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Surface Microstructure Control of Cr-Mo Steels by High-Pressure Gas Cooling after Vacuum Carbonitriding

Research Project

Project/Area Number 20569003
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research Institution仙台高等専門学校 (2009-2010)
Miyagi National College of Technology (2008)

Principal Investigator

WATANABE Youichi  仙台高等専門学校, マテリアル環境工学科, 教授 (60515154)

Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥3,660,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥660,000)
Fiscal Year 2010: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2009: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2008: ¥800,000 (Direct Cost: ¥800,000)
Keywords鉄鋼材料 / 浸炭窒化 / 窒素 / ガス冷却 / ダイヤモンドライクカーボン(DLC) / 面圧疲れ / ピッティング / 真空浸炭窒化 / 熱伝達率 / 熱処理シミュレーション / 摩擦係数 / 窒素含有マルテンサイト / 窒化物 / ショットピーニング / 焼戻し軟化抵抗 / ピッチング / 残留オーステナイト / 加圧ガス焼入れ / 窒素マルテンサイト
Research Abstract

We have investigated surface microstructures of high silicon containing Cr-Mo steel carbonitrided to high nitrogen content and quenched using cooling power-controlled N2 gas. Pitting resistance of the steel DLC(Diamond-like-carbon)-coated by ion plating process after the carbonitriding and quenching have been investigated under the conditions of a high Hertzian pressure(Pmax) of up to 4.5GPa with slipping of-60% and a 95℃oil-lubricating using roller-pitting tester. XRD analysis shows that the surface hardness and softening resistance during tempering are improved by precipitation ofεand/orγ' nitrides from nitrogen-solute martensite at the carbonitrided layer. Pitting lifetime of the steel DLC-coated after the carobonitriding is approximately 6 times longer than that of non-DLC coated one when Pmax is 4.2GPa. This excellent pitting endurance can be explained from both the DLC adhesion and the friction coefficient decreased by approximately 17% due to the DLC coating. Thus, this hybrid treatment will be expected to be able to applied to the several super-high pressure and/or high revolution speed gears for next generation automobiles.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (21 results)

All 2012 2011 2010 2009 2008

All Journal Article (9 results) (of which Peer Reviewed: 4 results) Presentation (12 results)

  • [Journal Article] 真空浸炭窒化焼入れ後DLC被膜処理した高強度歯車用鋼の耐ピッティング性2012

    • Author(s)
      渡邊陽一,橋本裕絵,大野航,濱本浩幸,堤奈保,中村翔,全永夏
    • Journal Title

      仙台高専研究紀要

      Volume: 第48号 Pages: 5-12

    • NAID

      110009464581

    • Related Report
      2010 Final Research Report
  • [Journal Article] 真空浸炭窒化した高強度歯車用鋼のDLC被覆による摺動および疲労特性の改善2012

    • Author(s)
      濱本浩幸,中村翔,星野新一,渡邊陽一,全永夏
    • Journal Title

      日本パーカライジング技報

      Volume: 24 Pages: 35-41

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 真空浸炭窒化焼入れ後DLC被膜処理した高強度歯車用鋼の耐ピッティング性2012

    • Author(s)
      渡邊陽一, 橋本裕絵, 大野航, 濱本浩幸, 堤奈保, 中村翔, 全永夏
    • Journal Title

      仙台高等専門学校紀要

      Volume: 48号(掲載確定)

    • NAID

      110009464581

    • Related Report
      2010 Annual Research Report
  • [Journal Article] 真空浸炭窒化した高強度歯車用鋼のDLC被覆による摺動および疲労特性の改善2012

    • Author(s)
      濱本浩行, 中村翔, 星野新一, 渡邊陽一, 全永夏
    • Journal Title

      日本パーカーライジング技報

      Volume: No.24 Pages: 35-41

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 自動車歯車の面圧疲れ対策の現状と将来動向2011

    • Author(s)
      渡邊陽一
    • Journal Title

      熱処理

      Volume: 51 Pages: 108-113

    • NAID

      10029407727

    • Related Report
      2010 Annual Research Report 2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 浸炭2010

    • Author(s)
      渡邊陽一
    • Journal Title

      表面技術 61

      Pages: 179-180

    • NAID

      10026348513

    • Related Report
      2009 Annual Research Report
  • [Journal Article] Effective Heat Treatment Processes and High Strength Steel designed to improve the Contact Fatigue Strength of Automotive Powertrain Parts2009

    • Author(s)
      渡邊陽一
    • Journal Title

      NETSU SHORT Proc.of the 17^<th> IFHTSE Congress 2008 49

      Pages: 35-42

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 表面硬化鋼部品の熱処理CAE2009

    • Author(s)
      渡邊陽一
    • Journal Title

      特殊鋼 58

      Pages: 77-102

    • Related Report
      2009 Annual Research Report
  • [Journal Article] クリーンファクトリー化に貢献する次世代真空熱処理技術2009

    • Author(s)
      渡邊陽一
    • Journal Title

      日刊工業新聞 朝刊 5月22日

      Pages: 10-10

    • Related Report
      2009 Annual Research Report
  • [Presentation] 真空浸炭窒化後DLCコーティングしたCr-Mo鋼の耐ピッティング性2011

