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Study on how to extract nano fiber clusters from bamboo and their application

Research Project

Project/Area Number 20360058
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionDoshisha University

Principal Investigator

FUJII Toru  Doshisha University, 理工学部, 教授 (20156821)

Co-Investigator(Kenkyū-buntansha) OKUBO Kazuya  同志社大学, 理工学部, 教授 (60319465)
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥19,240,000 (Direct Cost: ¥14,800,000、Indirect Cost: ¥4,440,000)
Fiscal Year 2010: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Fiscal Year 2009: ¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2008: ¥10,530,000 (Direct Cost: ¥8,100,000、Indirect Cost: ¥2,430,000)
Keywordsナノコンポジット / 竹繊維 / 複合材料 / セルロースミクロフィブリル / ナノファイバークラスター / BNFC(竹ナノファイバークラスター) / ナノ繊維 / CFRP / 微細構造 / 耐久性
Research Abstract

Nano fibers called MFC (Micro-Fibrillated Cellulose) were extracted from raw bamboo as well as other plant pulps. When they are mechanically extracted, MFC forms NFC (Nano Fiber Cluster). First, PLA was reinforced with fibrillated bamboo mono-filaments/BNFC. PLA is brittle and less temperature resistance. With an increase of mechanical process for extracting, NFC becomes complicated. The degree of cluster, α was well quantitatively determined by water absorption since the surface of nano fiber cellulose being hydrophilic increased with an increase of fibrillating process. When BNFC was mixed with PLA to form compounds for improving its toughness, strength and thermal resistance, α=3.5 was suitable. Light curing epoxy was well modified in its ductility by adding a small amount of NFC. NFC was hydrophilic, and solvent replacement method such as ethanol was developed. The fracture toughness of light curing epoxy significantly increased due to a small amount of NFC, 0.5~1% dispersion. Finally, epoxy matrix of carbon fiber composites was modified with NFC up to 1% and their high cycle fatigue strength was examined under tension-tension loading. The significant extension of fatigue life was obtained when 0.3wt% NFC was mixed into epoxy resin, where the ethanol replacement method was also applied.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (45 results)

All 2011 2010 2009 2008 Other

All Journal Article (19 results) (of which Peer Reviewed: 19 results) Presentation (17 results) Book (1 results) Remarks (2 results) Patent(Industrial Property Rights) (6 results)

  • [Journal Article] Modeling of Stiffness Reduction of Conveyer Springs Subjected to Ultra High Cyclic Loading under High Humidity2011

    • Author(s)
      Takahiko YOSHI, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Key Engineering Materials

      Volume: 471-172(合併号) Pages: 975-98

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Interfacial adhesion improvement of plain woven carbon fiber reinforced epoxy filled with micro-fibrillated cellulose by addition liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABDELRAHMAN, 大窪和也, 藤井透
    • Journal Title

      Journal of Materials Science Vol 45

      Pages: 3841-3850

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of microfibrillated cellulose onmechanical properties of plain woven CFRP reinforced epoxy2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABDELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Composite Structures Vol 92

      Pages: 1999-2006

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] A Study on mechanical properties of bacterial cellulose/epoxy reinforced by plain woven carbon fiber modified with liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABDELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      COMPOSITE A Vol.41,1

      Pages: 1263-1271

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Interfacial adhesion improvement of plain woven carbon fiber reinforced epoxy filled with micro-fibrillated cellulose by addition liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa Abd ELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Journal of Materials Science

      Volume: 45 Pages: 3841-3850

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of micro-fibrillated cellulose on mechanical properties of plaino-woven CFRP reinforcxed epoxy.2010

    • Author(s)
      Mohamed H.GABR, Mostafa Abd ELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      composite Structures

      Volume: 92 Pages: 1999-2006

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A study on mechanical properties of bacterial cellulose / epoxy reinforeed by plain woven fiber modified with liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa Abd ELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      composite : part A

      Volume: 41 Pages: 1263-1271

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Stiffness reduction of woven CFRP and CFRTP spring under ultra high cyclic fatigue for vibration conveyor2010

    • Author(s)
      Takahiko YOSHI, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Advanced Materials Research

      Volume: 123-125(合併号) Pages: 217-220

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Characterization of Biomaterials Based on Microfibrillated Cellulose with Different Modifications2010

    • Author(s)
      Gabriele Rampinelli, Luca Di Landro, Toru Fujii
    • Journal Title

