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Degradation control of bioabsorbable magnesium alloys with anodized films

Research Project

Project/Area Number 20760499
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Material processing/treatments
Research InstitutionNational Institute for Materials Science

Principal Investigator

HIROMOTO Sachiko  National Institute for Materials Science, 生体材料センター, 主幹研究員 (00343880)

Project Period (FY) 2008 – 2009
Project Status Completed (Fiscal Year 2009)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2009: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2008: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Keywords生体吸収性マグネシウム / 陽極酸化 / 水熱処理 / リン酸カルシウム / 腐食 / 浸漬試験
Research Abstract

It is crucial for bioabsorbable magnesium alloys to control the corrosion rate depending on the condition of affected parts. The morphology and composition of anodized films of pure magnesium was then varied with the anodizing voltage and composition of electrolytes. It was revealed that the corrosion rate of pure magnesium in a simulated body fluid noticeably decreased by the incorporation of phosphate ions in the anodized film. On the other hand, the corrosion morphology depended on the porous morphology of the anodized film.

Report

(3 results)
  • 2009 Annual Research Report   Final Research Report ( PDF )
  • 2008 Annual Research Report
  • Research Products

    (38 results)

All 2009 2008

All Journal Article (11 results) (of which Peer Reviewed: 9 results) Presentation (23 results) Patent(Industrial Property Rights) (4 results)

  • [Journal Article] High corrosion resistance of magnesium coated with hydroxyapatite directly synthesized in an aqueous solution2009

    • Author(s)
      S. Hiromoto, A. Yamamoto
    • Journal Title

      Electrochimica Acta 54

      Pages: 7085-7093

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] High corrosion resistance of magnesium coated with hydroxyapatite directly synthesized in an aqueous solution2009

    • Author(s)
      S.Hiromoto, A.Yamamoto
    • Journal Title

      Electrochimica Acta 54

      Pages: 7085-7093

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Improvement of the corrosion resistance of bioabsorbable magnesium with hydroxyapatite coating2009

    • Author(s)
      S.Hiromoto, M.Tomozawa
    • Journal Title

      Proceedings of the Processing and Fabrication of Advanced Materials XVIII 3

      Pages: 1159-1164

    • Related Report
      2009 Annual Research Report
  • [Journal Article] Morphological Variation of Hydroxyapatite on Magnesium Substrate Depending on pH, Temperature and Concentration of Aqueous Solution2009

    • Author(s)
      M.Tomozawa, S.Hiromoto
    • Journal Title

      Proceedings of the Processing and Fabrication of Advanced Materials XVIII 3

      Pages: 1249-1256

    • Related Report
      2009 Annual Research Report
  • [Journal Article] Precipitation control of calcium phosphate on pure magnesium by anodization2008

    • Author(s)
      S. Hiromoto, T. Shishido, A. Yamamoto, N. Maruyama, H. Somekawa, T. Mukai
    • Journal Title

      Corrosion Science 50

      Pages: 2906-2913

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Polarization Behavior of Pure Magnesium under a Controlled Flow in a NaCl Solution2008

    • Author(s)
      S. Hiromoto, A. Yamanioto, N. Maruyama, H. Somekawa, T. Mukai
    • Journal Title

      Materials Transactions 49(6)

      Pages: 1456-1461

    • NAID

      10021147888

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation control of calcium phosphate on pure magnesium by anodizatipn2008

    • Author(s)
      S. Hiromoto, T. Shishido, A. Yamamoto, N. Maruyama, H. Somekawa, T. Mukai
    • Journal Title

      Corrosion Science 50

      Pages: 2906-2913

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Influence of pH and flow on the polarization behavior of pure magnesium in borate buffer solutions2008

    • Author(s)
      S. Hiromoto, A. Yamamoto, N. Maruyama, H. Somekawa, T. Mukai
    • Journal Title

      Corrosion Science 50(12)

      Pages: 3561-3568

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Morphological Change of Fibroblast Cells on Titanium and Platinum Cultured at Anodic and Cathodic Potentials2008

    • Author(s)
      S. Hiromoto, J. Ziegler, A. Yamamoto
    • Journal Title

      Zairyo-to-Kankyo 57(9)

      Pages: 400-408

    • NAID

      10024328862

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fabrication and Mechanical Properties of Composite Structure by Warm Spraying of Zr-Base Metallic Glass2008

    • Author(s)
      J. Kawakita, N. Maruyama, S. Kuroda, S. Hiromoto, A. Yamamoto
    • Journal Title

      Materials Transactions 49(2)

      Pages: 317-323

    • NAID

      10021144216

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fatigue Behaviors and Microstructures in an Extruded Mg-Al-Zn Alloy2008

    • Author(s)
      H. Somekawa, N. Maruyaina, S. Hiromoto, A. Yamamoto, T. Mukai
    • Journal Title

      Materials Transactions 49(3)

