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Boron modified O phase-based titanium alloy with new phase constitution and reduced Nb content.

Research Project

Project/Area Number 20613012
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Element strategy
Research InstitutionKyushu Institute of Technology

Principal Investigator

HAGIHARA Masuo (HAGIWARA Masuo)  九州工業大学, 先端エコフィッティング技術研究開発センター, 研究職員 (80354182)

Co-Investigator(Kenkyū-buntansha) KITAURA Tomoyuki  九州工業大学, 先端エコフィッティング技術研究開発センター, 助教 (30467948)
Project Period (FY) 2008 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2011: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2010: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2009: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2008: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Keywordsチタン / O相基合金 / 組成制御 / 組織制御 / ボロン添加 / 引張り特性 / 〇相基合金 / 軽量耐熱 / 微視組織制御 / 機械的特性 / 軽量耐熱合金 / アルファ2相 / 希少金属低減 / 結晶粒 / 室温延性 / O相基チタン合金 / 室温引張り強さ / 高温引張り強さ / 高温延性 / クリープ特性
Research Abstract

The(O+α2)-type O phase-based Ti-27. 5Al-13Nb is a new type of lightweight and high-strength titanium intermetallic alloy. In the present study, the composition was modified to reduce the Nb content, and three derivative alloys, Ti-27. 5Al-8. 7Nb-1Mo, Ti-27. 5Al-5. 5 Nb-1Fe and Ti-27. 5Al-4. 9Nb-1Mo-0. 5Fe, were newly designed. A minor addition of boron(B) and a thermo-mechanical treatment in the(B+α2) two-phase region were found to be effective in refining their microstructures and thus in improving their ductility. Among these alloys, the Ti-27. 5Al-8. 7 Nb-1Mo-0. 1B alloy showed the highest tensile strength and ductility in the whole temperature range up to 800°C, and thus turned out to be a most promising alloy for high temperature applications.

Report

(5 results)
  • 2011 Final Research Report ( PDF )
  • 2010 Annual Research Report   Self-evaluation Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (38 results)

All 2012 2010 2009 Other

All Journal Article (13 results) (of which Peer Reviewed: 11 results) Presentation (21 results) Remarks (2 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] 微量ボロンを含有し希少金属を減量した高温用(O+α2)型Ti2AlNb基合金の開発2012

    • Author(s)
      萩原益夫, 北浦知之
    • Journal Title

      日本金属学会誌

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] High Cycle Fatigue Properties of a Minor Boron-Modified Ti-6Al-4V Alloy2012

    • Author(s)
      M. Hagiwara, T. Kitaura, Y. Ono, T. Yuri, T. Ogata and O. Kanou
    • Journal Title

      Mater. Trans

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Tensile and High Cycle Fatigue Properties of a Minor Boron-Modified Ti-22Al-11Nb-2 Mo-1Fe Alloy2012

    • Author(s)
      M. Hagiwara, T. Kitaura, Y. Ono, T. Yuri, T. Ogata, and S. Emura
    • Journal Title

      Mater. Trans

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Ti-22Al-11Nb-2Mo-1Fe合金の高サイクル疲労特性に及ぼす微量B添加の影響2010

    • Author(s)
      北浦知之, 萩原益夫
    • Journal Title

      日本学術振興会耐熱金属材料第123委員会研究報告

      Volume: 51 Pages: 113-120

    • Related Report
      2011 Final Research Report 2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of Trace Boron Addition on the Micro-structure and Tensile Elongation of Ti2AlNb-Based Orthorhombic Titanium Alloys2010

    • Author(s)
      M. Hagiwara and T. Kitaura
    • Journal Title

      Materials Science Forum

      Volume: 638-642 Pages: 1439-1444

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Ti-22Al-11Nb-2Mo-1Fe合金の高サイクル疲労特性に及ぼす微量B添加の影響2010