      Journal of Reinforced Plastics and Composites

      Volume: 29 Pages: 1793-1803

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of microfibrillated cellulose on mechanical properties of plain woven CFRP reinforced epoxy2010

    • Author(s)
      Mohamed H.GABR, Kazuya OKUBO, Mostafa ABD ELRAHMAN, Toru FUJII
    • Journal Title

      Composite Structures 92

      Pages: 1999-2006

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Interfacial Adhesion Improvement of Plain Woven Carbon Fibre Reinforced Epoxy Filled with Micro-fibrillated Cellulose by Addition Liquid Rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABD ELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Journal of materials science (掲載確定)

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A Study on mechanical properties of bacterial cellulose/epoxy reinforced by plain woven carbon fiber modified with liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABD ELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      COMPOSITE A (掲載確定)

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 摩砕した竹繊維のフィブリル化度の最適化によるPLA複合材料の機械的特性の改善2009

    • Author(s)
      田中千晶,大窪和也,藤井透
    • Journal Title

      材料 Vol.58, No.15

      Pages: 368-373

    • NAID

      130000133375

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 摩砕した竹繊維のフィブリル化度の最適化によるPLA複合材料の機械的特性の改善2009

    • Author(s)
      Ryoko Tokoro, Due Minh Vu, Kazuya Okubo, Tastuya Tanaka, Toru Fujii
    • Journal Title

      材料(日本材料学会誌) 58巻 5号

      Pages: 368-373

    • NAID

      130000133375

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Study on tensile properties and interfacial shear strength of bamboo fiber bundles. (in pressing)2009

    • Author(s)
      Hyojin Kim, Toru Fujii
    • Journal Title

      International Journal of Materials and Product Technology 36巻(掲載確定)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Improvement of fatigue strength and impact properties of plain-woven CFRP modified with Micro Fibrillated cellulose2008

    • Author(s)
      Norifumi Takagaki, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Advanced Material Research Vols.47-50

      Pages: 133-136

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of surface treatment of bamboo fiber with sodium hydroxide and silane coupling agent on mechanical properties of its composite2008

    • Author(s)
      Hyolin Kim, Kazuya Okubo, Toru Fujii
    • Journal Title

      Progress of Composites 2008 in Asia and Australasia (Proc. of ACCM-6)

      Pages: 215-218

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Improvement of fatigue strength and impact properties of plain-woven CFRP modified with Micro Fibrillated Cellulose2008

    • Author(s)
      Norifumi Takagakil, Kazuya Okubol, Toru Fujii
    • Journal Title

      Advanced Materials Research Vols. 47-50

      Pages: 133-136

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High homogenization technique for micro-fibrillated bacteria celluloseto fabricate electric testing prove disk2008

    • Author(s)
      Kaho Matsuoka, Kazuya Okubo, ToruFujii
    • Journal Title

      Proc. of the Fifth International Workshop on Green Composites 電子版

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] Improvement of Strength of Carbon/Carbon Composite by addision of Carbonized Micro Fibrillated Cellulose Into its Precursor.2011

    • Author(s)
      Yasunori Takeuchi, Kazuya OKUBO, Toru FUJII
    • Organizer
      ICMAC International Conference on Manufacturing of advanced Composites 2011
    • Place of Presentation
      Belfast Waterfront
    • Year and Date
      2011-03-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] Improvement of fatique life of CFRP pipe modified with microfibrillated cellose subjected to cyclic impact loading.2011

    • Author(s)
      Shunichi Uematsu, Kazuya OKUBO, Toru FUJII
    • Organizer
      Hybrid Materials 2011
    • Place of Presentation
      the Palais des Congre
    • Year and Date
      2011-03-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] Can Bio-nano-fibers (MFC) Extend The Fatigue Life of Carbon Fiber/epoxy Composites?2011

    • Author(s)
      Toru FUJII
    • Organizer
      Changwon National Univ., The 5th International Symposium on Advanced Mechatronics Engineering
    • Place of Presentation
      Changwon National Univ., Korea
    • Year and Date
      2011-01-06
    • Related Report
      2010 Final Research Report
  • [Presentation] Can Bio-nano-fibers (MFC) Extend The Fatigue Life of Carbon Fiber/epoxy Composites2011

