• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

ADF-STEM observation of polymer composites without staining

Research Project

Project/Area Number 20550188
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Polymer/Textile materials
Research InstitutionKyoto University

Principal Investigator

ISODA Seiji  Kyoto University, 物質ー細胞統合システム拠点, 研究員(WPI) (00168288)

Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2010: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2009: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2008: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Keywords高分子 / STEM / ADF / コントラスト / 無染色 / HAADF
Research Abstract

As an electron microscopic method on polymer composites without staining, annular dark-field scanning transmission electron microscopy (ADF-STEM) was examined on its effectiveness for making contrast and established for a quantitative analysis of nanoscale structures. Relatively low-angle scattering electrons were found to be available for the formation of contrast owing to a density difference, which was confirmed by image simulation. Thus, the density of nanoscale phases was expected to be identified by ADF-STEM such as the case of identification of glass transition temperatures for micro-phases.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (24 results)

All 2011 2010 2009 2008

All Journal Article (16 results) (of which Peer Reviewed: 15 results) Presentation (8 results)

  • [Journal Article] Analytical electron microscopy investigation of elemental composition and bonding structure at the Sb-doped Ni-fully-silicide/SiO_2 interface2011

    • Author(s)
      N.Kawasaki, N.Sugiyama, Y.Otsuka, H.Hashimoto, H.Kurata, S.Isoda
    • Journal Title

      Journal of Applied Physics 109

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Study of Structures at the Boundary and Defects in Organic Thin Films of Perchlorocoronene by High-resolution and Analytical Transmission Electron Microscopy2010

    • Author(s)
      M.Koshino, H.Kurata, S.Isoda
    • Journal Title

      Ultramicroscopy 110

      Pages: 1465-1474

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Gelation behavior by the lanthanoid adsorption of the cyanobacterial extracellular polysaccharide sacran2010

    • Author(s)
      M.K.Okajima, T.Higashi, R.Asakawa, T.Mitsumata, D.Kaneko, T.Kanekol, T.Ogawa, Hi.Kurata, S.Isoda
    • Journal Title

      Biomacromolecules 1 1(11)

      Pages: 3172-3177

    • Related Report
      2010 Final Research Report
  • [Journal Article] HRTEM and ADF-STEM of Precipitates at Peak-Ageing in Cast A 563 Aluminium Alloy2010

    • Author(s)
      N.Chomsaeng, M.Haruta, T.Chairuangsri, H.Kurata, S.Isoda, M.Shiojiri
    • Journal Title

      Journal of Alloys and Compounds 496

      Pages: 478-487

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Study of Structures at the Boundary and Defects in Organic Thin Films of Perchlorocoronene by High-resolution and Analytical Transmission Electron Microscopy2010

    • Author(s)
      Masanori Koshino, Hiroki Kurata, Seiij Isoda
    • Journal Title

      Ultramicroscopy

      Volume: 110 Pages: 1465-1474

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] HRTEM and ADF-STEM of Precipitates at Peak-Ageing in Cast A 563 Aluminium Alloy2010

    • Author(s)
      N.Chomsaeng, M.Haruta, T.Chairuangsri, H.Kurata, S.Isoda, M.Shiojiri
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 496 Pages: 478-487

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effects of Electron channeling in HAADF-STEM intensity in La_2CuSnO_62009

    • Author(s)
      M.Haruta, H.Kurata, H.Komatsu, Y.Shimakawa, S.Isoda
    • Journal Title

      Ultramicroscopy 109

      Pages: 361-367

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Local analysis of the edge-dislocation core in BaTiO_3 thin film by STEM-EELS2009

    • Author(s)
      H.Kurata, S.Isojima, M.Kawai, Y.Shimakawa, S.Isoda
    • Journal Title

      J.Microscopy 236

      Pages: 128-131

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] HAADF-STEM analysis of layered double Perovskite La_2CuSnO_6 grow epitaxially2009

    • Author(s)
      M.Haruta, H.Komatsu, H.Kurata, M.Azuma, Y.Shimakawa, S.Isoda
    • Journal Title

      J.Microscopy 236

      Pages: 100-103

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Site-resolved oxygen K-edge ELNES of layered double perovskite La_2CuSnO_62009

    • Author(s)
      M.Haruta, H.Kurata, H.Komatsu, Y.Shimakawa, S.Isoda
    • Journal Title

      Phys.Rev., B 80

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Local analysis of the edge-dislocation core in BaTiO3 the film by STEM-EELS2009

    • Author(s)
      H.Kurata, S.Isojima, M.Kawai, Y.Shimakawa, S.Isoda
    • Journal Title

      J. Microscopy 236

      Pages: 128-131

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] HAADF-STEM analysis of layered double Perovskite La2CuSnO6 grow epitaxially2009