      Pages: 681-684

    • NAID

      10021145463

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] 陽極酸化による生体吸収性マグネシウムの腐食速度制御の試み2009

    • Author(s)
      廣本祥子
    • Organizer
      第73回金属のアノード酸化皮膜の機能化部会(ARS)例会
    • Place of Presentation
      東京都
    • Year and Date
      2009-10-01
    • Related Report
      2009 Final Research Report
  • [Presentation] 陽極酸化による生体吸収性マグネシウムの腐食速度制御の試み2009

    • Author(s)
      廣本祥子
    • Organizer
      第73回金属のアノード酸化皮膜の機能化部会(ARS)例会
    • Place of Presentation
      工学院大学新宿キャンパス(東京都)
    • Year and Date
      2009-10-01
    • Related Report
      2009 Annual Research Report
  • [Presentation] Improvement of the corrosion resistance of bioabsorbable magnesium with hydroxyapatite coating2009

    • Author(s)
      S. Hiromoto, M. Tomozawa
    • Organizer
      PFAM XVIII
    • Place of Presentation
      東北大学金属材料研究所(仙台)
    • Related Report
      2009 Final Research Report
  • [Presentation] 向井敏司, リン酸溶液中で陽極酸化したAZ系マグネシウム合金の大気腐食の形態2009

    • Author(s)
      廣本祥子, 宍戸玉緒, 染川英俊
    • Organizer
      日本金属学会2009年秋期大会
    • Place of Presentation
      京都
    • Related Report
      2009 Final Research Report
  • [Presentation] Improvement of the corrosion resistance of bioabsorbable magnesium with hydroxyapatite coating2009

    • Author(s)
      廣本祥子, 友澤方成
    • Organizer
      Processing and Fabrication of Advanced Materials XVIII
    • Place of Presentation
      東北大学金属材料研究所(仙台)
    • Related Report
      2009 Annual Research Report
  • [Presentation] Formation of Hydroxyapatite Coatings on Bioabsorbable Magnesium to Improve its Corrosion Resistance2009

    • Author(s)
      廣本祥子, 友澤方成
    • Organizer
      The 26th International Japan-Korea Seminar on Ceramics
    • Place of Presentation
      EPOCHAL Tsukuba(つくば)
    • Related Report
      2009 Annual Research Report
  • [Presentation] Formation of Calcium Phosphate Layer on Bioabsorbable Magnesium to Improve its Corrosion Resistance2009

    • Author(s)
      廣本祥子, 友澤方成
    • Organizer
      ECS 216th Meeting
    • Place of Presentation
      Austria Center Vienna, ウィーン, オーストリア
    • Related Report
      2009 Annual Research Report
  • [Presentation] リン酸溶液中で陽極酸化したAZ系マグネシウム合金の大気腐食の形態2009

    • Author(s)
      廣本祥子, 宍戸玉緒, 染川英俊, 向井敏司
    • Organizer
      日本金属学会2009年秋期大会
    • Place of Presentation
      京都大学吉田キャンパス(京都)
    • Related Report
      2009 Annual Research Report
  • [Presentation] 水酸アパタイト被覆による生体吸収性マグネシウムの疑似体液中での耐食性改善2009

    • Author(s)
      廣本祥子, 友澤方成, 山本玲子
    • Organizer
      日本金属学会2009年秋期大会
    • Place of Presentation
      京都大学吉田キャンパス(京都)
    • Related Report
      2009 Annual Research Report
  • [Presentation] Formation of Calcium Phosphate Coatings on Bioabsorbable Magnesium to Control its Corrosion Resistance2009

    • Author(s)
      廣本祥子, 友澤方成, 山本玲子
    • Organizer
      NIMS WEEK 2009
    • Place of Presentation
      EPOCHAL Tsukuba(つくば)
    • Related Report
      2009 Annual Research Report
  • [Presentation] Morphological Variation of Hydroxyapatite on Magnesium Substrate Depending on pH, Temperature and Concentration of Aqueous Solution2009

    • Author(s)
      友澤方成, 廣本祥子
    • Organizer
      Processing and Fabrication of Advanced Materials XVIII
    • Place of Presentation
      東北大学金属材料研究所(仙台)
    • Related Report
      2009 Annual Research Report
  • [Presentation] Corrosion behavior of magnesium coated with hydroxyapatite in various morphology2009

    • Author(s)
      友澤方成, 廣本祥子, 山本玲子
    • Organizer
      The 26th International Japan-Korea Seminar on Ceramics
    • Place of Presentation
      EPOCHAL Tsukuba(つくば)
    • Related Report
      2009 Annual Research Report
  • [Presentation] Influence of pH Buffer on Polarization Behavior of Magnesium2008

    • Author(s)
      S. Hiromoto
    • Organizer
      Corrosion Cluster Workshop
    • Place of Presentation
      Tsukuba
    • Year and Date
      2008-07-15
    • Related Report
      2008 Annual Research Report
  • [Presentation] Corrosion Behavior of Anodized Bioabsorbable Magnesium in Medium2008