    • Author(s)
      Toru FUJII
    • Organizer
      The 5th International Symposium on Advanced Mechatronics Engineering, January 6-8, 2011
    • Place of Presentation
      Changwon National Univ., Changwon-city, Korea
    • Year and Date
      2011-01-06
    • Related Report
      2010 Annual Research Report
  • [Presentation] An Application of Bamboo Fiber in Japan : Effect of Needle Punching and Spring Back Molding On Stiffness of Stampable Bamboo Fiber Sheet Processed with Pressed Mat2010

    • Author(s)
      Kazuya OKUBO, Toru FUJII, XIAOCHEN FU
    • Organizer
      5^<th> Vietnam conference on Chemical Science Hanoi University of Tecnology
    • Year and Date
      2010-11-16
    • Related Report
      2010 Final Research Report
  • [Presentation] Improvement of Strength of Bamboo Fiber Paper by Addition of MFC (Micro Fibrillated cellulose)2010

    • Author(s)
      Keisuke WAKASUGI, Kazuya OKUBO, Toru FUJII
    • Organizer
      The Sixth International Workshop on Green Composites (IWGC-6)
    • Place of Presentation
      Geumosan Hotel
    • Year and Date
      2010-09-10
    • Related Report
      2010 Final Research Report
  • [Presentation] Improvement of strength of bamboo fiber paper by addition of MFC (Micro Fibrillated cellulose)2010

    • Author(s)
      Keisuke WAKASUGI, Kazuya OKUBO, Toru FUJII
    • Organizer
      The Sixth International Workshop on Green Composites (IWGC-6)
    • Place of Presentation
      Geumosan Hotel
    • Year and Date
      2010-09-10
    • Related Report
      2010 Annual Research Report
  • [Presentation] 竹繊維を用いて抄紙された工業紙へのフェノール樹脂含侵による強度改善2009

    • Author(s)
      若杉景祐, 大窪和也, 藤井透
    • Organizer
      第1回自動車コンポジットシンポジウム
    • Place of Presentation
      同志社大学 寒梅館(京都市)
    • Year and Date
      2009-12-12
    • Related Report
      2009 Annual Research Report
  • [Presentation] 炭素繊維強化炭素複合材料(C/Cコンポジット)の微細繊維添加による機械的特性の改善2009

    • Author(s)
      竹内康徳, 小武内清貴, 大窪和也, 藤井透, 仲辻毅
    • Organizer
      日本材料学会,第1回自動車用途コンポジットシンポジウム
    • Place of Presentation
      同志社大学 寒梅館(京都市)
    • Year and Date
      2009-12-12
    • Related Report
      2009 Annual Research Report
  • [Presentation] 竹繊維を用いた紙の低濃度フェノール樹脂の天下による強度改善2009

    • Author(s)
      若杉景祐, 大窪和也, 藤井透
    • Organizer
      第19回日本MRS学術シンポジウム
    • Place of Presentation
      横浜市開港記念会館
    • Year and Date
      2009-12-08
    • Related Report
      2009 Annual Research Report
  • [Presentation] Application of natural MFC (Micro Fibrillated cellulose) to improve fatigue life of plain CFRP2009

    • Author(s)
      Tomoya YASHIRO, Kazuya Okubo, Toru Fujii
    • Organizer
      JISSE-11 (11th Japan International SAMPE Sympo.& Exhibition, "Advanced Material Technology for Sustainable Development"
    • Place of Presentation
      Tokyo
    • Year and Date
      2009-11-27
    • Related Report
      2010 Final Research Report
  • [Presentation] Application of natural(Micro Fibrillated cellulose)to improve fatigue life of plain CFRP2009

    • Author(s)
      Tomoya YASHIRO, Kazuya Okubo Toru Fujii
    • Organizer
      JISSE-11(11th Japan International SAMPE Symposium & Exhibition
    • Place of Presentation
      Tokyo Big Sight, Tokyo
    • Year and Date
      2009-11-27
    • Related Report
      2009 Annual Research Report
  • [Presentation] Can Micro-fibrillated Cellulose(MFC)fibers extend the fatigue life of carbon fabric composites?2009

    • Author(s)
      Toru FUJII
    • Organizer
      11th Conference on Materials Science and Technology
    • Place of Presentation
      Ho Chi Minh City Univ.Of Tech.
    • Year and Date
      2009-10-22
    • Related Report
      2009 Annual Research Report
  • [Presentation] 竹単繊維を用いて沙紙する紙の比剛性に及ぼす竹齢の影響2009

