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Novel X-ray structure imaging based on the combination of X-ray diffraction and X-ray absorption fine structure

Research Project

Project/Area Number 20350041
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Analytical chemistry
Research InstitutionNational Institute for Materials Science

Principal Investigator

SAKURAI Kenji  National Institute for Materials Science, 量子ビームセンター, グループリーダー (00354176)

Research Collaborator 江場 宏美  東京都市大学, 準教授
水沢 多鶴子  独立行政法人物質・材料研究機構, 研究業務員
小林 俊一  筑波大学, 大学院生
HSU Hsiang-Han  筑波大学, 大学院生
SAMSON Vallerie Ann Innis  筑波大学, 大学院生
JERAB Martin  Charles Univ in Prague, 大学院生
MAREK Vysinka  Charles Univ in Prague, 大学院生
JAKUB Vaverka  Charles Univ in Prague, 大学院生
ZHANG Yang-Ping  独立行政法人物質・材料研究機構, 研修生
GLESAAEN Jonnas Rylund  独立行政法人物質・材料研究機構, 研修生
OGER Kevin  独立行政法人物質・材料研究機構, 研修生
BICER Mehmet  独立行政法人物質・材料研究機構, 研修生
CHANG Emma  独立行政法人物質・材料研究機構, 研修生
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥19,240,000 (Direct Cost: ¥14,800,000、Indirect Cost: ¥4,440,000)
Fiscal Year 2010: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2009: ¥12,740,000 (Direct Cost: ¥9,800,000、Indirect Cost: ¥2,940,000)
Fiscal Year 2008: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Keywords分析・計測 / X線技術 / 可視化 / イメージング / 原子レベル構造
Research Abstract

In the present research, novel X-ray imaging, which combines X-ray diffraction and X-ray absorption fine structure (XAFS), has been developed to visualize the inhomogeneous samples in terms of the crystalline structure, the atomic-scale structure, the valence number, the electronic state etc etc…The technique has been applied to the structure imaging of the mixture of crystalline and non-crystalline materials, the valence number imaging of the mixture of metals and oxides, and combinatorial imaging.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (37 results)

All 2011 2010 2009 2008 Other

All Journal Article (12 results) (of which Peer Reviewed: 12 results) Presentation (16 results) Remarks (5 results) Patent(Industrial Property Rights) (4 results)

  • [Journal Article] X-ray Diffraction Imaging of Ana tase and Rutile2010

    • Author(s)
      Kenji Sakurai, Mari Mizusawa
    • Journal Title

      Analytical Chemistry 82

      Pages: 3519-3522

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 投影型X線回図6銅ミラー腐食部のX線回折イメージングの結果折イメージング法による液体金属ガリウムの凝固・融解時不均一結晶組織のin-situ観察2010

    • Author(s)
      水沢まり,桜井健次
    • Journal Title

      分析化学 59

      Pages: 499-511

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 投影型X線回折イメージング法による液体金属ガリウムの凝固・融解時不均一結晶組織のin-situ観察2010

    • Author(s)
      水沢まり, 桜井健次
    • Journal Title

      分析化学

      Volume: 59 Pages: 499-511

    • NAID

      10026476426

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] X-ray Diffraction Imaging of Anatase and Rutile2010

    • Author(s)
      Kenji Sakurai, Mari Mizusawa
    • Journal Title

      Analytical Chemsitry

      Volume: 82 Pages: 3519-3522

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Inter-correlation of impurity trace elements in bloodstone rock : X-ray fluorescence mapping studies2009

    • Author(s)
      Yang-ping Zhang, Kenji Sakurai
    • Journal Title

      Journal of Analytical Atomic Spectrometry 24

      Pages: 1579-1583

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of High-Resolution X-ray Absorption and Emission Spectroscopy for the Chemical Speciation of Binary Titanium Compounds2009

    • Author(s)
      F.Reinhardt, B.Beckhof, H.Eba, B.Kanngiesser, M.Kolbe, M.Mizusawa, M.Mller, B.Pollakowski, Kenji Sakurai, G.Ulm
    • Journal Title

