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The use of xenon for synthesis of new carbon materials and analysis of microporous structure

Research Project

Project/Area Number 20750166
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Inorganic industrial materials
Research InstitutionOkayama University

Principal Investigator

GOTOH Kazuma  Okayama University, 大学院・自然科学研究科, 助教 (20385975)

Research Collaborator ISHIDA Hiroyuki  岡山大学, 大学院・自然科学研究科, 教授 (70193331)
UEDA Takahiro  大阪大学, 総合学術博物館, 准教授
KAWABATA Koji  , 岡山県工業技術センター, 研究員
FUJII Eiji  , 岡山県工業技術センター, 研究員
MORISHIGE Kunimitsu  岡山理科大学, 理学部, 教授
HAYAKAWA Satishi  岡山大学, 大学院・自然科学研究科, 准教授
KINUMOTO Taro  大分大学, 工学部, 助教
Project Period (FY) 2008 – 2009
Project Status Completed (Fiscal Year 2009)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2009: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2008: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Keywords炭素 / キセノン / アモルファス / 細孔解析 / 酸化黒鉛 / 炭素材料 / 核磁気共鳴 / ハードカーボン / 金属ナノ粒子
Research Abstract

This research showed that pore structure of amorphous carbon can be evaluated using xenon and Xe NMR. Xenon also can be used for improvement of carbon surface. On the other hand, porous graphene materials having platinum, ruthenium or palladium nanoparticles on exfoliated graphene sheets were produced from graphite oxide and metal complexes. The research showed that the samples have catalytic activity for some reactions, for example, oxygen reduction reaction on full cell.

Report

(3 results)
  • 2009 Annual Research Report   Final Research Report ( PDF )
  • 2008 Annual Research Report
  • Research Products

    (53 results)

All 2010 2009 2008 Other

All Journal Article (30 results) (of which Peer Reviewed: 30 results) Presentation (15 results) Book (5 results) Remarks (1 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Two solid phases of pyrimidin-1-ium hydrogen chloranilate monohydrate determined at 225 and 120 K2010

    • Author(s)
      K. Gotoh, T. Asaji, H. Ishida
    • Journal Title

      Acta Cryst. C66

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Two solid phases of pyrimidin-1-ium hydrogen chloranilate monohydrate determined at 225 and 120 K2010

    • Author(s)
      K.Gotoh, T.Asaji, H.Ishida
    • Journal Title

      Acta Cryst. C66

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] The use of graphite oxide to produce mesoporous carbon supporting Pt, Ru, or Pd nanoparticles2009

    • Author(s)
      K. Gotoh, K. Kawabata E. Fujii, K. Morishige, T. Kinumoto, Y. Miyazaki, H. Ishida
    • Journal Title

      Carbon 47

      Pages: 2120-2124

    • NAID

      120002307007

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Pore structure of hard carbon made from phenolic resin studied by 129Xe NMR2009

    • Author(s)
      K. Gotoh, T. Ueda, T. Eguchi, K. Kawabata, K. Yamamoto, Y. Murakami, S. Hayakawa, H. Ishida
    • Journal Title

      Bull. Chem. Soc. Jpn. 82

      Pages: 1232-1239

    • NAID

      10025864389

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen-bonded structures of the isomeric compounds of quinoline with 2-chloro-5-nitrobenzoic acid, 3-chloro-2-nitrobenzoic acid, 4-chloro-2-nitrobenzoic acid and 5-chloro-2-nitrobenzoic acid2009

    • Author(s)
      K. Gotoh, H. Ishida
    • Journal Title

      Acta Cryst. C65

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen-bonded structures of the isomeric 2-, 3- and 4-carbamoylpyridinium hydrogen chloranilates2009

    • Author(s)
      K. Gotoh, H. Nagoshi, H. Ishida
    • Journal Title

      Acta Cryst. C65

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Pore structure of hard carbon made from phenolic resin studied by ^<129>Xe NMR2009

    • Author(s)
      K.Gotoh, T.Ueda, H.Ishida, et al.
    • Journal Title

      Bull.Chem.Soc.Jpn. 82

      Pages: 12321239-12321239

    • NAID

      10025864389

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] The use of graphite oxide to produce mesoporous carbon supporting Pt, Ru, or Pd nanoparticles2009

    • Author(s)
      K.Gotoh, K.Kawabata, et al.
    • Journal Title

      Carbon 47

      Pages: 21202124-21202124

    • NAID

      120002307007

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen-bonded structures of the isomeric compounds of quinoline with 2-chloro-5-nitrobenzoic acid, 3-chloro-2-nitrobenzoic acid, 4-chloro-2-nitrobenzoic acid and 5-chloro-2-nitrobenzoic acid2009