    • Author(s)
      大窪和也, 藤井透, 鈴木茂之
    • Organizer
      日本機械学会,2009年度年次大会
    • Place of Presentation
      岩手大学キャンパス(盛岡市)
    • Year and Date
      2009-09-16
    • Related Report
      2009 Annual Research Report
  • [Presentation] フィブリル化アラミド繊維により強化した圧縮化セルロースの機械的および熱特性2009

    • Author(s)
      若杉景祐, 大窪和也, 藤井透
    • Organizer
      第58期日本材料学会学術講演会
    • Place of Presentation
      愛媛大学(松山市)
    • Year and Date
      2009-05-24
    • Related Report
      2009 Annual Research Report
  • [Presentation] Effect of needle punching and PVA treatment on mechanical properties of stamp able sheet processed with bamboo fiber mat2009

    • Author(s)
      Xiaochen Fu, Kazuya OKUBO, Toru FUJII
    • Organizer
      Third Japan-China Joint Seminar on Green Composites
    • Place of Presentation
      Donghua University, Shanghai
    • Related Report
      2009 Annual Research Report
  • [Presentation] Application of High Homogenization Technique to Fabrication of Electric Testing Prove Disk Using Micro-Fibrillated Bacteria Cellulose2008

    • Author(s)
      Kaho MATSUOKA, Kazuya OKUBO, Toru FUJII
    • Organizer
      the Third International Conference on Material and Processing MSEC ICMP2008-72473
    • Place of Presentation
      Northwestern University, Evanston, Illinois, USA
    • Related Report
      2010 Final Research Report
  • [Book] 竹の基礎科学と高度利用技術(ISBN 978-4-7813-0027-6)2008

    • Author(s)
      藤井透(監修, 著), 内村悦三, 柴田昌三, 坂本正弘, ほか
    • Total Pages
      236
    • Publisher
      シーエムシー出版
    • Related Report
      2008 Annual Research Report
  • [Remarks] ホームページ等

    • URL

      http://engineering.doshisha.ac.jp/kenkyu/labo/mech/me_02/index.html

    • Related Report
      2010 Final Research Report
  • [Remarks]

    • URL

      http://engineering.doshisha.ac.jp/kenkyu/labo/mech/me_02/index.html

    • Related Report
      2010 Annual Research Report
  • [Patent(Industrial Property Rights)] 炭素繊維強化複合材料及びその製造方法2010

    • Inventor(s)
      藤井透.大窪和也.小武内清貴.竹内康徳.中辻毅
    • Industrial Property Rights Holder
      学校法人同志社サンスター技研株式会社
    • Industrial Property Number
      2010-188976
    • Filing Date
      2010-08-25
    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] 樹脂組成物の製造方法及び混練押出機2010

    • Inventor(s)
      藤井透、大窪和也、植松峻一、大森一寛、御園和則
    • Industrial Property Rights Holder
      学校法人同志社株式会社神戸製鋼所
    • Filing Date
      2010-01-18
    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] 繊維強化複合体2010

    • Inventor(s)
      藤井透、大窪和也、植松峻一、大森一寛、御園和則
    • Industrial Property Rights Holder
      学校法人同志社美津濃株式会社
    • Filing Date
      2010-01-22
    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] 特許 MFCをC/C複合材料用プリフォーム材への添加による高強度C/C素材2010

    • Inventor(s)
      藤井透, ほか
    • Industrial Property Rights Holder
      同志社大学、サンスター技研(株)
    • Industrial Property Number
      2009-194259
    • Filing Date
      2010-04-22
    • Related Report
      2010 Annual Research Report
  • [Patent(Industrial Property Rights)] 特許 炭素繊維強化炭素複合材料及びその製造法2010

    • Inventor(s)
      藤井透, ほか
    • Industrial Property Rights Holder
      同志社大学、サンスター技研(株)
    • Filing Date
      2010-08-26
    • Related Report
      2010 Annual Research Report
  • [Patent(Industrial Property Rights)] 炭素繊維強化炭素複合材料及びその製造方法2009

    • Inventor(s)
      藤井透.大窪和也.小武内清貴.竹内康徳.中辻毅
    • Industrial Property Rights Holder
      学校法人同志社サンスター技研株式会社
    • Industrial Property Number
      2009-194259
    • Filing Date
      2009-08-25
    • Related Report
      2010 Final Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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