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Measurement and control of internal stress in thin film metallic glass using combinatorial technology

Research Project

Project/Area Number 19H02040
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Review Section Basic Section 18020:Manufacturing and production engineering-related
Research InstitutionNagoya University

Principal Investigator

HATA SEIICHI  名古屋大学, 工学研究科, 教授 (50293056)

Co-Investigator(Kenkyū-buntansha) 櫻井 淳平  名古屋大学, 工学研究科, 准教授 (40345385)
岡 智絵美  名古屋大学, 工学研究科, 助教 (70823285)
山崎 貴大  名古屋大学, 工学研究科, 学振特別研究員(PD) (40847240)
Project Period (FY) 2019-04-01 – 2023-03-31
Project Status Completed (Fiscal Year 2022)
Budget Amount *help
¥17,420,000 (Direct Cost: ¥13,400,000、Indirect Cost: ¥4,020,000)
Fiscal Year 2022: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2021: ¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2020: ¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2019: ¥5,720,000 (Direct Cost: ¥4,400,000、Indirect Cost: ¥1,320,000)
Keywords内部応力 / 薄膜 / コンビナトリアル技術 / アニール / 薄膜金属ガラス
Outline of Research at the Start

本研究では,ナノからマイクロメートルオーダの膜厚を有する薄膜金属ガラスの内部応力を体系的かつ効率的に解明し,それを制御可能か?を研究課題の核心をなす学術的「問い」として,以下の研究目的にて本研究を進める.
1)薄膜金属ガラスの内部応力を体系的に調査するためのコンビナトリアル技術の確立
2)上記コンビナトリアル技術を用いて,膜厚10 nm~10 umのRu系およびTi系薄膜金属ガラスの成膜条件,アニール条件と内部応力の関係解明
3)実証とし薄膜金属ガラスの内部応力を±200 MPaの範囲,精度±2 MPaにて自在に制御された直径400 nm~800 umのダイアフラム構造を製作

Outline of Final Research Achievements

The aim of this study was to investigate the internal stress of thin film metallic glasses using combinatorial techniques, elucidate the relationship between deposition conditions and internal stress of thin film metallic glasses, and demonstrate the fabrication of diaphragm structures with a diameter ranging from 400 nm to 800 um, allowing for precise control of the internal stress within a range of ±200 MPa. In particular, we developed a differential exhaust combinatorial opposing target sputtering apparatus, established a thin film library for evaluating internal stress, and explored the correlation between annealing conditions and internal stress. Consequently, we successfully devised a novel method for measuring internal stress and unveiled the relationship between internal stress and annealing conditions for Ru-based and Ni-based thin film metallic glasses. Moreover, we accomplished the fabrication of diaphragm structures with meticulously controlled internal stress.

Academic Significance and Societal Importance of the Research Achievements

MEMS構造の一部は基板から分離しており,材料内の応力により形状が変わり破壊されることがある.Si系材料は成膜条件等により内部応力を制御できるが,小型化や高機能化には限界があるため,代替材料が求められている.この状況に着目し,薄膜金属ガラスを利用したMEMS構造と内部応力制御を実現した.近年,薄膜金属ガラスをMEMSに適用する事例が増えてきたため,内部応力を解明し制御する必要性が浮かび上がってきた.この研究では,薄膜金属ガラスの内部応力を体系的かつ効率的に解明し,制御可能かを明らかにするために行われた.

Report

(5 results)
  • 2022 Annual Research Report   Final Research Report ( PDF )
  • 2021 Annual Research Report
  • 2020 Annual Research Report
  • 2019 Annual Research Report
  • Research Products

    (41 results)

All 2022 2021 2020 2019 Other

All Journal Article (6 results) (of which Peer Reviewed: 6 results,  Open Access: 2 results) Presentation (31 results) (of which Int'l Joint Research: 10 results,  Invited: 2 results) Remarks (4 results)

  • [Journal Article] Effect of structural relaxation at bellow crystallization temperature on internal stress of Ni-Nb-Zr thin-film amorphous alloys diaphragm for Micro electromechanical systems sensors2022

    • Author(s)
      F. Haga, T. Yamazaki, C. Oka S. Hata Y. Hoshino, J. Sakurai
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: - Issue: SD Pages: SD1027-SD1027