    • Author(s)
      K.Gotoh, H.Ishida
    • Journal Title

      Acta Cryst. C65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 3-Hydroxypyridinium hydrogen chloranilate monohydrate2009

    • Author(s)
      K.Gotoh, H.Ishida
    • Journal Title

      Acta Cryst. E65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Pyridine-3-carbonittile-chloranilic acid-acetonitrile (2/1/2)2009

    • Author(s)
      K.Gotoh, H.Ishida
    • Journal Title

      Acta Cryst. E65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen-bonded structures of the isomeric 2-, 3- and 4-carbamoylpyridinium hydrogen chloranilates2009

    • Author(s)
      K.Gotoh, H.Ishida, et al.
    • Journal Title

      Acta Cryst. C65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 2-Carboxypyridinium hydrogen chloranilate2009

    • Author(s)
      K.Gotoh, H.Ishida, et al.
    • Journal Title

      Acta Cryst. E65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen bonding in 1,2-diazine-chloranilic acid (2:1) studied by a ^<14>N nuclear quadrupole coupling tensor and multi-temperature X-ray diffraction2009

    • Author(s)
      J.Seliger, K.Gotoh, T.Asaj, et al.
    • Journal Title

      Phys.Chem.Chem.Phys. 11

      Pages: 22812286-22812286

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 4-Bromo-N-(3,4,5-trimethoxybenzylidene)aniline2009

    • Author(s)
      A.D.Khalaji, K.Gotoh H.Ishida, et al.
    • Journal Title

      Acta Cryst. E65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] catena-Poly[[[N,N'-bis(3-methoxybenzylidene)ethylenediamine]copper(I)]-thiocyanato-2N:S]2009

    • Author(s)
      A.D.Khalaji, K.Gotoh. H.Ishida, et al.
    • Journal Title

      Acta Cryst. E65

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen bonding in 1, 2-diazine-chloranilic acid (2:1) studied by a 14N nuclear quadrupole coupling tensor and multi-temperature X-ray diffraction2009

    • Author(s)
      J. Seliger, K. Gotoh, T. Asaj, et.al.
    • Journal Title

      Phys. Chem. Chem. Phys. 11

      Pages: 2281-2286

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 4-Bromo-N-(3, 4, 5-trimethoxybenzylidene) aniline2009

    • Author(s)
      A. D. Khalaji, K. Gotoh H. Ishida, et.al.
    • Journal Title

      Acta Cryst E65

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] catena-Poly [[[P, N'-bis (3-methoxybenzylidene) ethylenediamine] copper (I)]-□-thiocyanato-□2N:S]2009

    • Author(s)
      Khalaji, K. Gotoh. H. Ishida, et.al.
    • Journal Title

      Acta Cryst. E65

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen bonding in 1, 2-diazine-chloranilic acid (2/1) and 1, 4-diazine-chloranilic acid (2/1) determined at 110 K2008

    • Author(s)
      K. Gotoh, T. Asaji, H. Ishida
    • Journal Title

      Acta Cryst. C64

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Observation of micropores in hard-carbon using 129Xe NMR porosimetry2008

    • Author(s)
      K. Gotoh, T. Ueda, H. Omi, T. Eguchi, M. Maeda, M. Miyahara, A. Nagai, H. Ishida
    • Journal Title

      J. Phys. Chem. Sol. 69

      Pages: 147-152

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen bonding in 1, 2-diazine-chloranilic acid (2/1) and 1, 4-diazine-chloranilic acid (2/1) determined at 110K2008

    • Author(s)
      K. Gotoh, T. Asaji and H. Ishida
    • Journal Title

      Acta Cryst. C64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Observation of micropores in hard-carbon using 129 Xe NMR porosimetry2008

    • Author(s)
      K. Gotoh, T. Ueda, H. Ishida, et.al.
    • Journal Title

      J. Phys. Chem. Sol. 69

      Pages: 147-152

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 3, 4, 5-Trimethoxybenzohydrazidium chloride2008

    • Author(s)
      A. Saeed, K. Gotoh, H. Ishida, et.al.
    • Journal Title

      Acta Cryst. E64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 3-Fluoro-N-(p-tolyl)benzamide2008

    • Author(s)
      A. Saeed, K. Gotoh, H. IshidaJ, et.al.
    • Journal Title

      Acta Cryst. E64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 1, 2-Diazinium hydrogen chloranilate2008

    • Author(s)
      K. Gotoh and H. Ishida
    • Journal Title

      Acta Cryst. E64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 4-Chloro-N-o-tolylbenzamide2008