    • Author(s)
      北浦知之, 萩原益夫
    • Journal Title

      日本学術振興会耐熱金属材料第123委員会研究報告 51

      Pages: 113-120

    • Related Report
      2010 Self-evaluation Report
    • Peer Reviewed
  • [Journal Article] Effect of Trace Boron Addition on the Microstructure and Tensile Elongation of Ti_2AlNb-Based Orthorhombic Titanium Alloys2010

    • Author(s)
      M.Hagiwara, T.Kitaura
    • Journal Title

      Materials Science Forum 638-642

      Pages: 1439-1444

    • Related Report
      2010 Self-evaluation Report
    • Peer Reviewed
  • [Journal Article] Effect of Trace Boron Addition on the Microstructure and Tensile Elongation of Ti_2AlNb-Based Orthorhombic Titanium Alloys2010

    • Author(s)
      M.Hagiwara, T.Kitaura
    • Journal Title

      Materials Science Forum

      Volume: 638-642 Pages: 1439-1444

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Tensile Behavior and Hot Formability of Ortho-rhombic Ti-22Al-11Nb-2Mo-1Fe Alloy with Trace Boron Addition2009

    • Author(s)
      T. Kitaura and M. Hagiwara
    • Journal Title

      Proc. Processing and Fabrication of Advanced Materials-XVIII

      Volume: 2 Pages: 805-814

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] 微量のTiB化合物の分散によるチタン合金の金属組織制御と特性向上2009

    • Author(s)
      北浦知之, 萩原益夫
    • Journal Title

      日本学術振興会耐熱金属材料第123委員会研究報告

      Volume: 50 Pages: 325-330

    • Related Report
      2011 Final Research Report
  • [Journal Article] Tensile Behavior and Hot Formability of Orthorhombic Ti-22Al-11Nb-2Mo-1Fe Alloy with Trace Boron Addition2009

    • Author(s)
      T.Kitaura, M.Hagiwara
    • Journal Title

      Proc. Processing and Fabrication of Advanced Materials-XVIII 2

      Pages: 805-814

    • Related Report
      2010 Self-evaluation Report
    • Peer Reviewed
  • [Journal Article] 量のTiB化合物の分散によるチタン合金の金属組織制御と特性向上2009

    • Author(s)
      北浦知之, 萩原益夫
    • Journal Title

      日本学術振興会耐熱金属材料第123委員会研究報告 50

      Pages: 325-330

    • Related Report
      2010 Self-evaluation Report
  • [Journal Article] Effect of Trace Boron Addition on the Microstructure and Tensile Elongation of Ti_2AINb-Based Orthorhombic Titanium Alloys2009

    • Author(s)
      Masuo Hagiwara, Tomoyuki Kitaura
    • Journal Title

      Materials Science Forum (掲載確定)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] 微量ボロンを含有し希少金属を減量したTi2AlNb基軽量耐熱合金の開発2012

    • Author(s)
      萩原益夫、北浦知之、江村聡
    • Organizer
      第150回日本金属学会春期講演大会
    • Place of Presentation
      横浜国立大学(横浜)
    • Year and Date
      2012-03-30
    • Related Report
      2011 Final Research Report
  • [Presentation] Improving Properties of Titanium Alloys and Titanium Inter-metallic Alloys by Minor Addition of boron2010

    • Author(s)
      M. Hagiwara, T. Kitaura, Y. Ono, T. Yuri, and T. Ogata
    • Organizer
      11th IUMRS Int' l Conf. in Asia
    • Place of Presentation
      Qingdao(China)
    • Related Report
      2011 Final Research Report
  • [Presentation] (O+ B2)型Ti2AlNb基合金の金属組織制御による室温および高温強度特性の高性能化2010

    • Author(s)
      北浦知之, 萩原益夫, 佐田鉄哉
    • Organizer
      日本鉄鋼協会第160回秋季講演大会
    • Place of Presentation
      北海道大学(札幌)
    • Related Report
      2011 Final Research Report
  • [Presentation] (O+.α2)型Ti-27. 5Al-13Nb合金の金属組織と引張特性に及ぼすB添加と熱処理の影響2010