      Analytical Chemistry 81

      Pages: 1770-1776

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 投影型X線回折イメージング法による氷の融解・凝固過程のin-situ観察2009

    • Author(s)
      水沢まり,桜井健次
    • Journal Title

      X線分析の進歩 40

      Pages: 279-290

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 投影型X線回折イメージング法による氷の融解・凝固過程のin-situ観察2009

    • Author(s)
      水沢まり, 桜井健次
    • Journal Title

      X線分析の進歩 40

      Pages: 279-290

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of High-Resolution X-ray Absorption and Emission Spectroscopy for the Chemical Speciation of Binary Titanium Compounds2009

    • Author(s)
      F.Reinhardt, B.Beckhof, H.Eba, B.Kanngiesser, M.Kolbe, M.Mizusawa, M.Mller, B.Pollakowski, K.Sakurai, G.Ulm
    • Journal Title

      Analytical Chemistry 81

      Pages: 1770-1776

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Inter-correlation of impurity trace elements in bloodstone rock : X-ray fluorescence mapping studies2009

    • Author(s)
      Yan-ping Zhang, Kenji Sakurai
    • Journal Title

      Journal of Analytical Atomic Spectrometry 24

      Pages: 1579-1583

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] X線吸収スペクトルによる亜鉛ガリウム酸化物ナノ粒子の結晶性評価2008

    • Author(s)
      江場宏美,桜井健次
    • Journal Title

      X線分析の進歩 39

      Pages: 199-207

    • NAID

      40015956295

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] X線吸収スペクトルによる亜鉛ガリウム酸化物ナノ粒子の結晶性評価2008

    • Author(s)
      江場宏美, 桜井健次
    • Journal Title

      X線分析の進歩 39

      Pages: 199-207

    • NAID

      40015956295

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] Traubeの人工細胞の蛍光X線イメージング2011

    • Author(s)
      水沢まり, 桜井健次
    • Organizer
      第24回日本放射光学会年会・放射光科学合同シンポジウム
    • Place of Presentation
      つくば国際会議場(茨城県)
    • Related Report
      2010 Annual Research Report
  • [Presentation] X-ray fluorescence imaging of Liesegang rings2011

    • Author(s)
      Vsynka Marek, Mari Mizusawa, Kenji Sakurai
    • Organizer
      第24回日本放射光学会年会・放射光科学合同シンポジウム
    • Place of Presentation
      つくば国際会議場(茨城県)
    • Related Report
      2010 Annual Research Report
  • [Presentation] Traubeの人工細胞の蛍光X線イメージング2010

    • Author(s)
      水沢まり, 桜井健次
    • Organizer
      日本顕微鏡学会第65回学術講演会
    • Place of Presentation
      名古屋国際会議場(愛知県)
    • Related Report
      2010 Annual Research Report
  • [Presentation] X-ray fluorescence imaging of growing chemical patterns2010

    • Author(s)
      Kenji Sakurai, Mari Mizusawa
    • Organizer
      7th International Conference on Synchrotron Radiati on in Materia
    • Place of Presentation
      The Said Business School, Oxford (英国)
    • Related Report
      2010 Annual Research Report
  • [Presentation] 時々刻々の変化を追う蛍光X線イメージングとX線反射率法2010

    • Author(s)
      桜井健次
    • Organizer
      埋もれた界面のX線・中性子解析に関するワークショップ2010
    • Place of Presentation
      名古屋大学ベンチャービジネスラボラトリー(愛知県)
    • Related Report
      2010 Annual Research Report
  • [Presentation] Traubeの人工細胞の蛍光X線イメージング2010

    • Author(s)
      水沢まり, 桜井健次
    • Organizer
      第46回X線分析討論会
    • Place of Presentation
      広島県情報プラザ(広島県)
    • Related Report
      2010 Annual Research Report
  • [Presentation] Silver chromate Liesegang rings observed by X-ray fluorescence technique2010

    • Author(s)
      Vsynka Marek, Mari Mizusawa, Kenji Sakurai
    • Organizer
      第46回X線分析討論会
    • Place of Presentation
      広島県情報プラザ(広島県)
    • Related Report
      2010 Annual Research Report
  • [Presentation] X-ray fluorescence imaging of growing chemical patterns2010

