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Increase in Adhesion Strength of SiC Film with Super Low Friction Coefficient by Formation Technique of Nano-precipitates at Interface

Research Project

Project/Area Number 20560134
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Design engineering/Machine functional elements/Tribology
Research InstitutionHiroshima University

Principal Investigator

KATO Masahiko  Hiroshima University, 大学院・工学研究院, 准教授 (70274115)

Co-Investigator(Kenkyū-buntansha) SUGETA Atsushi  広島大学, 大学院・工学研究院, 教授 (60162913)
AKEBONO Hiroyuki  広島大学, 大学院・工学研究院, 助教 (50447215)
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2010: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2009: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2008: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
KeywordsSiC薄膜 / はく離強度 / 界面制御 / アンカー効果 / 微細円錐突起物 / SiC / スパッタ / はく離エネルギ / 微細円錐状突起物
Research Abstract

In this research, improvement of delamination strength of sputtered film was attempted by utilizing an anchor effect of fine conical precipitates formed at interface. Fine conical precipitates were formed on a tool steel substrate (JIS : SKH51) by sputter etching treatment under various conditions, and the relationship between the etching condition and shape of the precipitates was investigated. The result showed that height and radius of the precipitates was controllable by etching time, power, and pressure. The delamination strength of the amorphous SiC film formed on the substrates with fine conical precipitates using helicon sputtering apparatus was measured by micro edge-indent method. The delamination strength of the SiC film varied with the size and density of the precipitates, and exceeded that of un-etched specimens, when appropriate size precipitates were formed on the substrate.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (10 results)

All 2010 2009 2008 Other

All Journal Article (3 results) (of which Peer Reviewed: 3 results) Presentation (6 results) Remarks (1 results)

  • [Journal Article] Measurement of Delamination Energy of Sputtered SiC Film Coated on Tool Steel Substrate2010

    • Author(s)
      Masahiko KATO, Koumei FUJIOKA, Hiroyuki AKEBONO, Atsushi SUGETA
    • Journal Title

      Journal of JSEM vol.10

      Pages: 141-145

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Measurement of Delamination Energy of Sputtered SiC Film Coated on Tool Steel Substrate2010

    • Author(s)
      Masahiko KATO, Koumei FUJIOKA, Hiroyuki AKEBONO, Atsushi SUGETA
    • Journal Title

      Journal of JSEM

      Volume: 10 Pages: 141-145

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of Intermediate Layer on Wear-delamination Life of Low-frictional SiC-2.6mass% Ti Film Sputter-deposited on Titanium Substrate2010

    • Author(s)
      Jin-Hua Zheng, Masahiko Kato, Keijiro Nakasa
    • Journal Title

      Surface & Coatings Technology

      Volume: 205 Pages: 2532-2537

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] SiCスパッタ薄膜のはく離強度に及ぼす界面微細突起物の影響2010

    • Author(s)
      加藤昌彦, 林真人, 曙紘之, 菅田淳
    • Organizer
      日本材料学会第59期学術講演会
    • Place of Presentation
      北海道大学
    • Year and Date
      2010-05-22
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] Improvement of Delamination Energy of Sputtered SiC Film by Forming Conical Precipitates at Interface2009

    • Author(s)
      加藤昌彦, 林真人, 曙紘之, 菅田淳
    • Organizer
      4th International Symposium on Advanced Fluid/Solid Science and Technology in Experimental Mechanics
    • Place of Presentation
      Niigata
    • Year and Date
      2009-11-28
    • Related Report
      2010 Final Research Report
  • [Presentation] Improvement of Delamination Energy of Sputtered SiC Film by Forming Conical Precipitates at Interface2009

    • Author(s)
      加藤昌彦, 林真人, 曙紘之, 菅田淳
    • Organizer
      4th International Symposium on Advanced Fluid/Solid Science and Technology in Experimental Mechanics
    • Place of Presentation
      新潟市
    • Year and Date
      2009-11-28
    • Related Report
      2009 Annual Research Report
  • [Presentation] 下地表面に形成させた微細突起物がSiC薄膜のはく離強度に及ぼす影響2009

    • Author(s)
      林真人, 加藤昌彦, 曙紘之, 菅田淳
    • Organizer
      日本鉄鋼協会・日本金属学会 中国四国支部 鉄鋼第52回・金属第49回 合同講演大会
    • Place of Presentation
      高松市
    • Year and Date
      2009-08-06
    • Related Report
      2009 Annual Research Report
  • [Presentation] マイクロエッジインデント法によるSiC薄膜のはく離強度評価および界面微細円錐状突起物がSiC薄膜のはく離強度に及ぼす影響2008

    • Author(s)
      加藤昌彦
    • Organizer
      日本材料学会第4回マイクロマテリアルシンポジウム
    • Place of Presentation
      東京都文京区
    • Year and Date
      2008-09-24
    • Related Report
      2008 Annual Research Report
  • [Presentation] 微細円錐状突起物を形成させた基板に成膜したSiC薄膜のはく離強度評価2008

    • Author(s)
      加藤昌彦
    • Organizer
      日本材料学会第57期学術講演会
    • Place of Presentation
      鹿児島市
    • Year and Date
      2008-05-24
    • Related Report
      2008 Annual Research Report
  • [Remarks] ホームページ等

    • Related Report
      2010 Final Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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