    • Author(s)
      S. Hiromoto, A. Yamamoto
    • Organizer
      214th ECS Meeting
    • Place of Presentation
      Hawaii (USA)
    • Related Report
      2009 Final Research Report
  • [Presentation] 陽極酸化した生体吸収性マグネシウムの細胞培養液中での腐食挙動2008

    • Author(s)
      廣本祥子, 山本玲子
    • Organizer
      表面技術協会第118回講演大会
    • Place of Presentation
      東大阪
    • Related Report
      2009 Final Research Report
  • [Presentation] Precipitation of Calcium Phosphate on Anodically Oxidised Bioabsorbable Magnesium Alloy2008

    • Author(s)
      S. Hiromoto, A. Yamamoto, N. Maruyama, H. Somekawa, T. Mukai
    • Organizer
      8th World Biomaterials Congress 2008
    • Place of Presentation
      Amsterdam (Netherlands)
    • Related Report
      2009 Final Research Report 2008 Annual Research Report
  • [Presentation] 陽極酸化した生体吸収性マグネシウムの細胞培養液中での腐食挙動2008

    • Author(s)
      廣本祥子, 山本玲子
    • Organizer
      表面技術協会 第118回講演大会
    • Place of Presentation
      東大阪
    • Related Report
      2008 Annual Research Report
  • [Presentation] 陽極酸化した生体吸収性マグネシウム合金の培養液中でのMgイオン溶出挙動2008

    • Author(s)
      廣本祥子, 山本玲子
    • Organizer
      日本金属学会2008年秋期大会
    • Place of Presentation
      熊本
    • Related Report
      2008 Annual Research Report
  • [Presentation] Corrosion Behavior of Anodized Bioabsorbable Magnesium in Medium2008

    • Author(s)
      S. Hiromoto, A. Yamamoto
    • Organizer
      The 214th Meeting of The Electrochemical Society
    • Place of Presentation
      Hawaii (USA)
    • Related Report
      2008 Annual Research Report
  • [Presentation] 様々な電圧で陽極酸化した生体吸収性マグネシウムの細胞培養液中での溶出挙動2008

    • Author(s)
      廣本祥子, 山本玲子
    • Organizer
      第25回ARS軽井沢コンファレンス,表面技術協会・金属のアノード酸化皮膜の機能化部会(ARS)
    • Place of Presentation
      軽井沢
    • Related Report
      2008 Annual Research Report
  • [Presentation] 表面処理による生体吸収性マグネシウムの培養液中での腐食速度制御2008

    • Author(s)
      廣本祥子, 山本玲子
    • Organizer
      日本バイオマテリアル学会シンポジウム2008
    • Place of Presentation
      東京
    • Related Report
      2008 Annual Research Report
  • [Presentation] In vitro degradability evaluation of magnesium alloys for biomedical uses2008

    • Author(s)
      A. Yamamoto, S. Hiromoto, N. Maruyama, T. Mukai, H. Somekawa
    • Organizer
      8th World Biomaterials Congress 2008
    • Place of Presentation
      Amsterdam (Netherlands)
    • Related Report
      2008 Annual Research Report
  • [Presentation] 生体吸収性マグネシウム合金の疑似体液中の腐食に及ぼす細胞の影響2008

    • Author(s)
      山本玲子, 廣本祥子. 丸山典夫, 向井敏司, 染川英俊
    • Organizer
      日本金属学会2008年秋期講演大会
    • Place of Presentation
      熊本
    • Related Report
      2008 Annual Research Report
  • [Patent(Industrial Property Rights)] Mg基構造部材2009

    • Inventor(s)
      廣本祥子, 山本玲子, 丸山典夫, 向井敏司, 染川英俊
    • Industrial Property Rights Holder
      独立行政法人物質・材料研究機構
    • Industrial Property Number
      2009-021268
    • Filing Date
      2009-02-02
    • Related Report
      2009 Final Research Report
  • [Patent(Industrial Property Rights)] Mg基構造部材2009

    • Inventor(s)
      廣本祥子, 山本玲子, 丸山典夫, 向井敏司, 染川英俊
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Filing Date
      2009-02-02
    • Related Report
      2008 Annual Research Report
  • [Patent(Industrial Property Rights)] 医療用生体吸収性部材とその製造方法2008

    • Inventor(s)
      廣本祥子, 山本玲子, 丸山典夫, 向井敏司, 染川英俊
    • Industrial Property Rights Holder
      独立行政法人物質・材料研究機構
    • Industrial Property Number
      2008-330445
    • Filing Date
      2008-12-25
    • Related Report
      2009 Final Research Report
  • [Patent(Industrial Property Rights)] 医療用生体吸収性部材とその製造方法2008

    • Inventor(s)
      廣本祥子, 山本玲子, 丸山典夫, 向井敏司, 染川英俊
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Filing Date
      2008-12-25
    • Related Report
      2008 Annual Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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