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Establishment of a method for quantitative evaluation of microstructures by serial sectioning using X-ray CT

Research Project

Project/Area Number 20K05146
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionMuroran Institute of Technology

Principal Investigator

Kusumoto Kenta  室蘭工業大学, 大学院工学研究科, 准教授 (30764998)

Co-Investigator(Kenkyū-buntansha) 清水 一道  室蘭工業大学, 大学院工学研究科, 教授 (60206191)
Project Period (FY) 2020-04-01 – 2023-03-31
Project Status Completed (Fiscal Year 2022)
Budget Amount *help
¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2022: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2021: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2020: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Keywordsエロージョン摩耗 / 高クロム白鋳鉄 / 炭化物の微細化 / X線CT / High Cr / Multicomponent / Titanium / Wear resistance / Carbide refinement / X ray CT / Erosive Wear / High chromium / Multi Alloys / Morphology of carbides / Erosive wear / Hi-Cr white cast iron / Titanium addition / Refinement / シリアルセクショニング / 凝固組織 / 組織制御 / 耐摩耗特性
Outline of Research at the Start

部材の耐摩耗性は機器の運用経費とも直接関係し,経済的な点からも摩耗は重要な技術課題となっている.申請者は,部材の摩耗寿命延長のため,高合金鋳造材料に着目し,金属材料中の微細な晶出・析出炭化物及び基地組織制御が耐熱耐摩耗特性に有効であることを実証してきた.しかし,炭化物の三次元形態や体積率等を二次元画像から求め,定量評価するのは極めて困難であった.
本研究では,耐熱耐摩耗材料の開発を目指して,シリアルセクショニングを援用した炭化物の形態および分布を三次元観察し,定量評価を行うことで,合金設計および評価手法を確立する.

Outline of Final Research Achievements

In this study, carbide morphology was observed using X-ray CT to quantitatively evaluate the effect of carbides on wear resistance. High-chromium white cast iron was used as the basic composition, and the carbon content was varied from 3.0% to 4.0 mass% and the titanium content from 0 to 2.0 mass%. X-ray CT showed that the carbide grain size ranged from 5 to 30 μm, decreasing with increasing titanium content. The dominant factors in high temperature erosion wear are carbide area fraction, carbide type, and high temperature hardness, but these factors have little effect in this cast iron family. On the other hand, a correlation was observed between the primary carbide grain size and wear rate. It was found that the wear resistance increase as carbide grain size decrease. Therefore, it is clear that the primary carbide grain size has a significant effect on wear resistance.

Academic Significance and Societal Importance of the Research Achievements

炭化物形態は粉体衝突時の塑性変形を抑制させる効果があり,中でも炭化物粒径が耐摩耗特性向上に寄与していることを定量的に明らかにしたことは,今後の耐熱耐摩耗合金開発における合金設計および微細組織観察手法として価値がある.今後,炭化物粒径のみならず,分布や体積を統計処理し,定量評価を試みることで,将来的に様々なニーズに応じた最適合金設計が可能となり,耐摩耗材料の新たな品質評価手法となり得る.

Report

(4 results)
  • 2022 Annual Research Report   Final Research Report ( PDF )
  • 2021 Research-status Report
  • 2020 Research-status Report
  • Research Products

    (23 results)

All 2023 2022 2021 2020

All Journal Article (6 results) (of which Peer Reviewed: 6 results) Presentation (17 results) (of which Int'l Joint Research: 6 results)

  • [Journal Article] Three-Body Abrasive Wear-Resistance Characteristics of a 27Cr-Based 3V-3Mo-3W-3Co Multicomponent White Cast Iron with Different Ti Additions2023

    • Author(s)
      Purba Riki Hendra、Shimizu Kazumichi、Kusumoto Kenta
    • Journal Title

      Journal of Manufacturing and Materials Processing

      Volume: 7 Issue: 1 Pages: 21-21

    • DOI

      10.3390/jmmp7010021

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Three-Body Abrasive Wear Performance of High Chromium White Cast Iron with Different Ti and C Content2022