    • DOI

      10.35848/1347-4065/ac5d12

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Combinatorial search for Ti-Ni-Hf high formable shape memory alloys2022

    • Author(s)
      S. Inoue, T. Yamazaki, C. Oka, S. Hata, J. Sakurai
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: - Issue: 6 Pages: 065507-065507

    • DOI

      10.35848/1347-4065/ac6a97

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Fabrication and Evaluation of Actuators for Reaction Force Variable Passive-type Tactile Displays2021

    • Author(s)
      南原 圭汰,山崎 貴大,岡 智絵美,秦 誠一,櫻井 淳平
    • Journal Title

      IEEJ Transactions on Sensors and Micromachines

      Volume: 141 Issue: 9 Pages: 304-309

    • DOI

      10.1541/ieejsmas.141.304

    • NAID

      130008082227

    • ISSN
      1341-8939, 1347-5525
    • Year and Date
      2021-09-01
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Examination of Mechanical Properties and Photoelastic Properties of Gel Material for Blood Vessel Mimics2021

    • Author(s)
      D. Yamada, S. Hori, S. Abe, Y. Kumeno, T. Yamazaki, C. Oka, J. Sakurai, S. Hata
    • Journal Title

      Journal of Medical Devices

      Volume: 15 Issue: 3 Pages: 31011-31011

    • DOI

      10.1115/1.4051516

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Particle-in-cell Monte Carlo collision simulation and experimental measurement of Ar plasma in a fast atom beam source for surface-activated bonding2021

    • Author(s)
      Ryo Morisaki , Takahiro Yamazaki , Chiemi Oka , Junpei Sakurai , Takami Hirai , Tomonori Takahashi , Hiroyuki Tsuji , Noriyasu Ohno , and Seiichi Hata
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 60 Issue: SC Pages: SCCB01-SCCB01

    • DOI

      10.35848/1347-4065/abe683

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of a fast atom beam gun for surface-activated bonding2020

    • Author(s)
      Ryo Morisaki, Yuuki Hirai, Chiemi Oka, Mizue Mizoshiri, Takahiro Yamazaki, Junpei Sakurai, Takami Hirai, Tomonori Takahashi, Hiroyuki Tsuji and Seiichi Hata
    • Journal Title

      Precision Engineering

      Volume: 62 Pages: 106-112

    • DOI

      10.1016/j.precisioneng.2019.11.006

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Presentation] Combinatorial Search for Chlorine Evolution Electrode Catalyst using Bayesian optimization2022

    • Author(s)
      Junpei Sakurai, Kimihiko Sugiura, Chiemi Oka, Seiichi Hata
    • Organizer
      11th International Workshop on Combinatorial Materials Science and Technology
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of tactile pin height on driving characteristics using high formable shape-memory alloy for reaction force variable tactile displays2022

    • Author(s)
      Masanori Murase, Keita Nambara, Chiemi Oka, Seiichi Hata, Junpei Sakurai
    • Organizer
      International Conference on Materials & Processing 2022 (ICM&P 2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Novel Measurement Method of Internal Stress in Thin Films Using Micro Spring Structure2022

    • Author(s)
      Shun Takase, Takahiro Yamazaki, Chiemi Oka, Junpei Sakurai, Seiichi Hata
    • Organizer
      International Conference on Materials & Processing 2022 (ICM&P 2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Combinatorial search and evaluation for new Ti?Ni?Hf high formable shape memory alloys2022

    • Author(s)
      Yishu Wang, Shin Inoue, Chiemi Oka, Seiichi Hata, Junpei Sakurai
    • Organizer
      International Conference on Materials & Processing 2022 (ICM&P 2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Fabrication and evaluation of capacitive pressure sensor using thin film metallic glass2022

    • Author(s)
      H. Osuka, T. Ninoseki, C. Oka, S. Hata, J. Sakurai
    • Organizer
      35th International Microprocesses and Nanotechnology Conference (MNC2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Combinatorial search and evaluation for new Ti- Ni?Hf high formable shape memory alloys2022

