed Integrita Strutturale

      Volume: 48 Issue: 48 Pages: 545-553

    • DOI

      10.3221/igf-esis.48.52

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Effect of Bimodal Harmonic Structure on Fatigue Properties of Austenitic Stainless Steel under Axial Loading2019

    • Author(s)
      Shoichi KIKUCHI, Yuhei NUKUI, Yuta NAKATSUKA, Yoshikazu NAKAI, Masashi NAKATANI, Mie Ota KAWABATA, Kei AMEYAMA
    • Journal Title

      International Journal of Fatigue

      Volume: 127 Pages: 222-228

    • DOI

      10.1016/j.ijfatigue.2019.06.016

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Presentation] 切欠きを有する調和組織制御オーステナイト系ステンレス鋼の疲労損傷メカニズム2022

    • Author(s)
      石村芳暉,藤田佳佑,中井善一,川畑美絵,藤原弘,飴山惠,菊池将一
    • Organizer
      日本材料学会東海支部第16回学術講演会
    • Related Report
      2021 Annual Research Report
  • [Presentation] ハイエントロピー合金CrMnFeCoNiの四点曲げ疲労特性に及ぼす結晶粒径の影響評価2021

    • Author(s)
      藤田佳佑,中澤謙太,藤原弘,菊池将一
    • Organizer
      日本材料学会 第70期学術講演会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 不均一調和組織で創成したTi-6Al-4V合金の4点曲げ疲労特性における寸法効果について2021

    • Author(s)
      ゲネック ベンジャミン,石栗崇之,川畑美絵,菊池将一,上野明,飴山惠
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 周期的に窒素拡散制御した多機能チタンの疲労特性2021

    • Author(s)
      伊藤秀明,鈴木潮里,菊池将一
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 放電プラズマ焼結により作製したCrMnFeCoNi合金の疲労き裂伝ぱ特性に及ぼす結晶粒径の影響2021

    • Author(s)
      藤田佳佑,坪井颯都,菊池将一
    • Organizer
      日本機械学会M&M2021材料力学カンファレンス
    • Related Report
      2021 Annual Research Report
  • [Presentation] 周期ミクロ強度勾配制御による多機能材料設計2021

    • Author(s)
      菊池将一
    • Organizer
      日本機械学会M&M2021材料力学カンファレンス
    • Related Report
      2021 Annual Research Report
    • Invited
  • [Presentation] Effects of grain size on fatigue crack propagation in rolled commercially pure titanium with harmonic structure2021

    • Author(s)
      Y. Nakai, S. Kikuchi, K. Osaki, M.O. Kawabata and K. Ameyama
    • Organizer
      European Congress and Exhibition on Advanced Materials and Processes - EUROMAT2021
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Fatigue properties of CrMnFeCoNi high-entropy alloy fabricated by spark plasma sintering under four-point bending2021

    • Author(s)
      K. Fujita, K. Nakazawa, H. Fujiwara, S. Kikuchi
    • Organizer
      JSSUME2020+1
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 放電プラズマ焼結を用いた周期構造制御ハイエントロピー合金CrMnFeCoNiの創製2021

    • Author(s)
      藤田佳佑,藤原弘,菊池将一
    • Organizer
      日本材料学会東海支部第15回学術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Effect of rolling on fatigue crack propagation in harmonic structured commercially pure titanium2021

    • Author(s)
      Y. Nakai, S. Kikuchi, K. Osaki, M.O. Kawabata and K. Ameyama
    • Organizer
      TMS2021
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Size effect issue on the fatigue properties of Ti-6Al-4V designed in heterogeneous harmonic structure2021

    • Author(s)
      B. Guennec, T. Ishiguri, M.O. Kawabata, S. Kikuchi, A. Ueno and K. Ameyama
    • Organizer
      TMS2021
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 高輝度放射光を用いたDCTインライン計測による調和組織制御オーステナイト系ステンレス鋼の疲労損傷評価2021

    • Author(s)
      菊池将一,塩澤大輝,中井善一,川畑美絵,飴山惠
    • Organizer
      日本金属学会2021年春期講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] チタン合金の微視組織と力学特性に及ぼす三次元窒素拡散相の影響2020

    • Author(s)
      伊藤秀明,鈴木潮里,菊池将一
    • Organizer
      日本材料学会 第69期学術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 放電プラズマ焼結により作製したハイエントロピー合金CrMnFeCoNiの四点曲げ疲労特性評価2020

    • Author(s)
      藤田佳佑,中澤謙太,藤原弘,菊池将一
    • Organizer
      日本材料学会 第69期学術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 三次元窒素拡散制御による多機能チタン系材料の創製2020

    • Author(s)
      伊藤秀明,菊池将一
    • Organizer
      日本材料学会第1回生体・医療材料部門委員会学生研究交流会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 放電プラズマ焼結を援用した生体用多機能窒化チタンの創製2020

    • Author(s)
      伊藤秀明,鈴木潮里,井尻政孝,倉科佑太,菊池将一
    • Organizer
      日本機械学会2020年度年次大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 四点曲げ疲労試験におけるハイエントロピー合金CrMnFeCoNiの疲労き裂発生・進展挙動のその場観察2020

    • Author(s)
      藤田佳佑,中澤謙太,藤原弘,菊池将一
    • Organizer
      日本材料学会 第6回材料シンポジウムワークショップ
    • Related Report
      2020 Annual Research Report
  • [Presentation] 粉末冶金を利用した周期構造制御による多機能金属材料の創製2020

    • Author(s)
      菊池将一
    • Organizer
      広島大学デジタルものづくり教育研究センター 材料MBRプロジェクト講演会
    • Related Report
      2020 Annual Research Report
    • Invited
  • [Presentation] 先進チタン合金の曲げ疲労特性とその破面2020