    • Author(s)
      M.Haruta, H.Komatsu.H.Kurata, M.Azuma, Y.Shimakawa, S.
    • Journal Title

      J. Microscopy 236

      Pages: 100-103

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Site-resolved oxygen K-edge ELNES of layered double perovskite La2CuSnO62009

    • Author(s)
      M.Haruta, H.Kurata, H.Komatsu, Y.Shimakawa, S.Isoda
    • Journal Title

      Phys. Rev., B 80

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High Resolution ADF-STEM Imaging Application for Organic Crystals2008

    • Author(s)
      M.Haruta, K.Yoshida, H.Kurata, S.Isoda
    • Journal Title

      Mol.Cryst. & Liq.Cryst 492

      Pages: 200-209

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis and Microphase-Seperated Structure of poly (Tricyclodecyl Vinyl Ether)-block-Poly(n-Butyl Vinyl2008

    • Author(s)
      Tamotsu Hashimoto, Takeshi Namikoshi, Satoshi Irie, Michio
    • Journal Title

      Journal of Polymer Science, Part A, Polymer Chemistry 46

      Pages: 1902-1906

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] HIGH RESOLUTION ADF-STEM IMAGING APPLICATION FOR ORGANIC CRYSTALS2008

    • Author(s)
      Mitsutaka Haruta, Kaname Yoshida, Hiroki Kurata, Seiji Isoda
    • Journal Title

      Mol. Cryst. & Liq. Cryst 492

      Pages: 200-209

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] Direct Imaging of Microphase -Separated Structure of Poly(Tri cyclodecyl Vinyl Ether)-block -Poly(N-Butyl Vinyl Ether) by ADF-STEM2010

    • Author(s)
      R.Aso, M.Haruta, T.Namikoshi, T.Hashimoto, H.Kurata, S.Isoda
    • Organizer
      International Congress of Microscopy IMC 17
    • Place of Presentation
      Rio de Janeiro, Brazil
    • Year and Date
      2010-09-22
    • Related Report
      2010 Final Research Report
  • [Presentation] Direct Imaging of Microphase-Separated Structure of Poly (Tricyclodecyl Vinyl Ether)-block-Poly(N-Butyl Vinyl Ether) by ADF-STEM2010

    • Author(s)
      R.Aso, M.Haruta, T.Namikoshi, T.Hashimoto, H.Kuala, S.Isoda
    • Organizer
      International Congress of Microscopy IMC 17
    • Place of Presentation
      Rio de Janeiro, Brazil
    • Year and Date
      2010-09-22
    • Related Report
      2010 Annual Research Report
  • [Presentation] Interface Structure of Gold Particles on TiO_2 Anatase2010

    • Author(s)
      D.Nagamatsu, T.Nemoto, H.Kurata, J.Jiu, M.Adachi, M.Tsujimoto, S.Isoda
    • Organizer
      8th Japanese-Polish Joint Seminar on Micro and Nano Analysis
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2010-09-06
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] Epitaxial 1D-polymerization on Substrate2010

    • Author(s)
      D.Takajo, T.Nemoto, S.Isoda
    • Organizer
      The 3rd International Symposium on Polymer Morphology & Microscopy
    • Place of Presentation
      Changchun, China
    • Year and Date
      2010-06-14
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] HAADF-STEMによる無染色有機物の観察2010

    • Author(s)
      麻生亮太郎、浪越毅、橋本保、治田充貴、倉田博基、磯田正二
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋
    • Year and Date
      2010-05-25
    • Related Report
      2010 Final Research Report
  • [Presentation] Electron Crystallography of Organic Materials by TEM2009

    • Author(s)
      磯田正二
    • Organizer
      NSYSU-KU Bilateral Symposium on Materials Chemistry
    • Place of Presentation
      Kaohsiung, Taiwan
    • Year and Date
      2009-09-23
    • Related Report
      2010 Final Research Report 2009 Annual Research Report
  • [Presentation] Electron Crystallography of Organic Materials by TEM2009

    • Author(s)
      T.Ogawa, S.Isoda
    • Organizer
      The 26th MST Annual Conference
    • Place of Presentation
      Chiangmai, Thai
    • Year and Date
      2009-01-29
    • Related Report
      2010 Final Research Report 2008 Annual Research Report
  • [Presentation] Electron Microscopy for Organized Molecules2008

    • Author(s)
      磯田正二, 倉田博基
    • Organizer
      International Conference on Advanced Functional Polymers and Self-Organized Materials
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2008-09-24
    • Related Report
      2010 Final Research Report 2008 Annual Research Report

URL: 

Published: 2008-04-01   Modified: 2016-04-21  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi