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Development of precipitation-hardenable magnesium sheet alloys with strong and rapid age-hardening response

Research Project

Project/Area Number 20K15067
Research Category

Grant-in-Aid for Early-Career Scientists

Allocation TypeMulti-year Fund
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionNational Institute of Advanced Industrial Science and Technology

Principal Investigator

Bian Mingzhe  国立研究開発法人産業技術総合研究所, 材料・化学領域, 研究員 (30848320)

Project Period (FY) 2020-04-01 – 2022-03-31
Project Status Completed (Fiscal Year 2021)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2021: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2020: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywordsマグネシウム合金 / 時効硬化 / 混合エンタルピー / 原子半径 / 析出物 / Magnesium alloys / Age-hardening response / Precipitate / Atomic radius / Mixing enthalpy
Outline of Research at the Start

Solid-state precipitation is one of the most effective methods to strengthen various engineering alloys, particularly in 6xxx series aluminum alloys. However, the same approach has not been widely adopted in commercial Mg alloys due to their poor and sluggish age-hardening response. This research aims to develop a new precipitation-hardenable Mg alloy that shows strong and rapid age-hardening response.

Outline of Final Research Achievements

This project successfully developed new types of precipitation-hardenable Mg wrought alloys with quick age-hardening response. In addition, this project demonstrated that the mixing enthalpy value between the solute elements and the atomic radius of solute atoms are important factors in designing Mg alloys with fast aging kinetics. However, the hardness increment is rather low. Further work is required to enhance the hardness increment by the short-time artificial aging in order to compete with 6000 series Al alloys.

Academic Significance and Societal Importance of the Research Achievements

Precipitation has not been widely adopted in commercial magnesium alloys due to their poor and sluggish age-hardening response. This project aims to provide a knowledge platform that can provide us valuable insight into the formation mechanism of the precipitates in magnesium alloys.

Report

(3 results)
  • 2021 Annual Research Report   Final Research Report ( PDF )
  • 2020 Research-status Report
  • Research Products

    (22 results)

All 2022 2021 2020

All Journal Article (8 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 7 results,  Open Access: 1 results) Presentation (14 results) (of which Int'l Joint Research: 3 results)

  • [Journal Article] Improvement of deep drawing formability of Mg-6Al-1Zn magnesium alloy sheets with high strength utilizing aging precipitation2022

    • Author(s)
      Huang Xinsheng、Bian Mingzhe、Chino Yasumasa
    • Journal Title

      Scripta Materialia

      Volume: 215 Pages: 114709-114709

    • DOI

      10.1016/j.scriptamat.2022.114709

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Simulation-aided analysis on mechanical properties of dilute Mg-Zn-Ca alloy sheets2022

    • Author(s)
      Matsuoka Yusuke、Bian Mingzhe、Huang Xinsheng、Tsukada Yuhki、Koyama Toshiyuki、Chino Yasumasa
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 906 Pages: 164285-164285

    • DOI

      10.1016/j.jallcom.2022.164285

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Towards Improving Cold Formability of a Concentrated Mg-Al-Zn-Ca Alloy Sheet2022

    • Author(s)
      Bian Mingzhe、Huang Xinsheng、Chino Yasumasa
    • Journal Title

      Magnesium Technology 2022

      Volume: - Pages: 227-231

    • DOI

      10.1007/978-3-030-92533-8_38

    • ISBN
      9783030925321, 9783030925338
    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Substantial improvement in cold formability of concentrated Mg?Al?Zn?Ca alloy sheets by high temperature final rolling2021

    • Author(s)
      Bian Mingzhe、Huang Xinsheng、Chino Yasumasa
    • Journal Title

      Acta Materialia

      Volume: 220 Pages: 117328-117328

    • DOI

      10.1016/j.actamat.2021.117328

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Solute segregation assisted grain boundary precipitation and its impact to ductility of a precipitation-hardenable magnesium alloy2021

    • Author(s)
      Bian Mingzhe、Huang Xinsheng、Chino Yasumasa
    • Journal Title

      Materials Science and Engineering: A

      Volume: 819 Pages: 141481-141481

    • DOI

      10.1016/j.msea.2021.141481

    • Related Report
      2021 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 優れた室温成形性と強度を兼備したマグネシウム合金板材の開発に向けて2021

    • Author(s)
      Bian Mingzhe
    • Journal Title

      マグネシウム(日本マグネシウム研究会)

      Volume: 50-9 Pages: 3-5

    • Related Report
      2021 Annual Research Report
  • [Journal Article] Toward Development of Strong and Formable Magnesium Alloy Sheets with Bake-Hardenability2021

    • Author(s)
      T.T. Sasaki, M.-Z. Bian, Z.H. Li and K. Hono
    • Journal Title

      JOM

      Volume: 73 Issue: 5 Pages: 1471-1483

    • DOI

      10.1007/s11837-021-04613-1

    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructures and Mechanical Properties of Precipitation-Hardenable Magnesium-Silver-Calcium Alloy Sheets2020

    • Author(s)
      Mingzhe Bian, Xinsheng Huang and Yasumasa Chino
    • Journal Title

      Metals

      Volume: 10 Issue: 12 Pages: 1632-1632

    • DOI

      10.3390/met10121632

    • Related Report
      2020 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Presentation] 高温圧延法による難燃性マグネシウム合金の集合組織弱化メカニズムの解明2022

    • Author(s)
      Bian Mingzhe、黄 新ショウ、千野 靖正
    • Organizer
      日本金属学会2022年春期(第170回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Towards Improving Cold Formability of Concentrated Mg-Al-Zn-Ca Alloy Sheet2022

    • Author(s)
      Bian Mingzhe、黄 新ショウ、千野 靖正
    • Organizer
      TMS 2022 Annual Meeting & Exhibition
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 高温圧延法による難燃性マグネシウム合金圧延材の冷間成形性の大幅な改善2021

    • Author(s)
      Bian Mingzhe、黄 新ショウ、千野 靖正
    • Organizer
      軽金属学会 第141回秋期大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 日本金属学会2021年秋期(第169回)講演大会2021

    • Author(s)
      Bian Mingzhe、黄 新ショウ、千野 靖正
    • Organizer
      Ag含有量の最適化によるMg-xAg-0.1Ca/A5052セルフピアスリベット接合部の接合強度向上
    • Related Report
      2021 Annual Research Report
  • [Presentation] 熱間圧延による爆発圧着AZX611/A6005Cクラッド材の引張特性と界面結合強度の改善2021

    • Author(s)
      Bian Mingzhe、黄 新ショウ、斎藤 尚文、中津川 勲、千野 靖正
    • Organizer
      日本金属学会2021年秋期(第169回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 難燃性Mg-Ag-Ca合金圧延材の時効硬化特性の加速化について2021

    • Author(s)
      Bian Mingzhe、黄 新ショウ、千野 靖正
    • Organizer
      軽金属学会 第140回春期大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Development of precipitation-hardenable Mg-Ag based sheet alloys2021

    • Author(s)
      Bian Mingzhe、黄 新ショウ、千野 靖正
    • Organizer
      12th International Conference on Magnesium Alloys and their Applications (Mg2021)
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Improving Adhesive Bonding of Explosive-welded Magnesium/Aluminum Joints by Interface Design2021

    • Author(s)
      Bian Mingzhe、黄 新ショウ、斎藤 尚文、中津川 勲、千野 靖正
    • Organizer
      12th International Conference on Magnesium Alloys and their Applications (Mg2021)
    • Related Report
      2021 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Mg-Zn-Ca希薄合金圧延材の室温成形性に及ぼす亜鉛濃度の影響2021

    • Author(s)
      松岡 佑亮、黄 新ショウ、Bian Mingzhe、塚田祐貴、小山敏幸、千野 靖正
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Mg-Zn-Ca-Al-Mn系合金の機械的特性と室温成形性に及ぼすアルミニウム濃度の影響2021

    • Author(s)
      黄 新ショウ、Bian Mingzhe、中津川 勲、千野 靖正、佐藤 雅彦、山崎 一正、城戸 太司、上田 祐規、井上 正士
    • Organizer
      軽金属学会第140回春期大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Mg-Zn-Ca希薄合金圧延材の室温成形性 とその 決定 因子2021

    • Author(s)
      松岡 佑亮、Bian Mingzhe、黄 新ショウ、塚田 祐貴、小山 敏幸、千野 靖正
    • Organizer
      日本金属学会2021年秋期(第169回)講演大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] Mg-Zn-Ca希薄合金圧延材の室温成形性と亜鉛濃度の関係解明2021

    • Author(s)
      松岡 佑亮、Bian Mingzhe、黄 新ショウ、塚田 祐貴、小山 敏幸、千野 靖正
    • Organizer
      軽金属学会 第141回秋期大会
    • Related Report
      2021 Annual Research Report
  • [Presentation] 溶質偏析による粒界析出の誘起と析出強化型マグネシウム合金の延性への影響2021

    • Author(s)
      BIAN Mingzhe、黄新ショウ、千野靖正
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2020 Research-status Report
  • [Presentation] 析出硬化型Mg-Ag-Ca合金圧延材の開発2020

    • Author(s)
      BIAN Mingzhe、黄新ショウ、千野靖正
    • Organizer
      軽金属学会2020秋期(第139回)講演大会
    • Related Report
      2020 Research-status Report

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Published: 2020-04-28   Modified: 2023-01-30  

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