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Three-dimensional observation of magnetic domain structures to elucidate the magnetic functionality using X-ray magnetic tomography

Research Project

Project/Area Number 20H00349
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Review Section Medium-sized Section 29:Applied condensed matter physics and related fields
Research InstitutionKwansei Gakuin University (2021-2023)
Japan Synchrotron Radiation Research Institute (2020)

Principal Investigator

Suzuki Motohiro  関西学院大学, 工学部, 教授 (60443553)

Co-Investigator(Kenkyū-buntansha) 関 真一郎  東京大学, 大学院工学系研究科(工学部), 准教授 (70598599)
小野 輝男  京都大学, 化学研究所, 教授 (90296749)
Project Period (FY) 2020-04-01 – 2024-03-31
Project Status Completed (Fiscal Year 2023)
Budget Amount *help
¥45,630,000 (Direct Cost: ¥35,100,000、Indirect Cost: ¥10,530,000)
Fiscal Year 2023: ¥8,190,000 (Direct Cost: ¥6,300,000、Indirect Cost: ¥1,890,000)
Fiscal Year 2022: ¥9,230,000 (Direct Cost: ¥7,100,000、Indirect Cost: ¥2,130,000)
Fiscal Year 2021: ¥9,230,000 (Direct Cost: ¥7,100,000、Indirect Cost: ¥2,130,000)
Fiscal Year 2020: ¥18,980,000 (Direct Cost: ¥14,600,000、Indirect Cost: ¥4,380,000)
Keywords3次元磁区観察 / スキルミオン / 焼結永久磁石 / X線イメージング / 3次元磁区観察 / 磁気イメージング / 3次元磁区構造 / 放射光 / X線イメージング / 磁区構造 / トポロジカル磁区構造 / トポロジカル磁気構造
Outline of Research at the Start

磁性体の物理的・工学的な性質は、内部に存在する「磁区」とよばれる構造によって支配される。そのため、磁区観察は磁性研究の有力な手段となっている。しかし従来の方法では試料表面の磁区観察しか行えなかった。本研究では、透過力の高い放射光X線を用いることで、試料内部の3次元的な磁区構造を直接観測可能とする磁気トモグラフィー法を開発し、立体的な3次元磁区構造と磁性との関係を解明することを目的とする。

Outline of Final Research Achievements

We developed the X-ray magnetic tomography technique at the synchrotron radiation facility SPring-8. This new experimental technique allowed non-destructive three-dimensional observation of the microscopic magnetic domain structure (distribution of N and S poles) inside bulk magnetic materials, clarifying the relationship between the magnetic domain structure and properties of the magnetic materials. Using X-ray magnetic tomography, we successfully visualized the theoretically predicted skyrmion strings and proved the presence of singularity points. The behavior of nucleation and magnetic domain propagation during the magnetization reversal process of neodymium-sintered magnets were directly observed, and the correlation with the microstructure was discussed.

Academic Significance and Societal Importance of the Research Achievements

将来の高密度情報記録・演算素子として有望視されているトポロジカル磁気構造や、モーター材料として重要な焼結永久磁石について、材料内部の磁区の挙動をナノメートルの分解能で可視化できる実験手法を開発した。本研究の成果は、新たな原理に基づく低消費電力の磁気メモリデバイスや、高効率・低燃費のモーターに搭載される高性能永久磁石材料の開発に資するものである

Report

(6 results)
  • 2023 Annual Research Report   Final Research Report ( PDF )
  • 2022 Annual Research Report
  • 2021 Annual Research Report
  • 2020 Comments on the Screening Results   Annual Research Report
  • Research Products

    (27 results)

All 2023 2022 2021 2020 Other

All Journal Article (11 results) (of which Peer Reviewed: 9 results,  Open Access: 5 results) Presentation (11 results) (of which Int'l Joint Research: 6 results,  Invited: 6 results) Book (2 results) Remarks (3 results)

  • [Journal Article] Intrinsic Magnetic Proximity Effect at the Atomically Sharp Interface of CoxFe3-xO4/Pt Grown by Molecular Beam Epitaxy2023

    • Author(s)
      Nodo Shoto、Yamane Ichiro、Suzuki Motohiro、Okabayashi Jun、Yokokura Seiya、Shimada Toshihiro、Nagahama Taro
    • Journal Title

      ACS Omega

      Volume: 8 Issue: 28 Pages: 24875-24882

    • DOI

      10.1021/acsomega.3c00935

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Unveiling the origin of the large coercivity in (Nd, Dy)-Fe-B sintered magnets2023

    • Author(s)
      Tang Xin、Li Jiangnan、Sepehri-Amin Hossein、Bolyachkin Anton、Martin-Cid Andres、Kobayashi Shintaro、Kotani Yoshinori、Suzuki Motohiro、Terasawa Asako、Gohda Yoshihiro、Ohkubo Tadakatsu、Nakamura Tetsuya、Hono Kazuhiro
    • Journal Title

      NPG Asia Materials

      Volume: 15 Issue: 1 Pages: 20-20

    • DOI

      10.1038/s41427-023-00498-5

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Three-dimensional visualization of magnetization reversal behavior inside a high-performance Nd-Fe-B permanent magnet2023

    • Author(s)
      M. Suzuki, S. Okamoto
    • Journal Title

      SPring-8/SACLA Research Frontiers 2022

      Volume: 1 Pages: 60-61

    • Related Report
      2023 Annual Research Report
  • [Journal Article] Extremely Long Chains of Magnetic Particles via Large Plastic Beads Observed in Bimodal Magnetic Elastomers2023

    • Author(s)
      Urano Rio、Chen Kejun、Akama Shota、Takeda Yoshihiro、Maruyama Takayuki、Suzuki Motohiro、Takeuchi Akihisa、Uesugi Masayuki、Kawai Mika、Mitsumata Tetsu
    • Journal Title

      Langmuir

      Volume: 39 Issue: 14 Pages: 5137-5144

    • DOI

      10.1021/acs.langmuir.3c00150

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 放射光X線を用いた磁気分光とイメージング2023

    • Author(s)
      鈴木基寛
    • Journal Title

      日本磁気学会誌「まぐね」

      Volume: 18 Pages: 87-97

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Real picture of magnetic domain dynamics along the magnetic hysteresis curve inside an advanced permanent magnet2022

    • Author(s)
      Takeuchi Makoto、Suzuki Motohiro、Kobayashi Shintaro、Kotani Yoshinori、Nakamura Tetsuya、Kikuchi Nobuaki、Bolyachkin Anton、Sepehri-Amin Hossein、Ohkubo Tadakatsu、Hono Kazuhiro、Une Yasuhiro、Okamoto Satoshi
    • Journal Title

      NPG Asia Materials

      Volume: 14 Issue: 1

    • DOI

      10.1038/s41427-022-00417-0

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Appearance of Ferromagnetism in Pt(100) Ultrathin Films Originated from Quantum-well States2022

    • Author(s)
      Yamada Tatsuru、Ochiai Keisuke、Kinoshita Hirofumi、Sakuragi Shunsuke、Suzuki Motohiro、Osawa Hitoshi、Kageshima Hiroyuki、Sato Tetsuya
    • Journal Title

      Journal of the Physical Society of Japan

      Volume: 91 Issue: 12

    • DOI

      10.7566/jpsj.91.124708

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] In Situ Observation of the Movement of Magnetic Particles in Polyurethane Elastomer Densely Packed Magnetic Particles Using Synchrotron Radiation X-ray Computed Tomography2022

    • Author(s)
      Chen Kejun、Watanabe Mayuko、Takeda Yoshihiro、Maruyama Takayuki、Uesugi Masayuki、Takeuchi Akihisa、Suzuki Motohiro、Uesugi Kentaro、Yasutake Masahiro、Kawai Mika、Mitsumata Tetsu
    • Journal Title

      Langmuir

      Volume: 38 Issue: 44 Pages: 13497-13505

    • DOI

      10.1021/acs.langmuir.2c02004

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 放射光X線磁気トモグラフィーによる永久磁石材料内部の3次元磁区構造観察2022

    • Author(s)
      鈴木基寛、岡本聡
    • Journal Title

      日本磁気学会誌「まぐね」

      Volume: 17 Pages: 187-193

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Direct visualization of the three-dimensional shape of skyrmion strings in a noncentrosymmetric magnet2022

    • Author(s)
      S. Seki, M. Suzuki, M. Ishibashi, R. Takagi, N. D. Khanh, Y. Shiota, K. Shibata, W. Koshibae, Y. Tokura & T. Ono
    • Journal Title

      Nature Materials

      Volume: 21 Issue: 2 Pages: 181-187

    • DOI

      10.1038/s41563-021-01141-w

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] X線磁気トモグラフィーによる3次元磁区構造観察2022

    • Author(s)
      鈴木基寛
    • Journal Title

      X線・EUV結像光学ニューズレター

      Volume: No. 54 Pages: 11-15

    • Related Report
      2021 Annual Research Report
    • Open Access
  • [Presentation] Magnetic tomography imaging using a scanning hard X-ray nanoprobe at BL39XU SPring-82023

    • Author(s)
      Motohiro Suzuki
    • Organizer
      The First Experiments Workshop for the 4-ID POLAR Beamline at the Argonne Photon Source (APS)
    • Related Report
      2023 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Three-dimensional observation of magnetic microstructures by scanning X-ray magnetic tomography2023