    • Author(s)
      菊池将一
    • Organizer
      日本材料学会第120回フラクトグラフィ部門委員会
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] Evaluation of misorientation and local deformation in bimodal harmonic structured stainless steel by hybrid imagings of diffraction and refraction contrast using synchrotron radiation X-ray2020

    • Author(s)
      Y. Nakai, S. Kikuchi, D. Shiozawa, K. Nonaka, T. Hase, Y. Nakagawa, K. Ameyama
    • Organizer
      2020 TMS Annual Meeting & Exhibition
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 三次元窒素拡散相を有するTi-6Al-4Vの創製とその力学特性評価2020

    • Author(s)
      伊藤秀明,鈴木潮里,菊池将一
    • Organizer
      日本材料学会東海支部第14回学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 放射光DCTインライン計測によるSUS304Lの疲労損傷の評価2020

    • Author(s)
      飯田柊志,長谷卓海, 三島一郎,中井善一,塩澤大輝,菊池将一
    • Organizer
      日本機械学会 関西学生会2019年度学生員卒業研究発表講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 切欠きを有する調和組織制御オーステナイト系ステンレス鋼の疲労特性2020

    • Author(s)
      松本修治,菊池将一,中井善一,川畑美絵,飴山惠
    • Organizer
      日本金属学会2020年春期(第166回)講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 調和組織を有するSUS304Lの疲労特性および疲労き裂伝ぱ特性評価2019

    • Author(s)
      菊池将一,温井悠平,中塚悠太,中井善一,中谷仁,川畑美絵,飴山惠
    • Organizer
      日本材料学会 第68期学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 三次元窒素拡散制御による工業用純チタンの高強度化2019

    • Author(s)
      和仁佑斗,鈴木潮里,菊池将一
    • Organizer
      日本材料学会 第68期学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Evaluation of misorientation and local deformation in bimodal harmonic structured stainless steel by hybrid imagings of diffraction and refraction contrast using synchrotron radiation X-ray2019

    • Author(s)
      Y. Nakai, S. Kikuchi, D. Shiozawa, K. Nonaka, T. Hase, Y. Nakagawa, K. Ameyama
    • Organizer
      EUROMAT2019
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 放射光DCTインライン計測による調和組織金属のミスオリエンテーション計測2019

    • Author(s)
      中井善一,塩澤大輝,菊池将一
    • Organizer
      第16回SPring-8産業利用報告会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 三次元窒素拡散制御した工業用純チタンの創製とその4点曲げ疲労特性2019

    • Author(s)
      鈴木潮里,和仁佑斗,菊池将一
    • Organizer
      日本機械学会2019年度年次大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 放射光 DCT インライン計測による金属材料中のミスオリエンテーション評価2019

    • Author(s)
      三島一朗,長谷卓海,塩澤大輝,菊池将一,中井善一,永廣怜平
    • Organizer
      日本機械学会M&M2019材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 高輝度放射光回折コントラストトモグラフィーによるSUS304L 調和組織材の疲労過程における損傷評価2019

    • Author(s)
      長谷卓海,中川湧紀,中井善一,菊池将一,塩澤大輝
    • Organizer
      日本機械学会M&M2019材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] Effect of bimodal harmonic structure on fatigue properties and fatigue crack propagation in austenitic stainless steel2019

    • Author(s)
      S. Kikuchi and Y. Nakai
    • Organizer
      The 6th Joint-Symposium on Mechanics of Advanced Materials & Structures (JSMAMS 2019)
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of thermo-mechanical processing on fatigue properties of commercially pure titanium with harmonic structure2019

    • Author(s)
      K. Osaki, S. Kikuchi, Y. Nakai, M. O. Kawabata, K. Ameyama
    • Organizer
      Materials Research Meeting 2019
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of three-dimensional nitrogen diffusion phase on mechanical properties of cp-titanium for biomedical applications2019

    • Author(s)
      S. Suzuki, H. Ito, Y. Kurashina, H. Akebono, S. Kikuchi
    • Organizer
      8th International Conference on Mechanics of Biomaterials and Tissues
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Remarks] 静岡大学教員データベース

    • URL

      https://tdb.shizuoka.ac.jp/RDB/public/Default2.aspx?id=11250&l=0

    • Related Report
      2021 Annual Research Report
  • [Remarks] Google Scholar

    • URL

      https://scholar.google.co.jp/citations?user=JDyyTcYAAAAJ&hl=ja

    • Related Report
      2021 Annual Research Report 2020 Annual Research Report 2019 Annual Research Report
  • [Remarks] researchmap

    • URL

      https://researchmap.jp/read0151423/

    • Related Report
      2021 Annual Research Report 2020 Annual Research Report 2019 Annual Research Report
  • [Remarks] Scopus

    • URL

      https://www.scopus.com/authid/detail.uri?authorId=15071312000

    • Related Report
      2021 Annual Research Report 2020 Annual Research Report 2019 Annual Research Report
  • [Remarks] ORCID

    • URL

      https://orcid.org/0000-0003-1127-8748

    • Related Report
      2021 Annual Research Report 2020 Annual Research Report 2019 Annual Research Report
  • [Remarks] 静岡大学教員データベース

    • URL

      https://tdb.shizuoka.ac.jp/RDB/public/Default2.aspx?id=11250&l=0&a2=1/1

    • Related Report
      2020 Annual Research Report
  • [Remarks] 静岡大学教員データベース

    • URL

      https://tdb.shizuoka.ac.jp/RDB/public/Default2.aspx?id=11250&l=0&t=21

    • Related Report
      2019 Annual Research Report

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Published: 2019-04-18   Modified: 2023-01-30  

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