    • Author(s)
      A. Saeed, K. Gotoh, H. Ishida, et.al.
    • Journal Title

      Acta Cryst. E64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 4-Chloro-N-(2-chlorophenyl)-benzamide2008

    • Author(s)
      A. Saeed, K. Gotoh H. Ishida, et.al.
    • Journal Title

      Acta Cryst. E64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Redetermination of pyridine-4-carbonitrile-chloranilic acid (1/1) at 180K2008

    • Author(s)
      K. Gotoh, H. Nagoshi and H. Ishida
    • Journal Title

      Acta Cryst. E64

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] The use of graphite oxide to produce mesoporous carbon supporting Pt, Ru, or Pd nanoparticles

    • Author(s)
      K. Gotoh, K. Kawabata, et.al.
    • Journal Title

      Carbon (in press)

    • NAID

      120002307007

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] 金および銀ナノ粒子を担持するグラフェンの作製2010

    • Author(s)
      後藤和馬, 山本亜季, 衣本太郎, 藤井英司, 大久保貴広, 石田祐之
    • Organizer
      日本化学会第90春季年会
    • Place of Presentation
      大阪(近畿大)
    • Year and Date
      2010-03-26
    • Related Report
      2009 Annual Research Report 2009 Final Research Report
  • [Presentation] クロラニル酸-1, 3-ジアジン(1/1)塩-水和物および(1/2)塩の結晶構造と相転移2010

    • Author(s)
      後藤和馬, 浅地哲夫, 石田祐之
    • Organizer
      日本化学会第90春季年会
    • Place of Presentation
      大阪(近畿大)
    • Year and Date
      2010-03-26
    • Related Report
      2009 Final Research Report
  • [Presentation] クロラニル酸-1,3-ジアジン(1/1)塩-水和物および(1/2)塩の結晶構造と相転移2010

    • Author(s)
      後藤和馬, 浅地哲夫, 石田祐之
    • Organizer
      日本化学会第90春季年会
    • Place of Presentation
      大阪(近畿大)
    • Year and Date
      2010-03-26
    • Related Report
      2009 Annual Research Report
  • [Presentation] 酸化黒鉛から作製されるRuおよびPdナノ粒子を持つ多孔質炭素2009

    • Author(s)
      後藤和馬, 宮崎由希, 川端浩二, 藤井英司, 衣本太郎, 石田祐之
    • Organizer
      日本化学会第89春季年会
    • Place of Presentation
      船橋(日本大)
    • Year and Date
      2009-03-27
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] 貴金属を含有する酸化グラファイト多孔触媒材料2009

    • Author(s)
      後藤和馬, 石田祐之, 宮崎由希, 池田祥子, 川端浩二, 藤井英司, 森重国光, 衣本太郎
    • Organizer
      第13回岡山リサーチパーク研究・展示発表会
    • Place of Presentation
      岡山(テクノサポート岡山)
    • Year and Date
      2009-02-06
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] Pore Structure of Hard Carbon for anodes of lithium ion batteries studied by 129Xe NMR2009

    • Author(s)
      K. Gotoh, T. Ueda, T. Eguchi, K. Kawabata, H. Ishida
    • Organizer
      the 4th International Symposium on Xenon NMR of Materials
    • Place of Presentation
      Ruka, Finland
    • Related Report
      2009 Final Research Report
  • [Presentation] Pore Structure of Hard Carbon for anodes of lithium ion batteries studied by ^<129>Xe NMR2009

    • Author(s)
      K.Gotoh, T.Ueda, H.Ishida, et al.
    • Organizer
      XeMat 2009 (the 4th International Symposium on Xenon NMR of Materials)
    • Place of Presentation
      Ruka(Finland)
    • Related Report
      2009 Annual Research Report
  • [Presentation] 酸化グラファイトを用いた白金ナノ粒子を含む多孔質炭素材料の開発2008

    • Author(s)
      後藤和馬, 森重國光, 川端浩二, 藤井英司, 河田卓也, 石田祐之
    • Organizer
      第35回炭素材料学会年会
    • Place of Presentation
      筑波(筑波大)
    • Year and Date
      2008-12-03
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] 129Xe NMRポロシメトリーによるフェノール樹脂焼成炭の構造解析2008

    • Author(s)
      後藤和馬, 上田貴広, 江口太郎, 塩見仁郎, 早川聡, 山本賢治, 石田祐之
    • Organizer
      第2回分子科学討論会2008
    • Place of Presentation
      福岡(福岡国際会議場)
    • Year and Date
      2008-09-25
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] 短い水素結合を持つキノリン-クロロニトロ安息香酸系化合物の結晶構造2008