    • Author(s)
      Yishu Wang, Shin Inoue, Chiemi Oka, Seiichi Hata, Junpei Sakurai
    • Organizer
      The 7th International Symposium on Biomedical Engineering (ISBE 2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Controlling internal stress of Ni-Nb-Zr thin film amorphous alloy diaphragms by beta-relaxation annealing2022

    • Author(s)
      Jinglan Xie, Fuyuki Haga, Chiemi Oka, Seiichi Hata, Junpei Sakurai
    • Organizer
      International Conference on Materials & Processing 2022 (ICM&P 2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] The effect of alloy composition on beta-relaxation of Ni-Nb-Zr thin film amorphous alloys2022

    • Author(s)
      Jinglan Xie, Fuyuki Haga, Chiemi Oka, Seiichi Hata, Junpei Sakurai
    • Organizer
      International Symposium on Micro-Nano Mechatronics and Human Science (MHS 2022)
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 薄膜金属ガラス製静電容量形圧力センサの作製と評価2022

    • Author(s)
      大塚 穂高,二関 隆史,岡 智絵美,秦 誠一,櫻井 淳平
    • Organizer
      2022年電気学会 E部門総合研究会 マイクロマシン・センサシステム研究会
    • Related Report
      2022 Annual Research Report
  • [Presentation] 熱処理による構造緩和を利用した薄膜金属ガラス製静電容量形圧力センサの評価2022

    • Author(s)
      大塚 穂高,二関 隆史,岡 智絵美,秦 誠一,櫻井 淳平
    • Organizer
      応用物理学会 第13回集積化MEMSワークショップ
    • Related Report
      2022 Annual Research Report
  • [Presentation] MEMSに向けたNi-Nb-Zr薄膜非晶質合金製ダイアフラムの内部応力制御2022

    • Author(s)
      謝靖蘭,羽賀冬樹,山崎貴大,岡智絵美,秦誠一,櫻井淳平
    • Organizer
      日本機械学会 2022年度 年次大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] 反力可変触覚ディスプレイ用アクチュエータの駆動特性2022

    • Author(s)
      村瀨正憲,南原圭汰,岡智絵美,秦誠一,櫻井淳平
    • Organizer
      応用物理学会 第13回集積化MEMSワークショップ
    • Related Report
      2022 Annual Research Report
  • [Presentation] 反力可変触覚ディスプレイ用アクチュエータの駆動特性に及ぼす触知ピン形状の影響2022

    • Author(s)
      村瀨正憲,南原圭汰,岡智絵美,秦誠一,櫻井淳平
    • Organizer
      第14回集積化MEMSシンポジウム
    • Related Report
      2022 Annual Research Report
  • [Presentation] MEMS デバイスを利用したNi基薄膜金属ガラスの内部応力測定2022

    • Author(s)
      高瀬駿,岡智絵美,櫻井淳平,秦誠一
    • Organizer
      第14回集積化MEMSシンポジウム
    • Related Report
      2022 Annual Research Report
  • [Presentation] 微細加工を応用したAI時代の材料探索2021

    • Author(s)
      秦 誠一
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
    • Invited
  • [Presentation] AIとコンビナトリアル技術を用いた新機能性材料・新磁歪材料の探索2021

    • Author(s)
      秦 誠一
    • Organizer
      第29回磁気応用技術シンポジウム
    • Related Report
      2021 Annual Research Report
    • Invited
  • [Presentation] HFSMAを用いたナノ繊毛構造体の作製2021

    • Author(s)
      佐藤 寛太,山崎 貴大,岡 智絵美,秦 誠一,櫻井 淳平
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] MEMS構造体を利用した薄膜内部応力の測定2021

    • Author(s)
      高瀬 駿,山崎 貴大,岡 智絵美,櫻井 淳平,秦 誠一
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 反力可変受動形触覚ディスプレイ用新規アクチュエータの駆動特性2021

    • Author(s)
      村瀬 正憲,南原 圭汰,山崎 貴大,岡 智絵美,秦 誠一,櫻井 淳平
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 薄膜金属ガラスを用いた自立微細構造体の基礎検討2021

    • Author(s)
      大西 拓也,永井 伶於,山崎 貴大,岡 智絵美,櫻井 淳平,秦 誠一
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 高成形性形状記憶合金を用いたナノ繊毛構造体の作製に向けた基礎検討2021