    • Author(s)
      Huq Mohammad Jobayer、Shimizu Kazumichi、Kusumoto Kenta、Purba Riki Hendra
    • Journal Title

      Lubricants

      Volume: 10 Issue: 12 Pages: 348-348

    • DOI

      10.3390/lubricants10120348

    • Related Report
      2022 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of boron addition on three-body abrasive wear characteristics of high chromium based multi-component white cast iron2022

    • Author(s)
      Riki Hendra Purba, Kazumichi Shimizu, Kenta Kusumoto, Yila Gaqi, Takayuki Todaka
    • Journal Title

      Materials Chemistry and Physics

      Volume: 275 Pages: 125232-125232

    • DOI

      10.1016/j.matchemphys.2021.125232

    • Related Report
      2021 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effect of Carbon Content on Three-body Abrasive Wear Characteristics of 28Cr-3Ni Cast Alloys2021

    • Author(s)
      Takayuki Todaka, Kazumichi Shimizu, Kenta Kusumoto,Riki Hendra Purba, Yila Gaqi
    • Journal Title

      ISIJ International

      Volume: 61 Issue: 8 Pages: 2274-2283

    • DOI

      10.2355/isijinternational.ISIJINT-2021-099

    • NAID

      130008075207

    • ISSN
      0915-1559, 1347-5460
    • Year and Date
      2021-08-15
    • Related Report
      2021 Research-status Report
    • Peer Reviewed
  • [Journal Article] Erosive wear characteristics of high-chromium based multi-component white cast irons2021

    • Author(s)
      Purba Riki Hendra, Kazumichi Shimizu, Kenta Kusumoto, Takayuki Todaka, Masato Shirai, Hiroya Hara, Jun Ito
    • Journal Title

      Tribology International

      Volume: 159 Pages: 106982-106982

    • DOI

      10.1016/j.triboint.2021.106982

    • Related Report
      2021 Research-status Report
    • Peer Reviewed
  • [Journal Article] 熱応力解析による超硬合金鋳ぐるみ多合金白鋳鉄の割れおよび変形に対する予測手法の検討2020

    • Author(s)
      村瀬滋哉,清水一道,楠本賢太,松本大樹,長船康裕,リキ ヘンドラ プルバ
    • Journal Title

      鋳造工学

      Volume: 92 Pages: 339-344

    • NAID

      130007883117

    • Related Report
      2020 Research-status Report
    • Peer Reviewed
  • [Presentation] Effect of Carbide Orientation on Wear Characteristics of High-alloy Wear-resistant Cast Iron2022

    • Author(s)
      Kenta Kusumoto, Kazumichi Shimizu, Yila Gaqi, Riki Hendra Purba, Mohammad Jobayer Huq
    • Organizer
      The 74th World Foundry Congress
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Three-body Abrasive Wear Resistance of 5V/5Nb-5Cr-5Mo-5W-5Co-Fe Multi-component Cast Alloys with Different Carbon Percentage2022

    • Author(s)
      Riki Hendra Purba, Kazumichi Shimizu, Kenta Kusumoto, Yila Gaqi, Muhammad Jobayer Huq
    • Organizer
      The 74th World Foundry Congress
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of Carbon and Titanium Addition on Erosive Wear Behavior of High Chromium White Cast Irons2022

    • Author(s)
      Huq Mohammad Jobayer, Kazumichi Shimizu, Kenta Kusumoto, Riki Hendra Purba, Yila Gaqi
    • Organizer
      The 74th World Foundry Congress
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] High Temperature Erosive Wear Characteristics of High Chromium White Cast Iron with Ti Addition2022

    • Author(s)
      Yudai Momma, Kazumichi Shimizu, Kenta Kusumoto
    • Organizer
      The 74th World Foundry Congress
    • Related Report
      2022 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of Titanium Addition on Three Body Abrasive Wear Characteristics of High Chromium Based Multicomponent White Cast Iron2022