    • Author(s)
      佐田鉄哉, 北浦知之, 萩原益夫
    • Organizer
      日本鉄鋼協会第160回秋季講演大会
    • Place of Presentation
      北海道大学(札幌)
    • Related Report
      2011 Final Research Report
  • [Presentation] Improved Properties of Boron-Modified Titanium Alloys2010

    • Author(s)
      M. Hagiwara, T. Kitaura, Y. Ono, T. Yuri, and T. Ogata
    • Organizer
      7th Pacific Rim Int' l Conf. on Advanced Materials and Processing
    • Place of Presentation
      Cairns(Australia)
    • Related Report
      2011 Final Research Report
  • [Presentation] Improving Properties of Titanium Alloys and Titanium Intermetallic Alloys by Minor Addition of boron2010

    • Author(s)
      M.Hagiwara, T.Kitaura, Y.Ono, T.Yuri, T.Ogata
    • Organizer
      11^<th> IUMRS Int'l Conf. in Asia
    • Place of Presentation
      Qingdao (China)
    • Related Report
      2010 Self-evaluation Report
  • [Presentation] (O+B2)型Ti_2AlNb 基合金の金属組織制御による室温および高温強度特性の高性能化2010

    • Author(s)
      北浦知之, 萩原益夫, 佐田鉄哉
    • Organizer
      日本鉄鋼協会第160回秋季講演大会
    • Place of Presentation
      北海道大学(札幌)
    • Related Report
      2010 Self-evaluation Report
  • [Presentation] (O+α2)型Ti-27.5Al-13Nb 合金の金属組織と引張特性に及ぼすB 添加と熱処理の影響2010

    • Author(s)
      佐田鉄哉, 北浦知之, 萩原益夫
    • Organizer
      日本鉄鋼協会第160回秋季講演大会
    • Place of Presentation
      北海道大学(札幌)
    • Related Report
      2010 Self-evaluation Report
  • [Presentation] Improved Properties of Boron-Modified Titanium Alloys2010

    • Author(s)
      M.Hagiwara, T.Kitaura, Y.Ono, T.Yuri, T.Ogata
    • Organizer
      7^<th> Pacific Rim Int'l Conf. on Advanced Materials and Processing
    • Place of Presentation
      Cairns (Australia)
    • Related Report
      2010 Self-evaluation Report
  • [Presentation] (O+α2)型Ti-27.5Al-13Nb合金の金属組織と引張特性に及ぼすB添加と熱処理の影響2010

    • Author(s)
      佐田鉄哉, 北浦知之, 萩原益夫
    • Organizer
      日本鉄鋼協会第160回秋季講演大会
    • Place of Presentation
      北海道大学(札幌)
    • Related Report
      2010 Annual Research Report
  • [Presentation] O+B2)型Ti_2AlNb基合金の金属組織制御による室温および高温強度特性の高性能化2010

    • Author(s)
      北浦知之, 萩原益夫, 佐田鉄哉
    • Organizer
      日本鉄鋼協会第160回秋季講演大会
    • Place of Presentation
      北海道大学(札幌)
    • Related Report
      2010 Annual Research Report
  • [Presentation] Improving Properties of Titanium Alloys and Titanium Intermetallic Alloys by Minor Addition of boron.2010

    • Author(s)
      M.Hagiwara, T.Kitaura, Y.Ono, T.Yuri, T.Ogata
    • Organizer
      11^<th> IUMRS Int'l Conf.in Asia (IUMRS-ICA2010)
    • Place of Presentation
      Qingdao, China
    • Related Report
      2010 Annual Research Report
  • [Presentation] Improved Properties of Boron-Modified Titanium Alloys.2010

    • Author(s)
      M.Hagiwara, T.Kitaura, Y.Ono, T.Yuri, T.Ogata
    • Organizer
      7^<th> Pacific Rim Int'l Conf.on Advanced Materials and Processing(PRICM-7)
    • Place of Presentation
      Cairns, Australia
    • Related Report
      2010 Annual Research Report
  • [Presentation] Improvement of formability, and tensile and high cycle fatigue properties of titanium alloys by minor addition of boron.2010