    • Author(s)
      佐藤 寛太,山崎 貴大,岡 智絵美,秦 誠一,櫻井 淳平
    • Organizer
      日本機械学会2021年度年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Ti-Ni-Hf高成形性形状記憶合金のコンビナトリアル探索2021

    • Author(s)
      井上 慎,岡 智絵美,秦 誠一,櫻井 淳平
    • Organizer
      形状記憶合金協会 第11期定時総会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Plasma analysis of the FAB source for the SAB process by PIC-MCC simulation2020

    • Author(s)
      Ryo Morisaki , Takahiro Yamazaki , Chiemi Oka , Junpei Sakurai , Takami Hirai , Tomonori Takahashi , Hiroyuki Tsuji , Noriyasu Ohno , and Seiichi Hata
    • Organizer
      33rd International Microprocesses and Nanotechnology Conference
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Ti-Ni-Cu高成形性形状記憶合金を用いた,反力可変受動形触覚ディスプレイ用触知ピンの作製2020

    • Author(s)
      南原 圭汰, 伊木 啓一郎, 岡 智絵美, 秦 誠一, 櫻井 淳平
    • Organizer
      日本機械学会2020年度年次大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Ti-Ni-Cu高成形性形状記憶合金を用いた,反力可変受動形触覚ディスプレイ用触知ピンの作製及び駆動評価2020

    • Author(s)
      南原 圭汰, 伊木 啓一郎, 岡 智絵美, 秦 誠一, 櫻井 淳平
    • Organizer
      第28回機械材料・材料加工技術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Ti-Ni-Cu高成形性形状記憶合金のソフトアクチュエータへの基礎検討2020

    • Author(s)
      浅井 泰平,青山 椋佑,岡智絵美,櫻井淳平,秦誠一
    • Organizer
      第28回機械材料・材料加工技術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 逆リフトオフ法を用いた MEMS ミラーデバイスの作製2020

    • Author(s)
      高瀬駿,山田恭平,中川優希,山崎貴大,岡智絵美,櫻井 淳平, 秦 誠一
    • Organizer
      第28回機械材料・材料加工技術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 逆リフトオフ法を用いたMEMSミラー構造体の作製2019

    • Author(s)
      山田 恭平,中川 優希,岡 智絵美,櫻井 淳平,吉田 沙織,清元 智文,秦 誠一
    • Organizer
      日本機械学会2019年度年次大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 表面活性化接合用新規高速原子ビームガン2019

    • Author(s)
      森崎 諒,岡 智絵美,櫻井 淳平,平井 隆巳,高橋 知典,辻 裕之,秦 誠一
    • Organizer
      精密工学会2019年度秋季大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 薄膜金属ガラスの大気中結晶化評価法の基礎検討2019

    • Author(s)
      鬼頭 直希,櫻井 淳平,岡 智絵美,林 裕美,山崎 宏明,秦 誠一
    • Organizer
      精密工学会2019年度秋季大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Development and evaluation of the novel FAB gun2019

    • Author(s)
      Ryo Morisaki, Yuuki Hirai, Junpei Sakurai, Mizue Mizoshiri, Chiemi Oka, Takami Hirai, Tomonori Takahashi, Hiroyuki Tsuji and Seiichi Hata
    • Organizer
      19th International Conference & Exhibition
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Remarks] マイクロ・ナノプロセス研究グループ

    • URL

      http://mnm.mae.nagoya-u.ac.jp/

    • Related Report
      2022 Annual Research Report 2021 Annual Research Report
  • [Remarks] デライトものづくりAIネットワークプラットフォーム

    • URL

      http://planet-aidea.com/

    • Related Report
      2021 Annual Research Report
  • [Remarks] マイクロ・ナノプロセス研究グループ

    • URL

      http://mnm.mae.nagoya-u.ac.jp/jp/

    • Related Report
      2020 Annual Research Report
  • [Remarks] 名古屋大学大学院工学研究科 秦研究室

    • URL

      http://mnp.mech.nagoya-u.ac.jp/jp/

    • Related Report
      2019 Annual Research Report

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Published: 2019-04-18   Modified: 2024-01-30  

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