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Development of Ultra-Lightweight High-Strength Heat-Resistant Magnesium Alloys with Excellent Nonflammability by Utilizing Advanced High-Temperature Strengthening Mechanism

Research Project

Project/Area Number 19K05054
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 26040:Structural materials and functional materials-related
Research InstitutionTokyo Institute of Technology

Principal Investigator

Terada Yoshihiro  東京工業大学, 物質理工学院, 准教授 (40250485)

Project Period (FY) 2019-04-01 – 2022-03-31
Project Status Completed (Fiscal Year 2021)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2021: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2020: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2019: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Keywordsマグネシウム合金 / 高温強度 / ラメラ組織 / 高分解能電子顕微鏡 / 転位 / 異相界面
Outline of Research at the Start

金属組織をナノラメラ状に制御し,異相界面強化という新規材料強化機構を最大限に利用することにより,高温強度が極めて高い高効率熱機関用の難燃性超軽量高強度耐熱マグネシウム合金を開発することが,本研究の最終目標である。『異相界面強化』は,極めて高い温度においてもナノラメラ組織が安定に維持されるため,高温材料強化機構として有望であると推定される。合金開発にあたり,(Ⅰ)高温変形特性調査,(Ⅱ)転位モビリティ解析,(Ⅲ)組織安定性評価という三つの独立した個別研究課題について,相互関係を持たせながらスパイラルアップ(図3)することにより計画を進める。

Outline of Final Research Achievements

An ultra-lightweight high-strength heat-resistant magnesium alloy with excellent nonflammability has been developed by utilizing the advanced high-temperature strengthening mechanism. We successfully produced the Mg-Ca two-phase alloy with a lamellar spacing of 900 nm, and investigated the academic knowledges necessary for its application as a high-temperature structural material. The temperature range where the fine lamellar structure in the developed alloy is thermally stable is below 573 K, and the lamellar microstructure coarsens above 573 K. When this alloy is creep-tested at 473 K, the lower minimum creep rate is obtained with decreasing the lamellar spacing, indicating that the lamellar interface plays a creep-strengthening role. It was elucidated that the creep for the alloy is controlled by the high-temperature climb of dislocations.

Academic Significance and Societal Importance of the Research Achievements

本研究の社会的意義として,エンジン周辺部の高温構造部材の軽量化を通じて,自動車の燃費向上を飛躍的に推進できることが挙げられる。また,学術的意義として,異相界面強化と称する新規な高温材料強化機構を世界で初めて提案し,実証したことが挙げられる。この新規な高温材料強化機構を最大限に発現できるよう,サブミクロンサイズの微細な層状組織に組織制御した点が独創的である。従来の高温構造材料とは全く新しい概念の金属組織を有する本開発合金について,基礎的な学術的知見として,組織安定性,界面構造,および,高温強度特性を明確化した。本研究において用いた研究手法は,今後,様々な合金系に適用できるものと期待される。

Report

(4 results)
  • 2021 Annual Research Report   Final Research Report ( PDF )
  • 2020 Research-status Report
  • 2019 Research-status Report
  • Research Products

    (20 results)

All 2021 2020 2019

All Journal Article (15 results) (of which Peer Reviewed: 15 results,  Open Access: 13 results) Presentation (4 results) (of which Int'l Joint Research: 2 results,  Invited: 1 results) Book (1 results)

  • [Journal Article] Effect of Lamellar Spacing on Creep Strength of α-Mg/C14–Mg<sub>2</sub>Ca Eutectic Alloy2021

    • Author(s)
      Koji Oishi, Satoshi Araki, Yoshihiro Terada
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 62 Issue: 9 Pages: 1414-1419

    • DOI

      10.2320/matertrans.MT-M2021101

    • NAID

      130008077611

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2021-09-01
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of Lamellar Spacing on Creep Strength of <i>α</i>-Mg/C14-Mg<sub>2</sub>Ca Eutectic Alloy2021

    • Author(s)
      大石航司,荒木聡司,寺田芳弘
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 85 Issue: 6 Pages: 223-228

    • DOI

      10.2320/jinstmet.J2021005

    • NAID

      130008042818

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Year and Date
      2021-06-01
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Lamellar Structure Stability of a Two-Phase α-Mg/C14–Mg<sub>2</sub>Ca Alloy2021

    • Author(s)
      Shuntaro Abe, Koji Oishi, Yoshihiro Terada
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 62 Issue: 4 Pages: 544-550

    • DOI

      10.2320/matertrans.MT-M2020376

    • NAID

      130008002784

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2021-04-01
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Coherency evaluation of <i>α</i>-Mg/C15-Al<sub>2</sub>Ca interface for a Mg-Al-Ca alloy2021

    • Author(s)
      久澤大夢,柏瀬早季子,寺田芳弘
    • Journal Title

      Journal of Japan Institute of Light Metals

      Volume: 71 Issue: 2 Pages: 127-129

    • DOI

      10.2464/jilm.71.127

    • NAID

      130007998316

    • ISSN
      0451-5994, 1880-8018
    • Year and Date
      2021-02-15
    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of Distributions of Constituent Phases on Mechanical Properties of C–Si–Mn Dual-phase Steel2021

    • Author(s)
      Tatsuya Nakagaito, Takako Yamashita, Takeshi Yokota, Yoshihiro Terada, Masanori Kajihara
    • Journal Title