    • Author(s)
      渡邊陽一,橋本裕絵,濱本浩幸,堤奈保,中村翔, Youngha Jun
    • Organizer
      第71回日本熱処理技術協会春季講演大会
    • Place of Presentation
      東京工業大学
    • Related Report
      2010 Final Research Report
  • [Presentation] The present status and future trend of technologies for improving performance of automotive power-train steel parts in Japan2011

    • Author(s)
      Youichi WATANABE
    • Organizer
      The fall seminar on heat treatment of materials by the Korean Society for Heat Treatment
    • Place of Presentation
      Korea Polytechnic Univ., Shihung-city, Korea.
    • Related Report
      2010 Final Research Report
  • [Presentation] 真空浸炭窒化後DLCコーティングしたCr-Mo鋼の耐ピッティング性2011

    • Author(s)
      渡邊陽一, 橋本裕絵, 濱本浩幸, 堤奈保, 中村翔, Youngha Jun
    • Organizer
      第71回日本熱処理技術協会講演大会
    • Place of Presentation
      東京工業大学(大岡山キャンパス)
    • Related Report
      2010 Annual Research Report
  • [Presentation] プラズマ高濃度浸炭焼入れ/DLC膜によるピッチング強度および曲げ疲労強度の向上2011

    • Author(s)
      横尾晃央, 作田英久, 山本啓介, 金山信幸, 渡邊陽一
    • Organizer
      第71回日本熱処理技術協会講演大会
    • Place of Presentation
      東京工業大学(大岡山キャンパス)
    • Related Report
      2010 Annual Research Report
  • [Presentation] The Present Status and Future Trend of Technologies for Improving Performance of Automotive Power-train Steel Parts in Japan2011

    • Author(s)
      Youichi Watanabe
    • Organizer
      the Fall Seminar on Heat Treatment of Materials by the Korean Society for Heat Treatment
    • Place of Presentation
      Korea Polytechnic Univ., Shihung city, Korea(invited)
    • Related Report
      2010 Annual Research Report
  • [Presentation] 自動車歯車の面圧疲労対策の現状と将来動向2010

    • Author(s)
      渡邊陽一
    • Organizer
      日本熱処理技術協会・西部支部、平成21年度特定テーマ講習会
    • Place of Presentation
      大阪国際会議場
    • Year and Date
      2010-02-12
    • Related Report
      2009 Annual Research Report
  • [Presentation] 真空浸炭の実際-真空浸炭および周辺技術の現状と将来-2009

    • Author(s)
      渡邊陽一
    • Organizer
      日本熱処理技術協会・熱処理セミナー,(2009年度第二回)
    • Place of Presentation
      東京工業大学(大岡山キャンパス)
    • Year and Date
      2009-09-03
    • Related Report
      2009 Annual Research Report
  • [Presentation] 高機能・高精度機械部品の次世代型生産技術開発の調査検討2009

    • Author(s)
      井上達雄、巨東英、奈良崎道治、吉田総仁、上原拓也、渡邊陽一、岡村一男、七野勇人、金森英夫、市谷克実
    • Organizer
      平成21年度(財)製造科学技術センター・IMSアイデアファクトリー総会
    • Place of Presentation
      虎ノ門パストラル(東京)
    • Year and Date
      2009-07-07
    • Related Report
      2009 Annual Research Report
  • [Presentation] Effect of Shot Peening after Carbonitriding on the Contact fatigue Strength of Chromium-containing Steel2008

    • Author(s)
      A. Golobolorodko, Y. Watanabe
    • Organizer
      Conference proceedings of the 10^<th> ICSP
    • Place of Presentation
      明治大学アカデミーコモン
    • Related Report
      2008 Annual Research Report
  • [Presentation] Effective Heat Treatment Processes and High Strength Steel designed to improve the Contact Fatigue Strength of Automotive Powertrain Parts2008

    • Author(s)
      Youichi Watanabe
    • Organizer
      Proceedings of the 17^<th> IFHTSE. Congress 2008
    • Place of Presentation
      神戸国際会議センター
    • Related Report
      2008 Annual Research Report
  • [Presentation] Optimization of Step Gas Quenching after Low Pressure Carburizing by Numerical Simulation with Experimental Validation2008

    • Author(s)
      Q. Ming, T. Sugimoto, Y. Watanabe
    • Organizer
      Proceedings of the 17^<th> IFHTSE Congress 2008
    • Place of Presentation
      神戸国際会議センター
    • Related Report
      2008 Annual Research Report
  • [Presentation] Practical Model to Predict Heat Transfer Coefficient in High Pressured Gas Quenching2008

    • Author(s)
      H. Nagami, K. Okamura, T. Sugimoto, Y. Watanabe, M. Narazaki
    • Organizer
      Proceedings of the 17^<th> IFHTSE Congress 2008
    • Place of Presentation
      神戸国際会議センター
    • Related Report
      2008 Annual Research Report

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Published: 2008-04-01   Modified: 2016-11-18  

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