    • Author(s)
      Riki Hendra Purba, Kazumichi Shimizu, Kenta Kusumoto
    • Organizer
      日本鋳造工学会 第180回全国講演大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] Influence of Additional Carbon & Titanium Composition on Erosive Wear Characteristics of High Chromium White Cast Irons2022

    • Author(s)
      Mohammad Jobayer Huq, Kazumichi Shimizu, Kenta Kusumoto
    • Organizer
      日本鋳造工学会 第180回全国講演大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] 高クロム系多合金白鋳鉄の高温エロージョン摩耗特性に及ぼすチタン添加の影響2022

    • Author(s)
      門間雄大,清水一道,楠本賢太
    • Organizer
      日本鋳造工学会 第180回全国講演大会
    • Related Report
      2022 Annual Research Report
  • [Presentation] Effect of molybdenum addition on three-body abrasive wear behavior of high chromium white cast irons2021

    • Author(s)
      Riki Hendra Purba, Kazumichi Shimizu, Kenta Kusumoto
    • Organizer
      The 12th International Symposium on the Science and Processing of Cast Iron (SPCI-Ⅻ)
    • Related Report
      2021 Research-status Report
    • Int'l Joint Research
  • [Presentation] Effect carbon and titanum addition on erosive wear characteristics of high chromium white cast iron2021

    • Author(s)
      Yila gaqi, Kazumichi Shimizu, Kenta Kusumoto
    • Organizer
      The 12th International Symposium on the Science and Processing of Cast Iron (SPCI-Ⅻ)
    • Related Report
      2021 Research-status Report
    • Int'l Joint Research
  • [Presentation] 高合金系耐摩耗鋳造材料の組織制御および摩耗特性に関する研究2021

    • Author(s)
      楠本賢太
    • Organizer
      日本鋳造工学会第178回全国講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] 耐摩耗鋳鉄のエロージョン摩耗における炭化物形状の影響2021

    • Author(s)
      伊豆裕介、清水一道、楠本賢太
    • Organizer
      日本鋳造工学会第178回全国講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] チタンを添加した高クロム白鋳鉄の高温エロージョン摩耗特性2021

    • Author(s)
      門間雄大、清水一道、楠本賢太、YILAGAQI、根本雄大
    • Organizer
      日本鋳造工学会第177回全国講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] 高クロム白鋳鉄のアブレッシブ摩耗特性における及ぼすチタンの影響2021

    • Author(s)
      根本雄大、清水一道、楠本賢太、門間雄大
    • Organizer
      日本鋳造工学会第177回全国講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] 高クロム白鋳鉄の摩耗特性における炭素及びチタンの影響2021

    • Author(s)
      YILAGAQI、清水一道、楠本賢太、根本雄大、門間雄大
    • Organizer
      日本鋳造工学会第177回全国講演大会
    • Related Report
      2021 Research-status Report
  • [Presentation] 超硬合金鋳ぐるみ多合金白鋳鉄の高温エロージョン摩耗特性と接合要件2020

    • Author(s)
      根本雄大、清水一道、楠本賢太、村瀬滋哉、白井雅人、原宏哉、伊藤淳
    • Organizer
      日本鋳造工学会第176回全国講演大会
    • Related Report
      2020 Research-status Report
  • [Presentation] 共焦点レーダー顕微鏡を用いた過共晶Fe-C-Cr合金におけるM7C3炭化物の形成過程観察2020

    • Author(s)
      伊藤慎、河合秀樹、大石義彦、埜上洋、楠本賢太、清水一道、Tambang manik
    • Organizer
      日本鋳造工学会第176回全国講演大会
    • Related Report
      2020 Research-status Report
  • [Presentation] 高クロム系多合金白鋳鉄のアブレシブ摩耗特性に及ぼすB添加の影響2020

    • Author(s)
      作見智之、清水一道、楠本賢太、白井雅人、原宏哉、伊藤淳
    • Organizer
      日本鋳造工学会第176回全国講演大会
    • Related Report
      2020 Research-status Report

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Published: 2020-04-28   Modified: 2024-01-30  

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