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Reaction synthesis of aluminum nitride in precision mold without sintering agents

Research Project

Project/Area Number 20613005
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Element strategy
Research InstitutionNagoya University

Principal Investigator

KOBASHI Makoto  Nagoya University, 大学院・工学研究科, 准教授 (90225483)

Co-Investigator(Kenkyū-buntansha) KUME Yuji  名古屋大学, 大学院・工学研究科, 助教 (30377890)
KANETAKE Naoyuki  名古屋大学, 大学院・工学研究科, 教授 (00115552)
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2010: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2009: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2008: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywords複合材料 / 窒化アルミニウム / in situ反応 / 無加圧浸透法 / 反応浸透法 / 低温合成
Research Abstract

The reactive infiltration of molten aluminum into a powder preform was investigated as a processing route for aluminum nitride (AlN). As the powder preform, titanium and boron nitride (BN) powders were blended and compacted. The infiltration occurred spontaneously at temperatures above 1173 K, and turned out to be irrelevant to the BN powder size and BN/Ti blending ratio. However, the conversion ratio of BN to AlN was prominent above 1673K. When the amount of aluminum is not sufficient, residual BN was observed in the microstructure, and the morphology of the mold was not copied precisely. The specimen containing rich aluminum showed the good transcriptional behavior.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (8 results)

All 2010 2009 Other

All Journal Article (2 results) (of which Peer Reviewed: 2 results) Presentation (5 results) Remarks (1 results)

  • [Journal Article] Effect of powder blending ratio on themicrostructure of AlN matrix composite fabricated by reactive infiltration Proc.2010

    • Author(s)
      S.Aoyama, M.Kobashi, N.Kanetake
    • Journal Title

      12th international conference on aluminum alloys ICAA-12

      Pages: 835-839

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of powder blending ratio on the microstructure of AIN matrix composite fabricated by reactive infiltration2010

    • Author(s)
      S.Aoyama, M.Kobashi, N.Kanetake
    • Journal Title

      Proc.12th international conference on aluminum alloys (ICAA-12)

      Pages: 835-839

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] In situ AlN/TiB2複合材料の合成過程に及ぼすTi, TiNの影響2010

    • Author(s)
      堺大記
    • Organizer
      軽金属学会
    • Place of Presentation
      長岡技術科学大学
    • Year and Date
      2010-11-13
    • Related Report
      2010 Final Research Report
  • [Presentation] In situ AIN/TiB_2複合材料の合成過程に及ぼすTi, TiNの影響2010

    • Author(s)
      堺大記
    • Organizer
      軽金属学会
    • Place of Presentation
      長岡技術科学大学
    • Year and Date
      2010-11-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] BN/Al間反応によるAlN生成に及ぼすプロセス因子の影響2010

    • Author(s)
      小橋眞
    • Organizer
      日本金属学会
    • Place of Presentation
      筑波大学
    • Year and Date
      2010-03-30
    • Related Report
      2010 Final Research Report 2009 Annual Research Report
  • [Presentation] BN/Al間反応により製造されたAlN複合材料の組織に及ぼす原料粉末種の影響2009

    • Author(s)
      小橋眞
    • Organizer
      日本金属学会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2009-03-30
    • Related Report
      2010 Final Research Report
  • [Presentation] BN/Al間反応により製造されたA1N複合材料の組織に及ぼす原料粉末種の影響2009

    • Author(s)
      小橋真
    • Organizer
      日本金属学会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2009-03-30
    • Related Report
      2008 Annual Research Report
  • [Remarks] ホームページ等

    • URL

      http://www.numse.nagoya-u.ac.jp/P6/research/research_of_composite.html

    • Related Report
      2010 Final Research Report

URL: 

Published: 2008-04-01   Modified: 2016-04-21  

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