      ISIJ International

      Volume: 61 Issue: 1 Pages: 452-462

    • DOI

      10.2355/isijinternational.ISIJINT-2020-435

    • NAID

      130007969913

    • ISSN
      0915-1559, 1347-5460
    • Year and Date
      2021-01-15
    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Precipitation Behavior of Ni-Based Superalloy Alloy 625 for A-USC Power Plants2021

    • Author(s)
      南龍之介,寺田芳弘
    • Journal Title

      Tetsu-to-Hagane

      Volume: 107 Issue: 10 Pages: 845-852

    • DOI

      10.2355/tetsutohagane.TETSU-2021-065

    • NAID

      130008094721

    • ISSN
      0021-1575, 1883-2954
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Interface Strengthening of α-Mg/C14-Mg2Ca Eutectic Alloy2021

    • Author(s)
      Satoshi Araki, Koji Oishi, Yoshihiro Terada
    • Journal Title

      Metals

      Volume: 11 Issue: 12 Pages: 1913-1913

    • DOI

      10.3390/met11121913

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Lamellar Structure Stability of a Two-Phase <i>α</i>-Mg/C14–Mg<sub>2</sub>Ca Alloy2020

    • Author(s)
      阿部俊太郎,大石航司,寺田芳弘
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 84 Issue: 12 Pages: 399-405

    • DOI

      10.2320/jinstmet.J2020029

    • NAID

      130007942358

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Year and Date
      2020-12-01
    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Morphology Evolution of γ′ Precipitates for Wrought Ni-Based Superalloys2020

    • Author(s)
      Yoshiya Yamaguchi, Ryotaro Tajima, Yoshihiro Terada
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 61 Issue: 11 Pages: 2185-2194

    • DOI

      10.2320/matertrans.MT-M2020183

    • NAID

      130007930239

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2020-11-01
    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Microstructure Evolution during Isothermal Aging for Wrought Nickel-Based Superalloy Udimet 5202020

    • Author(s)
      Yoshiya Yamaguchi, Mayumi Abe, Ryotaro Tajima, Yoshihiro Terada
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 61 Issue: 8 Pages: 1689-1697

    • DOI

      10.2320/matertrans.MT-M2020115

    • NAID

      130007879894

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2020-08-01
    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] C15–Al<sub>2</sub>Ca Precipitation in a Mg–Al–Ca Alloy2020

    • Author(s)
      Kashiwase Sakiko, Unekawa Mariko, Hisazawa Hiromu, Terada Yoshihiro
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 61 Issue: 2 Pages: 375-380

    • DOI

      10.2320/matertrans.MT-M2019291

    • NAID

      130007790215

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2020-02-01
    • Related Report
      2019 Research-status Report
    • Peer Reviewed
  • [Journal Article] 鍛造 Ni 基超合金における γ′ 析出粒子の形態変化2020

    • Author(s)
      山口義矢,田島遼太郎,寺田芳弘
    • Journal Title

      日本金属学会誌

      Volume: 84 Pages: 151-160

    • NAID

      130007835669

    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Three-Dimensional Morphology of C15–Al<sub>2</sub>Ca Precipitates in a Mg–Al–Ca Alloy2019

    • Author(s)
      Kashiwase Sakiko, Unekawa Mariko, Hisazawa Hiromu, Terada Yoshihiro
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 60 Issue: 9 Pages: 2048-2052

    • DOI

      10.2320/matertrans.MT-M2019149

    • NAID

      130007695373

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2019-09-01
    • Related Report
      2019 Research-status Report
    • Peer Reviewed
  • [Journal Article] Coarsening of Plate-Like C15–Al<sub>2</sub>Ca Precipitates in a Mg–Al–Ca Alloy2019

    • Author(s)
      柏瀬早季子,畝川真梨子,久澤大夢,寺田芳弘
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 83 Issue: 8 Pages: 282-287

    • DOI

      10.2320/jinstmet.J2019022

    • NAID

      130007683517

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Year and Date
      2019-08-01
    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Three-Dimensional Morphology of C15–Al<sub>2</sub>Ca Precipitates in a Mg–Al–Ca Alloy2019

    • Author(s)
      柏瀬早季子,畝川真梨子,久澤大夢,寺田芳弘
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 83 Issue: 6 Pages: 193-197

    • DOI

      10.2320/jinstmet.J2019009

    • NAID

      130007653145

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Year and Date
      2019-06-01
    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] Interface Strengthening of α-Mg/C14-Mg2Ca Eutectic Alloy2021

    • Author(s)
      Yoshihiro Terada
    • Organizer
      15th International Conference on Creep and Fracture of Engineering Materials and Structures
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Metallic-Intermetallic Eutectic Composites for High-Temperature Applications2021

    • Author(s)
      Yoshihiro Terada
    • Organizer
      2021 4th International Conference on Advanced Composite Materials
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Mg-Al-Ca合金の高温クリープ強度に及ぼす微細Al2Ca析出相の影響2019

    • Author(s)
      光楽弘基,寺田芳弘
    • Organizer
      日本金属学会 第165回講演大会
    • Related Report
      2019 Research-status Report
  • [Presentation] Mg-Ca二元系合金におけるC14-Mg2Ca相の時効析出挙動2019

    • Author(s)
      畝川真梨子,寺田芳弘
    • Organizer
      日本金属学会 第165回講演大会
    • Related Report
      2019 Research-status Report
  • [Book] 熱処理技術セミナー 熱処理基礎講座2021

    • Author(s)
      寺田芳弘
    • Total Pages
      8
    • Publisher
      一般社団法人 日本熱処理技術協会
    • Related Report
      2021 Annual Research Report

URL: 

Published: 2019-04-18   Modified: 2023-01-30  

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