    • Author(s)
      後藤和馬, 石田祐之
    • Organizer
      第2回分子科学討論会2008
    • Place of Presentation
      福岡(福岡国際会議場)
    • Year and Date
      2008-09-24
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] 14N核四極結合定数から見た1, 2-ジアジンークロラニル酸(2 : I)結晶中の水素結合状態2008

    • Author(s)
      J. Seliger, 後藤和馬, 浅地哲夫, ほか
    • Organizer
      第2回分子科学討論会2008
    • Place of Presentation
      福岡(福岡国際会議場)
    • Year and Date
      2008-09-24
    • Related Report
      2008 Annual Research Report
  • [Presentation] MFIゼオライト中の一価銅イオンの特異性-室温でのXe吸着の観点から-2008

    • Author(s)
      鳥越裕恵, 森俊謙, 大久保貴広, 小林久芳, 後藤和馬, 石田祐之, 黒田泰重
    • Organizer
      触媒討論会
    • Place of Presentation
      名古屋(名古屋大)
    • Year and Date
      2008-09-23
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] 室温付近でのAgMFIによるXe特異吸着2008

    • Author(s)
      鳥越裕恵, 森俊謙, 田中大士, 大久保貴広, 後藤和馬, 石田祐之, 黒田泰重
    • Organizer
      第61回コロイドおよび界面化学討論会
    • Place of Presentation
      福岡(九州大)
    • Year and Date
      2008-09-08
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] Porous Graphite oxide containing Pt nanoparticles2008

    • Author(s)
      K. Gotoh, K. Morishige, K. Kawabata, T. Kawata, H. Ishida
    • Organizer
      Post Conference on Carbon 2008
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2008-07-19
    • Related Report
      2009 Final Research Report
  • [Presentation] Porous Graphite oxide Containing Pt nanoparticles2008

    • Author(s)
      後藤和馬, 石田祐之, ほか
    • Organizer
      Post Conference on Carbon 2008
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2008-07-19
    • Related Report
      2008 Annual Research Report
  • [Book] A novel hard-carbon optimized to large size lithium-ion secondary batteries(M. Yoshio, R. J. Brodd, A. Kozawa Eds., Lithium-Ion Batteries: Science and Technologies, Chapter 22)2009

    • Author(s)
      A. Nagai, K. Shimizu, M. Maeda, K. Gotoh
    • Publisher
      Springer
    • Related Report
      2009 Final Research Report
  • [Book] Studies of Isolated Pores in Non-Graphitazable Carbon by Solid-State NMR(J. R. Telle, N. A. Pearlstine Eds., Amorphous Materials: Research, Technology and Applications, Chapter 4)2009

    • Author(s)
      K. Gotoh, A. Nagai
    • Publisher
      Nova Science
    • Related Report
      2009 Final Research Report
  • [Book] Amorphous Materials : Research, Technology and Applications2009

    • Author(s)
      J.R.Telle, N.A.Pearlstine(Eds.)
    • Total Pages
      11
    • Publisher
      Nova Science
    • Related Report
      2009 Annual Research Report
  • [Book] Lithium-Ion Batteries Science and Technologies2009

    • Author(s)
      M.Yoshio, R.J.Brodd, A.Kozawa(Eds.)
    • Total Pages
      7
    • Publisher
      Springer
    • Related Report
      2009 Annual Research Report
  • [Book] Lithium-Ion Batteries Science and Technologies2009

    • Author(s)
      Yoshio, Masaki ; Brodd, Ralph J. ; Kozawa, Akiya (Eds.)
    • Publisher
      Springer
    • Related Report
      2008 Annual Research Report
  • [Remarks]

    • URL

      http://chem.okayama-u.av.jp/~solid/

    • Related Report
      2009 Final Research Report
  • [Patent(Industrial Property Rights)] 多孔質炭素材料およびその製造方法ならびに燃料電池2008

    • Inventor(s)
      後藤和馬、石田祐之、藤井英司、川端浩二
    • Industrial Property Rights Holder
      国立大学法人岡山大学、岡山県
    • Industrial Property Number
      2008-331221
    • Filing Date
      2008-12-25
    • Related Report
      2009 Final Research Report
  • [Patent(Industrial Property Rights)] 多孔質炭素材料及びその製造方法並びに燃料電池2008

    • Inventor(s)
      後藤和馬、石田祐之、藤井英司、川端浩二
    • Industrial Property Rights Holder
      国立大学法人岡山大学、岡山県
    • Filing Date
      2008-12-25
    • Related Report
      2008 Annual Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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