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Development of high-quality biocompatible thin film coating method by laser beam and its application to implant materials

Research Project

Project/Area Number 20612009
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Quantum beam science
Research InstitutionKinki University

Principal Investigator

NAKAYAMA Takeyoshi  Kinki University, 理工学部, 教授 (60023313)

Co-Investigator(Kenkyū-buntansha) HASHISHIN Yuichi  近畿大学, 理工学部, 准教授 (90156266)
MATSUTANI Takaomi  近畿大学, 理工学部, 講師 (00411413)
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2010: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2009: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2008: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Keywords表面改質 / 生体親和性材料 / ハイドロキシアパタイト / チタン / インプラント材料 / コーティング / パルスレーザーアブレーション / レーザーアシストレーザーアブレーション / レーザーアシスレーザーアブレーション
Research Abstract

A method using two laser beams, namely the laser-assisted laser ablation (LALA) method, was developed for HAp coating of Ti substrates. This method meets the requirements for a HAp coating on implants, namely, high crystallinity, high adhesion strength, and not exceeding a certain thickness. By controlling the delay time of assist laser irradiation, a strongly-adhering, high-quality HAp coating was obtained. In the present method, crystallization of the deposited HAp is achieved by assist laser irradiation. No additional heat-treatment is required, which prevents oxidation of the substrate. The present method meets all the requirements for a HAp coating mentioned above in a single process. For these reasons, the LALA method can expect as an excellent method for a HAp coating on implants.
It has been also achieved to enhance adhesion strength of diamond-like carbon (DLC) thin film on Ti substrate.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (24 results)

All 2010 2009 2008

All Journal Article (10 results) (of which Peer Reviewed: 6 results) Presentation (14 results)

  • [Journal Article] 生体埋込金属材料のDLCコーティングによる高機能化2010

    • Author(s)
      久野秀剛、松谷貴臣、中野人志、塚本雅裕、中山斌義
    • Journal Title

      レーザー学会第402回研究会報告 RTM-10-20

      Pages: 1-6

    • NAID

      10026690955

    • Related Report
      2010 Final Research Report
  • [Journal Article] 生体埋め込み金属材料のDLCコーティングによる高機能化2010

    • Author(s)
      久野秀剛, ほか
    • Journal Title

      レーザー学会第402回研究会報告

      Volume: RTM-10-20 Pages: 1-6

    • Related Report
      2010 Annual Research Report
  • [Journal Article] Laser-Assisted Laser Ablation Method for High-Quality Hydroxyapatite Coating onto Titanium Substrate2009

    • Author(s)
      H.Katayama, M.Katto, T.Nakayama
    • Journal Title

      Surf.& Coat.Tech. Vol.204

      Pages: 135-140

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Characteristics of Hydroxyapatite Films Coated on a Titanium Substrate by Laser-Assisted Laser Ablation2009

    • Author(s)
      Toshihisa Miyazaki, Hirotaka Katayama, Takeyoshi Nakayama
    • Journal Title

      Advances in Applied Plasma Science Vol.7

      Pages: 277-278

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 紫外パルスレーザー光を用いて作製したHAp被膜の密着性評価2009

    • Author(s)
      宮崎聡久、久野秀剛、片山博貴、中山斌義
    • Journal Title

      レーザー学会第389回研究会報告 RTM-09-19

      Pages: 7-11

    • NAID

      10025078669

    • Related Report
      2010 Final Research Report
  • [Journal Article] Characteristics of Hydroxyapatite Films Coated on a Titanium Substrate by Laser-Assisted Laser Ablation2009

    • Author(s)
      宮崎聡久
    • Journal Title

      Advances in Applied Plasma Science Vol.7

      Pages: 277-278

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Laser-Assisted Laser Ablation Method for High-Quality Hydroxyapatite Coating onto Titanium Substrate2009

    • Author(s)
      H.Katayama
    • Journal Title

      Surf.& Coat.Tech. Vol.204

      Pages: 135-140

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 紫外パルスレーザー光を用いて作製したHAp被膜の密着性評価2009

    • Author(s)
      宮崎聡久
    • Journal Title

      レーザー学会第389回研究会報告 RTM-09-19

      Pages: 7-11

    • Related Report
      2009 Annual Research Report
  • [Journal Article] LALA法により作製されたTi基板上のHAp被膜の密着性について2008

    • Author(s)
      片山博貴、中山斌義
    • Journal Title

      日本レーザー医学会誌 28巻

      Pages: 362-366

    • NAID

      10024165698

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] PLD法によるDLC膜形成-Si-Cターゲットを用いた中間層の形成2008

    • Author(s)
      片山博貴、北川正憲、溝口佳宏、中山斌義
    • Journal Title

      レーザー研究 36巻

      Pages: 37-38

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Presentation] レーザーを用いた生体硬組織代替材料の開発2010

    • Author(s)
      中山斌義
    • Organizer
      電気学会関西支部講演会
    • Place of Presentation
      中央電気倶楽部、大阪
    • Year and Date
      2010-12-03
    • Related Report
      2010 Final Research Report
  • [Presentation] レーザーを用いた生体硬組織代替材料の開発2010