    • Author(s)
      M.Hagiwara, T.Kitaura, Y.Ono, T.Yuri, T.Ogata
    • Organizer
      The 6^<th> Int'l Conf.on Advanced Materials and Processing(ICAMP-6)
    • Place of Presentation
      Lijiang, China
    • Related Report
      2010 Annual Research Report
  • [Presentation] High Cycle Fatigue Properties of Minor Boron-Modified Ti-6Al-4V Alloy.2010

    • Author(s)
      M.Hagiwara, T.Kitaura, Y.Ono, T.Yuri, T.Ogata
    • Organizer
      Int'l Forum on Advanced Materials Science and Technology (IFAMST-7)
    • Place of Presentation
      Dalian, China
    • Related Report
      2010 Annual Research Report
  • [Presentation] 微量のTiB化合物の分散によるチタン合金の金属組織制御と特性向上2009

    • Author(s)
      北浦知之, 萩原益夫
    • Organizer
      第158回日本鉄鋼協会秋季講演大会
    • Place of Presentation
      京都大学(京都)
    • Year and Date
      2009-09-16
    • Related Report
      2011 Final Research Report
  • [Presentation] 微量のTiB 化合物の分散によるチタン合金の金属組織制御と特性向上2009

    • Author(s)
      北浦知之, 萩原益夫
    • Organizer
      第158回日本鉄鋼協会秋季講演大会
    • Place of Presentation
      京都大学(京都)
    • Year and Date
      2009-09-16
    • Related Report
      2010 Self-evaluation Report
  • [Presentation] 軽量耐熱Ti2AlNb基合金の開発2009

    • Author(s)
      萩原益夫, 北浦知之, 江村聡
    • Organizer
      第144回日本金属学会春期講演大会
    • Place of Presentation
      東京工業大学(東京)
    • Year and Date
      2009-03-28
    • Related Report
      2011 Final Research Report
  • [Presentation] 軽量耐熱Ti_2AlNb 基合金の開発2009

    • Author(s)
      萩原益夫, 北浦知之, 江村聡
    • Organizer
      第144回日本金属学会春期講演大会
    • Place of Presentation
      東京工業大学(東京)
    • Year and Date
      2009-03-28
    • Related Report
      2010 Self-evaluation Report
  • [Presentation] 軽量耐熱Ti_2AlNb(O相)基合金の開発2009

    • Author(s)
      萩原益夫, 北浦知之, 江村聡
    • Organizer
      日本金属学会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2009-03-28
    • Related Report
      2008 Annual Research Report
  • [Presentation] Effect of Trace Boron Addition on the Microstructure and Tensile Elongation of Ti_2AlNb-Based Orthorhombic Titanium Alloys.2009

    • Author(s)
      M.Hagiwara, T.Kitaura
    • Organizer
      Int.Conf.on Processing and Manufacturing of Advanced Materials(THERMEC'2009)
    • Place of Presentation
      Berlin, Germany
    • Related Report
      2009 Annual Research Report
  • [Remarks] ホームページ

    • URL

      http://www.lsse.kyutech.ac.jp/~ecofitting

    • Related Report
      2011 Final Research Report
  • [Remarks] ホームページ

    • URL

      http://www.lsse.kyutech.ac.jp/~ecofitting

    • Related Report
      2010 Self-evaluation Report
  • [Patent(Industrial Property Rights)] 相基耐熱チタン合金及びその製造方法2009

    • Inventor(s)
      北浦知之,萩原益夫
    • Industrial Property Rights Holder
      九州工業大学
    • Industrial Property Number
      2009-199407
    • Filing Date
      2009-09-27
    • Related Report
      2011 Final Research Report
  • [Patent(Industrial Property Rights)] O相基耐熱チタン合金及びその製造方法2009

    • Inventor(s)
      北浦知之, 萩原益夫
    • Industrial Property Rights Holder
      九州工業大学
    • Industrial Property Number
      2009-199407
    • Filing Date
      2009-09-27
    • Related Report
      2010 Self-evaluation Report

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Published: 2008-04-01   Modified: 2016-04-21  

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