    • Author(s)
      Kenji Sakurai, Mari Mizusawa
    • Organizer
      2010 International Chemical Congress of Pacific Basin Societies
    • Place of Presentation
      Hawaii Convention Center, Honolulu, Hawaii (米国)
    • Related Report
      2010 Annual Research Report
  • [Presentation] ブラッドストーンのX線分析2010

    • Author(s)
      Yan-ping Zhang、水沢まり、桜井健次
    • Organizer
      第23回日本放射光学会年会・放射光科学合同シンポジウム
    • Place of Presentation
      イーグレ姫路、姫路市
    • Related Report
      2009 Annual Research Report
  • [Presentation] ブラッドストーンのX線分析2009

    • Author(s)
      Yan-ping Zhang、桜井健次
    • Organizer
      第70回分析化学討論会
    • Place of Presentation
      和歌山大学、和歌山市
    • Related Report
      2009 Annual Research Report
  • [Presentation] 投影型X線回折イメージング法による氷の融解・凝固過程のin-situ観察2009

    • Author(s)
      水沢まり, 桜井健次
    • Organizer
      日本顕微鏡学会 第65 回学術講演会
    • Place of Presentation
      仙台国際センター、仙台市
    • Related Report
      2009 Annual Research Report
  • [Presentation] In-situ XRF and XRD movie experiments2009

    • Author(s)
      K. Sakurai, M. Mizusawa
    • Organizer
      JST international symposium on micro and trace X-ray analysis
    • Place of Presentation
      大阪市立大学、大阪市
    • Related Report
      2008 Annual Research Report
  • [Presentation] Instruments for X-ray imaging without scans -Historical review and future outlook2009

    • Author(s)
      K. Sakurai
    • Organizer
      JST international symposium on micro and trace X-ray analysis
    • Place of Presentation
      大阪市立大学、大阪市
    • Related Report
      2008 Annual Research Report
  • [Presentation] 空間的に分布のある試料のX線回折イメージング技術の開発2008

    • Author(s)
      桜井健次
    • Organizer
      日本分析化学会第57年会
    • Place of Presentation
      福岡大学、福岡市
    • Related Report
      2010 Final Research Report 2008 Annual Research Report
  • [Presentation] REALTIME XRF AND XRD IMAGING - THE INSTRUMENTATION AND THE APPLICATIONS2008

    • Author(s)
      K. Sakurai
    • Organizer
      57th Annual Denver X-ray Conference (DXC 2008)
    • Place of Presentation
      Denver Marriott Tech Center Hotel、アメリカ
    • Related Report
      2008 Annual Research Report
  • [Presentation] Realtime imaging in X-ray fluorescence and X-ray diffraction2008

    • Author(s)
      K. Sakurai, M. Mizusawa
    • Organizer
      XXI Congress and Assembly of the International Union of Crystallography (IUCr2008)
    • Place of Presentation
      Grand Cube Osaka (Osaka International Convention Center)、大阪市
    • Related Report
      2008 Annual Research Report
  • [Remarks] ホームページ等

    • URL

      http://www.nims.go.jp/xray/lab/

    • Related Report
      2010 Final Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/xray/lab/

    • Related Report
      2010 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/xray/lab/

    • Related Report
      2009 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/xray/lab/

    • Related Report
      2008 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/xray/lab/

    • Related Report
      2008 Annual Research Report
  • [Patent(Industrial Property Rights)] 酸化チタンの分析方法とこの方法を実施する酸化チタンの分析装置2011

    • Inventor(s)
      桜井健次、水沢多鶴子
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Filing Date
      2011-02-24
    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] 蛍光X線分析方法および蛍光X線分析装置2011

    • Inventor(s)
      江場宏美、桜井健次
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Filing Date
      2011-01-14
    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] X線回折分析装置およびX線回折分析方法2010

    • Inventor(s)
      桜井健次
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Filing Date
      2010-10-15
    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] X線回折分析方法およびX線回折分析装置2010

    • Inventor(s)
      桜井健次
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Filing Date
      2010-09-10
    • Related Report
      2010 Final Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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