    • Author(s)
      中山斌義
    • Organizer
      電気学会関西支部講演会
    • Place of Presentation
      大阪、中央電気倶楽部
    • Year and Date
      2010-12-03
    • Related Report
      2010 Annual Research Report
  • [Presentation] 生体埋込金属材料のDLCコーティング2010

    • Author(s)
      久野秀剛、松谷貴臣、中野人志、塚本雅弘、中山斌義
    • Organizer
      平成22年電気関係学会関西連合大会
    • Place of Presentation
      立命館大学びわこ・くさつキャンパス、草津
    • Year and Date
      2010-11-13
    • Related Report
      2010 Final Research Report
  • [Presentation] 生体埋込金属材料のDLCコーティング2010

    • Author(s)
      久野秀剛、松谷貴臣、中野人志、塚本雅弘、中山斌義
    • Organizer
      平成22年電気関係学会関西連合大会
    • Place of Presentation
      草津、立命館大学びわこ・くさつキャンパス
    • Year and Date
      2010-11-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] 生体埋込金属材料のDLCコーティングによる高機能化2010

    • Author(s)
      久野秀剛、松谷貴臣、中野人志、塚本雅弘、中山斌義
    • Organizer
      平成22年電気学会基礎・材料・共通部門大会
    • Place of Presentation
      琉球大学工学部、沖縄
    • Year and Date
      2010-09-13
    • Related Report
      2010 Final Research Report
  • [Presentation] 生体埋込金属材料のDLCコーティングによる高機能化2010

    • Author(s)
      久野秀剛、松谷貴臣、中野人志、塚本雅弘、中山斌義
    • Organizer
      平成22年電気学会基礎・材料・共通部門大会
    • Place of Presentation
      沖縄、琉球大学工学部
    • Year and Date
      2010-09-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] 生体埋込金属材料のDLCコーティングによる高機能化2010

    • Author(s)
      久野秀剛、松谷貴臣、中野人志、塚本雅弘、中山斌義
    • Organizer
      (社)レーザー学会第402回研究会
    • Place of Presentation
      広島県情報プラザ、広島
    • Year and Date
      2010-09-03
    • Related Report
      2010 Final Research Report
  • [Presentation] Adhesion Enhancement of Hydroxyapatite Coating by Laser-Assisted Laser Ablation Method2010

    • Author(s)
      T.Miyazaki, H.Kuno, H.Katayama, T.Nakayama
    • Organizer
      International Conference on Lasers, Applications, and Technologies 2010
    • Place of Presentation
      Kazan, Russia
    • Year and Date
      2010-08-24
    • Related Report
      2010 Final Research Report
  • [Presentation] Adhesion Enhancement of Hydroxyapatite Coating by Laser-Assisted Laser Ablation Method2010

    • Author(s)
      T.Miyazaki, H.Kuno, H.Katayama, T.Nakayama
    • Organizer
      ICONO/LAT2010
    • Place of Presentation
      Kazan, Russia
    • Year and Date
      2010-08-24
    • Related Report
      2010 Annual Research Report
  • [Presentation] Hydroxyapatite Coating Methods for Implant Materials2010

    • Author(s)
      T.Nakayama, T.Yonezawa
    • Organizer
      1st Nepal/Japan Combined Orthopaedic Symposium
    • Place of Presentation
      Pokhara, Nepal
    • Year and Date
      2010-02-18
    • Related Report
      2010 Final Research Report 2009 Annual Research Report
  • [Presentation] Characteristic of Hydroxyapatite Films Coated on a Titanium Substrate by Laser-Assisted Laser Ablation2009

    • Author(s)
      T.Miyazaki, H.Katayame, T.Nakayama
    • Organizer
      The 7th International Symposium on Applied Plasma Science
    • Place of Presentation
      Hamburg, Germany
    • Year and Date
      2009-09-01
    • Related Report
      2010 Final Research Report 2009 Annual Research Report
  • [Presentation] 紫外パルスレーザー光を用いて作製したHAp被膜の密着性評価2009

    • Author(s)
      宮崎聡久、久野秀剛、片山博貴、中山斌義
    • Organizer
      レーザー学会第389回研究会
    • Place of Presentation
      ザ・グラン・リゾート・エレガンテ・白浜、白浜
    • Year and Date
      2009-08-08
    • Related Report
      2010 Final Research Report
  • [Presentation] 紫外レーザーパルス光を用いて作製したHAp被膜の評価2009

    • Author(s)
      宮崎聡久
    • Organizer
      レーザー学会学術講演会第29回年次大会
    • Place of Presentation
      徳島大学
    • Year and Date
      2009-01-12
    • Related Report
      2008 Annual Research Report
  • [Presentation] 紫外パルスレーザー光を用いて作製したHAp被膜の評価2009

    • Author(s)
      宮崎聡久,片山博貴,中山斌義
    • Organizer
      レーザー学会学術講演会第29回年次大会
    • Place of Presentation
      徳島大学工学部、徳島
    • Year and Date
      2009-01-10
    • Related Report
      2010 Final Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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