ADF-STEM observation of polymer composites without staining
Project/Area Number |
20550188
|
Research Category |
Grant-in-Aid for Scientific Research (C)
|
Allocation Type | Single-year Grants |
Section | 一般 |
Research Field |
Polymer/Textile materials
|
Research Institution | Kyoto University |
Principal Investigator |
ISODA Seiji Kyoto University, 物質ー細胞統合システム拠点, 研究員(WPI) (00168288)
|
Project Period (FY) |
2008 – 2010
|
Project Status |
Completed (Fiscal Year 2010)
|
Budget Amount *help |
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2010: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2009: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2008: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
|
Keywords | 高分子 / STEM / ADF / コントラスト / 無染色 / HAADF |
Research Abstract |
As an electron microscopic method on polymer composites without staining, annular dark-field scanning transmission electron microscopy (ADF-STEM) was examined on its effectiveness for making contrast and established for a quantitative analysis of nanoscale structures. Relatively low-angle scattering electrons were found to be available for the formation of contrast owing to a density difference, which was confirmed by image simulation. Thus, the density of nanoscale phases was expected to be identified by ADF-STEM such as the case of identification of glass transition temperatures for micro-phases.
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Report
(4 results)
Research Products
(24 results)