    • Author(s)
      Motohiro Suzuki
    • Organizer
      2023 KPS Fall Meeting, Pioneer Symposium
    • Related Report
      2023 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Three-dimensional visualization of magnetic domain structures using X-ray magnetic micro-tomography2022

    • Author(s)
      Suzuki Motohiro
    • Organizer
      XOPT2022 International Conference on X-ray Optics and Applications
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Three-dimensional visualization of magnetic domain structures by X-ray magnetic tomography2022

    • Author(s)
      Suzuki Motohiro
    • Organizer
      ICMFS-2022, 24th International Colloquium on Magnetic Films and Surfaces
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Anomalous Hall effect and proximity induced magnetism in CoFe2O4/Pt interface2022

    • Author(s)
      S. Nodo, I. Yamane, M. Suzuki, S. Yokokura, T. Shimada, T. Nagahama
    • Organizer
      ICMFS-2022, 24th International Colloquium on Magnetic Films and Surfaces
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] X線磁気トモグラフィーによるスキルミオンひも構造の3次元形状の可視化2022

    • Author(s)
      鈴木基寛、関真一郎、石橋未央、高木里奈、Nguyen Duy Khanh、塩田陽一、柴田基洋、小椎八重航、十倉好紀、小野輝男
    • Organizer
      第35日本放射光学会年会・放射光科学合同シンポジウム
    • Related Report
      2021 Annual Research Report
  • [Presentation] XFEL照射によって誘起されるフェムト秒磁気ダイナミクス2022

    • Author(s)
      鈴木基寛、泉 瞭、岡部純、久保壮生、堀尾眞史、鷲見寿秀、和田哲弥、久保田雄也、宮西宏併、富樫 格、松田 巌、大河内拓雄、山田貴大、田中義人
    • Organizer
      第35日本放射光学会年会・放射光科学合同シンポジウム
    • Related Report
      2021 Annual Research Report
  • [Presentation] 可視光プローブ時間分解磁気顕微鏡の開発とXFEL誘起高速磁気ダイナミクスの解析2022

    • Author(s)
      泉 瞭、岡部純幸、久保壮生、久保田雄也、宮西宏併、富樫 格、大河内拓雄、山田貴大、松田 巌、和田哲弥、鷲尾眞史、鷲見寿秀、田中義人、鈴木基寛
    • Organizer
      第35日本放射光学会年会・放射光科学合同シンポジウム
    • Related Report
      2021 Annual Research Report
  • [Presentation] 磁気スキルミオンストリングの3次元形状の観察2022

    • Author(s)
      関真一郎、鈴木基寛、石橋未央、高木里奈、Nguyen Duy Khanh、塩田陽一、柴田基洋、小椎八重航、十倉好紀、小野輝男
    • Organizer
      日本物理学会第77回年次大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Visualizing three-dimensional magnetic domain structures by synchrotron-based magnetic X-ray microtomography2021

    • Author(s)
      Motohiro Suzuki
    • Organizer
      The 5th International Conference on Materials Engineering and The 6th International Conference on Nanotechnology and Nanomaterials in Energy
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 放射光によるNd-Fe-B焼結磁石の二次・三次元磁区解析2020

    • Author(s)
      鈴木基寛
    • Organizer
      日本学術振興会 結晶成長の科学と技術 第161委員会第116回研究会
    • Related Report
      2020 Annual Research Report
    • Invited
  • [Book] International Tables for Crystallography Vol. I (X-ray Absorption Spectroscopy and Related Techniques)2023

    • Author(s)
      Motohiro Suzuki
    • Total Pages
      800
    • Publisher
      International Union of Crystallograpy
    • Related Report
      2023 Annual Research Report
  • [Book] Nanomagnetic Materials, Fabrication, Characterization and Application2021

    • Author(s)
      Motohiro Suzuki, Eds. Akinobu Yamaguchi, Atsufumi Hirohata, Bethanie Stadler
    • Total Pages
      784
    • Publisher
      Elsevier
    • ISBN
      9780128223499
    • Related Report
      2021 Annual Research Report
  • [Remarks] 共同発表)最先端の永久磁石材料内部の微小磁石の振舞いを3次元で透視

    • URL

      https://www.kwansei.ac.jp/news/detail/4695

    • Related Report
      2022 Annual Research Report
  • [Remarks] 鈴木基寛・工学部教授ら研究グループが最先端の永久磁石材料内部の微小磁石の振舞いを3次元透視観察に成功

    • URL

      https://www.kwansei.ac.jp/news/detail/4696

    • Related Report
      2022 Annual Research Report
  • [Remarks] 磁石の中の竜巻(スキルミオンひも)の三次元形状の可視化に成功~新しい磁気情報処理手法の開拓に期待

    • URL

      https://www.kwansei.ac.jp/news/detail/4500

    • Related Report
      2021 Annual Research Report

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Published: 2020-04-28   Modified: 2025-01-30  

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